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景天三七多糖超声提取工艺研究
引用本文:杨艳俊,耿水连,吉慧杰,王亚红,祝波,曲小姝.景天三七多糖超声提取工艺研究[J].吉林化工学院学报,2014,31(9):17-20,49.
作者姓名:杨艳俊  耿水连  吉慧杰  王亚红  祝波  曲小姝
作者单位:吉林化工学院化学与制药工程学院,吉林吉林,132022
摘    要:在单因素试验的基础上,通过正交试验法对景天三七中多糖的超声提取工艺进行研究.探讨了超声温度、料液比、超声时间、提取次数对多糖提取效果的影响,并通过正交试验方法研究超声波辅助提取景天三七多糖的工艺条件.各因素影响多糖提取率的大小次序为:提取次数,料液比,超声时间,超声温度.超声提取景天三七多糖的最佳工艺参数是:提取温度50℃、料液比1 50、提取时间40 min、提取次数3次,在此最优条件下景天三七多糖的超声提取率为7.39%.本法准确可靠,重现性好,结果稳定,适合景天三七多糖的提取.

关 键 词:景天三七  多糖  超声提取  正交试验

Study on Ultrasonic Extraction Technology of Polysaccharide from Sedum Aizoom L.
YANG Yan-jun,GENG Shui-lian,JI Hui-jie,WANG Ya-hong,ZHU bo,QU Xiao-shu.Study on Ultrasonic Extraction Technology of Polysaccharide from Sedum Aizoom L.[J].Journal of Jilin Institute of Chemical Technology,2014,31(9):17-20,49.
Authors:YANG Yan-jun  GENG Shui-lian  JI Hui-jie  WANG Ya-hong  ZHU bo  QU Xiao-shu
Affiliation:YANG Yan-jun;GENG Shui-lian;JI Hui-jie;WANG Ya-hong;ZHU bo;QU Xiao-shu;College of Chemical and Pharmaceutical Engineering,Jilin Institute of Chemical Technology;
Abstract:On the basis of single factor experiments, the ultrasonic extraction process of polysaccharide from Sedum Aizoom L. was studied by orthogonal experimental method. Ultrasonic temperature, solid-liquid ratio, ultrasonic time, extraction times were discussed on the polysaccharide extraction effect. The results show that the order of the various factors influence respectively : extraction times, solid-liquid ratio, ultrasonic extraction time, ultrasonic extraction temperature. The optimum ultrasonic extraction conditions of Polysaccharide from Sedum Aizoom L. : Ultrasonic extraction temperature is 50℃, solid-liquid ratiois 1 : 50, ultrasonic extraction time is 40min, extraction times is 3, under this extraction condition the highest crude polysaccharide extraction yield was 7.39%.
Keywords:Sedum Aizoom L    polysaccharide  ultrasonic extraction  orthogonal test
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