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聚乳酸-石蜡微胶囊相变材料的制备及表征
引用本文:王锦成,郭曦,董星宇,徐楠,潘鑫辰,朱静涛.聚乳酸-石蜡微胶囊相变材料的制备及表征[J].塑料科技,2012,40(1):65-67.
作者姓名:王锦成  郭曦  董星宇  徐楠  潘鑫辰  朱静涛
作者单位:上海工程技术大学化学化工学院,上海,201620
基金项目:国家自然科学基金面上项目,上海市曙光计划项目,上海高校知识创新工程建设项目,上海市高校学科专业建设项目,上海市科委地方高校能力建设项目
摘    要:制备了以聚乳酸(PLA)为壁材、石蜡为芯材的相变储能微胶囊。采用红外光谱、扫描电镜、热失重分析仪和差示扫描量热仪分析了微胶囊的结构及性能。结果表明:PLA已包覆到石蜡上,该微胶囊的粒径为5~10μm;微胶囊的热稳定性能在一定范围内得到了较大程度的提高,在300℃以下无质量损失;微胶囊的储热能力高达170.52 J/g。

关 键 词:相变储能  微胶囊  聚乳酸  石蜡

Preparation and Characterization of PLA-Paraflin Wax Phase Change Microcapsules
Wang Jincheng , Guo Xi , Dong Xingyu , Xu Nan , Pan Xinchen , Zhu Jingtao.Preparation and Characterization of PLA-Paraflin Wax Phase Change Microcapsules[J].Plastics Science and Technology,2012,40(1):65-67.
Authors:Wang Jincheng  Guo Xi  Dong Xingyu  Xu Nan  Pan Xinchen  Zhu Jingtao
Affiliation:College of Chemistry and Chemical Engineering,Shanghai University of Engineering Science,Shanghai 20620,China
Abstract:The phase change and energy storage microcapsules were prepared by taking PLA as shell and paraffin wax as core.The structure and properties of the microcapsules were analyzed by FTIR,SEM,TGA and DSC.The results show that paraffin wax was successfully encapsulated by PLA,and the particle size of the microcapsules is about 5~10 μm;the thermal stability of the microcapsules improves obviously in a certain temperature range,and there is no mass loss below 300℃;the energy storage of the microcapsules reaches 170.52 J/g.
Keywords:Phase change and energy storage  Microcapsule  PLA  Paraffin wax
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