| 新型杀虫剂sulfoxaflor的合成与杀虫活性 |
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| 引用本文： | 武恩明,于海波,宋玉泉,梁博,王军锋,李斌.新型杀虫剂sulfoxaflor的合成与杀虫活性[J].农药,2011,50(1). |
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| 作者姓名： | 武恩明 于海波 宋玉泉 梁博 王军锋 李斌 |
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| 作者单位： | 沈阳化工研究院有限公司,新农药创制与开发国家重点实验室,沈阳110021 |
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| 摘 要： | 目的]Sulfoxaflor是由陶氏益农公司开发的新型杀虫剂,为了研究其杀虫活性,探索了其合成方法并进行了生物活性测试。结果]以四氢吡咯、正丁醛和4-乙氧基-1,1,1-三氟-3-丁烯-2-酮为起始原料制备了sulfoxaflor,经核磁、红外验证其结构。生测结果表明该化合物对刺吸式口器害虫蚜虫具有优异的杀虫活性。结论]选取了较佳的合成路线,对工业化生产具有一定的指导意义。可用于害虫抗性的治理。
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| 关 键 词： | sulfoxaflor 合成 杀虫活性 |
Synthesis and Insecticidal Activity of Sulfoxaflor |
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| WU En-ming,YU Hai-bo,SONG Yu-quan,LIANG Bo,WANG Jun-feng,LI Bin.Synthesis and Insecticidal Activity of Sulfoxaflor[J].Pesticides,2011,50(1). |
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| Authors: | WU En-ming YU Hai-bo SONG Yu-quan LIANG Bo WANG Jun-feng LI Bin |
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| Affiliation: | WU En-ming,YU Hai-bo,SONG Yu-quan,LIANG Bo,WANG Jun-feng,LI Bin(State Key Laboratory of the Discovery and Development of Novel Pesticide,Shenyang Research Institute of Chemical Industry co.,Ltd.,Shenyang 110021,China) |
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| Abstract: | Sulfoxaflor as a novel pesticide was developed by Dow AgroSciences LLC.In order to study the insecticidal activity of sulfoxaflor,the synthetic method and insecticidal activity were explored.Results] Sulfoxaflor was synthesized by pyrrolidine,butyraldehyde and 4-ethoxy-1,1,1-trifluorobut-3-en-2-one as starting materials,and its structure was confirmed by 1H NMR,IR.Preliminary bioassays indicated that sulfoxaflor exhibited good insecticidal activitiy against aphids.Conclusions] Sulfoxaflor was prepared wit... |
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| Keywords: | sulfoxaflor synthesis insecticidal activity |
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