| 聚六亚甲基胍基盐酸盐的合成 |
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| 引用本文： | 余磊,金学平,张婷,李健雄,卢凯.聚六亚甲基胍基盐酸盐的合成[J].陕西化工,2014(1):192-194. |
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| 作者姓名： | 余磊 金学平 张婷 李健雄 卢凯 |
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| 作者单位： | [1]武汉软件工程职业学院环境与生化工程学院,湖北武汉430205 [2]武汉桀升生物科技有限公司,湖北武汉430000 |
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| 摘 要： | 以己二胺和盐酸胍为原料,合成了聚六亚甲基胍基盐酸盐,研究了物料比、反应时间和反应温度对分子量的影响,建立了分子量与工艺条件的数学模型。对产物进行核磁共振表征,首次提出该聚合物在空间结构上可能以一个大环化合物的形式存在。
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| 关 键 词： | 聚六亚甲基胍基盐酸盐 合成 核磁共振 大环化合物 |
Synthesis of polyhexamethyleneguanidine hydrochloride |
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| YU Lei;JIN Xue-ping;ZHANG Ting;LI Jian-xiong;LU Kai.Synthesis of polyhexamethyleneguanidine hydrochloride[J].Applied Chemical Industry,2014(1):192-194. |
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| Authors: | YU Lei;JIN Xue-ping;ZHANG Ting;LI Jian-xiong;LU Kai |
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| Affiliation: | YU Lei;JIN Xue-ping;ZHANG Ting;LI Jian-xiong;LU Kai;Department of Environmental and Biochemical Engineering,Wuhan Vocational College of Software and Engineering;Wuhan Jiesheng Biological Technology Co.,Ltd.; |
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| Abstract: | Polyhexamethyleneguanidine hydrochloride was prepared by guanidine hydrochloride and hexamethylenediamine as raw materials. The impact of the reactional conditions on the molecular weight of the product was studied,and the mathematical model of the molecular weight and the conditions was established. The product was characterized by the 1H NMR,and it was proposed that the polymer may be macrocyclic compound. |
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| Keywords: | polyhexamethyleneguanidine hydrochloride synthesis 1H NMR macrocyclic compound |
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