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单分散Ni球制备及Ni/NiO的磁性研究
引用本文:刘先松 周圣强 黄凯 Udi Meridor Aviad Frydman Aharon Gedanken.单分散Ni球制备及Ni/NiO的磁性研究[J].稀有金属材料与工程,2006,35(9):1457-1460.
作者姓名:刘先松  周圣强  黄凯  Udi  Meridor  Aviad  Frydman  Aharon  Gedanken
作者单位:1. 安徽大学物理与材料学院,安徽,合肥,230093
2. The Physics Department and the Minerva Center, Bar-Ilan University, Ramat Gan 52900, Israel
3. Department of Chemistry, Bar-Ilan University, Ramat-Gan 52900, Israel
摘    要:使用微波辅助Poly方法制备了直径范围在100nm~180nm单分散的Ni球,用磁力显微镜(MFM)测其磁结构。进一步对Ni球表面氧化获得了高度球化的NicoreNiOshell结构,采用XRD,TEM,XPS和EDAX对其进行了测量分析,并用VSM和SQUID进一步讨论了铁磁/反铁磁的界面耦合效应。同时,估算了磁性交换偏置耦合场与颗粒尺寸的关系。

关 键 词:单分散Ni球  界面耦合  磁性
文章编号:1002-185X(2006)09-1457-04
收稿时间:2005-08-04
修稿时间:2005年8月4日

Monodispersed Ni Sphere Observation and Ni/NiO Magnetic Properties
Liu Xiansong,Zhou Shengqiang,Huang Kai,Udi Meridor,Aviad Frydman,Aharon Gedanken.Monodispersed Ni Sphere Observation and Ni/NiO Magnetic Properties[J].Rare Metal Materials and Engineering,2006,35(9):1457-1460.
Authors:Liu Xiansong  Zhou Shengqiang  Huang Kai  Udi Meridor  Aviad Frydman  Aharon Gedanken
Abstract:Monodispersed nickel spheres with diameters ranging from 100 nm to 180 nm were prepared by microwave-assisted(MW)polyol method.The magnetic stripe domain structure in these nickel spheres was measured by magnetic force microscopy(MFM).Furthermore,in this work we reported the formation of core-shell structures of highly globular NicoreNiOshell which were synthesized from the Ni spheres,and the magnetic properties of the core-shell structures have been investigated.
Keywords:monodispersed single-domain nickel spheres  interface coupling  magnetism
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