| 复方公英片质量标准的研究 |
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| 引用本文： | 植达诗,牟晓崟,袁遥.复方公英片质量标准的研究[J].中国药事,2010,24(3):280-282. |
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| 作者姓名： | 植达诗 牟晓崟 袁遥 |
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| 作者单位： | 广西玉林食品药品检验所,玉林,537000 |
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| 摘 要： | 目的建立复方公英片中板蓝根、蒲公英的薄层鉴别方法及板蓝根中腺苷的高效液相含量测定方法。方法采用Agilent C18色谱柱;流动相为甲醇-0.5%三乙胺溶液（8∶92）;流速为1.0mL.min-1;检测波长为260nm;柱温为25℃。结果腺苷在1.021~30.63μg范围内呈良好的线性关系,r=0.9994,平均回收率96.48%,RSD为1.18%（n=6）。结论该方法操作简便,重复性好,结果准确可靠,适用于该药的质量控制。
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| 关 键 词： | HPLC 复方公英片 腺苷 |
Study on the Establishment of the Quality Standard of Fufanggongying Tablets |
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| Zhi Dashi,Mu Xiaoyin,Yuan Yao.Study on the Establishment of the Quality Standard of Fufanggongying Tablets[J].Chinese Pharmaceutical Affairs,2010,24(3):280-282. |
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| Authors: | Zhi Dashi Mu Xiaoyin Yuan Yao |
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| Affiliation: | Zhi Dashi,Mu Xiaoyin* , Yuan Yao(Yulin Institute for Food , Drug Control,Yulin 537000) |
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| Abstract: | Objective To identify Radix Isatidis and Herba Taraxaci by TLC method and to determine adenosine in Fufanggongying Tablets by HPLC.Methods Using Agilent C18 column,methanol-0.5% triethylamine（8∶92） was mobile phase with the flow rate of 1.0mL·min-1.The detectve wavelength was 260nm and the column temperature was 25℃.Results The linear range of adenosine was 1.021～30.63μg（r=0.9994）.The average recovery rate was 96.48% with RSD as 1.18%（n=6）.Conclusion The method is simple,accurate and reliable.It can be used in the quality control of crude drug. |
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| Keywords: | HPLC |
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