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Microstructural and mechanical assessment of transient liquid phase bonded commercially pure titanium
Authors:Sajad Shakerin  Vahid Maleki  Seyyed Alireza Ziaei  Mohammad Reza Rahimipour  Seyyed Ehsan Mirsalehi
Affiliation:1. Department of Mining and Metallurgical Engineering, Amirkabir University of Technology (Tehran Polytechnic), Tehran, Iran;2. Department of Ceramic, Materials and Energy Research Center, Karaj, Iran
Abstract:Diffusion joining of commercially pure titanium was successfully prepared via transient liquid phase bonding in vacuum environment. The process was carried out using AMS 4772 silver-based filler alloy at 900–1000°C for various holding time under the vacuum of 6?×?10?7?Torr. Optical and scanning electron microscopy equipped with an EDS analyzer was conducted for microstructural evaluations. Mechanical properties were also investigated by shear test, fractographic assessment and X-ray diffraction analyses. The tendency to achieve isothermally solidified joint increased by increasing bonding time. No sign of athermal solidification was detected of sample bonded at 1000°C for 90?min. Consequently, the bonding condition of a high quality joint was obtained. Elemental analyses revealed that filler alloy’s elements (Ag, Cu) distributed more uniformly in fully isothermal solidified bond, whereas the aggregation of these elements is considerable in athermally solidified bond. Shear test results represented that the highest shear strength attributed to the sample bonded in isothermal solidified condition (bonded at 1000°C for 90?min).
Keywords:Commercially pure titanium  vacuum brazing  TLP bonding  solid solution  fracture surface
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