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| 狭瓣鹰爪花的生物碱成分研究 | |
| 引用本文： | 韩长日,朱国元,陈光英,张汉扬,毕和平,方宏勋.狭瓣鹰爪花的生物碱成分研究[J].中国中药杂志,2005,30(21):1660-1662. |
| 作者姓名： | 韩长日 朱国元 陈光英 张汉扬 毕和平 方宏勋 |
| 作者单位： | 1. 海南师范学院,化学系,海南海口571158 2. 香港城市大学,深圳研究院,广东,深圳,518057 3. 海南师范学院,化学系,海南海口571158;香港城市大学,生物及化学系,香港 4. 香港城市大学,生物及化学系,香港 5. 香港城市大学,深圳研究院,广东,深圳,518057;香港城市大学,生物及化学系,香港 |
| 摘 要： | 目的:研究海南狭瓣鹰爪花茎的生物碱成分。方法:生药用70%乙醇提取,提取物酸水溶解,酸水液氨水碱化后氯仿萃取,氯仿部位用硅胶柱色谱等色谱方法分离纯化,NMR等波谱法进行结构鉴定。结果:分离得到了8个生物碱类化合物,结构鉴定为spinosine(1),3-hydroxynornuciferine(2),juzirine(3),artabotrine(4),liridine(5),assim-ilobine(6),isococlaurine(7),-Ndemethylarmepavine(8)。结论:上述化合物均为首次从该植物中分得,化合物1,3,7,8为首次从该属植物分得。 |
| 关 键 词： | 狭瓣鹰爪花 化学成分 生物碱 |
| 文章编号： | 1001-5302（2005）21-1660-03 |
| 收稿时间： | 2004-10-10 |
| 修稿时间： | 2004-10-10 |
Studies on the alkaloids from stem of Artabotrys hainanensis |
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| HAN Chang-ri;ZHU Guo-yuan;CHEN Guang-ying;ZHANG Han-yang;BI He-ping;FANG Hong-xun.Studies on the alkaloids from stem of Artabotrys hainanensis[J].China Journal of Chinese Materia Medica,2005,30(21):1660-1662. | |
| Authors: | HAN Chang-ri;ZHU Guo-yuan;CHEN Guang-ying;ZHANG Han-yang;BI He-ping;FANG Hong-xun |
| Affiliation: | Department of Chemistry, Hainan Normal University, Haikou 571158, China. |
| Abstract: | Objective: To investigate the alkaloids from the stem of Artabotrys hainanensis.Method: Compounds in plant extracts were separated by silica gel and sephadex LH-20 column chromatography.Chemical structures were elucidated by chemical and spectral analyses including UV,1H-NMR,13C-NMR,ESIMS and ESI-MS-MS.Result: Eight alkaloids were isolated and identified as spinosine(1),3-hydroxynornuciferine(2),juzirine(3),artabotrine(4),liridine(5), assimilobine(6),isococlaurine(7),N-demethylarmepavine(8).Conclusion: All alkaloids were isolated from this plant for the first time and compounds 1,3,7 and 8 were isolated from genus Artabotrys for the first time. |
| Keywords: | Artabotrys hainanensis chemical constituents alkaloids |
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