| 三（5-氨基四唑）三嗪的合成与表征研究 |
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| 引用本文： | 郝晓春,毕福强,王磊,卜建华,葛忠学.三（5-氨基四唑）三嗪的合成与表征研究[J].陕西化工,2012(10):1852-1854. |
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| 作者姓名： | 郝晓春 毕福强 王磊 卜建华 葛忠学 |
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| 作者单位： | [1]西安近代化学研究所,陕西西安710065 [2]西安理工大学海军选培办,陕西西安710054 |
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| 摘 要： | 以5-氨基四唑和2,4,6-三氯-1,3,5-三嗪为起始原料,反应合成三（5-氨基四唑）三嗪。采用红外、核磁、元素分析、质谱等进行了表征。该化合物的含氮量高达77%。通过DSC研究分析,其分解温度高达296.6℃,具有对热稳定的性质。
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| 关 键 词： | 三（5-氨基四唑）三嗪 高氮化合物 热稳定性 |
Synthesis and characterization of TTAT |
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| HAO Xiao-chun,BI Fu-qiang,WANG Lei,BU Jian-hua,GE Zhong-xue.Synthesis and characterization of TTAT[J].Applied Chemical Industry,2012(10):1852-1854. |
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| Authors: | HAO Xiao-chun BI Fu-qiang WANG Lei BU Jian-hua GE Zhong-xue |
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| Affiliation: | 1.Xi＇an Modern Chemistry Research Institute,Xi＇an 710065,China;2.Navy Election Training Office, Xi＇an University of Technology,Xi＇an 710054,China) |
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| Abstract: | Tris（5-amino tetrazole） triazine was synthesized using 5-amino tetrazole and cyanuric chloride as starting materials.The structure has been identified by IR,13C NMR,element analysis,and MALDI-TOF-MS.The nitrogen-containing of the compound can reach 77%.DSC curve confirmed that it has thermal stability,and the temperature of analysis was 296.6 ℃. |
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| Keywords: | tris（5-amino tetrazole） triazine high nitrogen compound thermal stability |
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