| HPLC法测定仙乐雄胶囊中淫羊藿苷的含量 |
| |
| 引用本文： | 程世云,郝自新.HPLC法测定仙乐雄胶囊中淫羊藿苷的含量[J].安徽医药,2009,13(8):899-900. |
| |
| 作者姓名： | 程世云 郝自新 |
| |
| 作者单位： | 安徽省食品药品检验所,安徽,合肥,230051;安徽省安庆市药品检验所,安徽,安庆,246001 |
| |
| 摘 要： | 目的建立仙乐雄胶囊中淫羊藿苷的含量测定方法。方法采用高效液相色谱法测定。色谱柱：C18柱,流动相：乙腈-水（28∶72）,流速：1.0 ml.min-1,检测波长：270 nm。结果淫羊藿苷在0.104-1.040μg之间线性关系良好,r=0.9999;平均加样回收率为98.7%,（n=6,RSD=0.51%）。结论试验表明,该方法操作简单,分离效果好,灵敏度高,可以用于仙乐雄胶囊的质量控制。
|
| 关 键 词： | 仙乐雄胶囊 淫羊藿苷 含量测定 HPLC |
Determination of icariine in xianlexiong capsules by HPLC |
| |
| CHENG Shi-yun,HAO Zi-xin.Determination of icariine in xianlexiong capsules by HPLC[J].Anhui Medical and Pharmaceutical Journal,2009,13(8):899-900. |
| |
| Authors: | CHENG Shi-yun HAO Zi-xin |
| |
| Affiliation: | CHENG Shi-yun1,HAO Zi-xin2 (1.Anhui Provincial Institute for Food , Drug Control,Hefei 230051,2.Anqing Institute for Drug Control,Anqing 246001) |
| |
| Abstract: | Aim To establish an HPLC method for the determination of icariin in xianlexiong capsules.Methods C18 column was used.The mobile phase was acetonitrile-water（28∶72）.The flow rate was 1.0 ml·min-1.The detection wavelength was 270 nm.Results The linear range was from 0.104 to 1.040 μg（r=0.9999）and the average recovey was 98.7%（n=6,RSD=0.51%）.Conclusion The method is simple and sensitive with good separation efficiency.It can be used for routine quality control of xianlexiong capsules. |
| |
| Keywords: | HPLC |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
|
