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鳊肌肉中有机磷不同净化方法的对比研究
引用本文:崔雁娜,韦肖杭,姚伟忠,王俊,张敏,赵汉取.鳊肌肉中有机磷不同净化方法的对比研究[J].广东化工,2013(24):51-53.
作者姓名:崔雁娜  韦肖杭  姚伟忠  王俊  张敏  赵汉取
作者单位:浙江省淡水水产研究所,浙江湖州313001
基金项目:浙江省分析测试计划项目(2012C37064)
摘    要:为了找出一种更适合鳊肌肉中有机磷的净化方法.文章将鳊肌肉中有机磷提取液分别进行基质固相分散技术、SPE柱、GPC(全自动凝胶渗透色谱)净化,然后进行对比研究.表明:样品量大的情况下,并且资金足够,应选择GPC净化;样品量大资金不足,净化要求不高的情况下考虑选择分散固相净化;样品量少,资金不足但净化要求高,可以选择固相萃取柱净化.

关 键 词:鳊肌肉  有机磷  净化  基质固相分散  SPE柱  GPC

Comparative Study of Different Purification Methods of Organophosphorus in the Muscle of Parabramis Pekinensis
Cui Yanna,Wei Xiaohang*,Yao Weizhong,Wang Jun,Zhang Min,Zhao Hanqu.Comparative Study of Different Purification Methods of Organophosphorus in the Muscle of Parabramis Pekinensis[J].Guangdong Chemical Industry,2013(24):51-53.
Authors:Cui Yanna  Wei Xiaohang*  Yao Weizhong  Wang Jun  Zhang Min  Zhao Hanqu
Affiliation:(Zhejiang Institute of Freshwater Fisheries, Huzhou 313001, China)
Abstract:In order to find a more suitable method for purifying the muscle of parabramis pekinensis of organic phosphorus. Organophosphorus extracts of the muscle of Parabramis pekinensis were purified by matrix solid-phase dispersion technique, SPE columns purification, GPC (automatic gel permeation chromatography) purification, which were compared. The results show :Under large sample, and adequate funds case, GPC should be selected; Under large sample, lack of funds and low requirements for purification, case, dispersive solid phase purification should be selected; Under less sample, lack of funds case, but high requirements for purification, you can choose a solid-phase extraction column purification.
Keywords:themuscleofParabramispekinensis~ organic phosphorus: purification: matrix solid phase dispersion~ SPEcolumns: GPC
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