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混合醇与微波辅助提取姜黄素的工艺研究
引用本文:张丽,刘怀金,黄力,李扬,彭中,顾磊磊,杜还宇,阎建辉.混合醇与微波辅助提取姜黄素的工艺研究[J].广东化工,2009,36(10):14-15,43.
作者姓名:张丽  刘怀金  黄力  李扬  彭中  顾磊磊  杜还宇  阎建辉
作者单位:湖南理工学院,化学化工系,湖南,岳阳,414006
基金项目:湖南省科技计划项目,湖南省大学生研究性学习和创新性实验计划项目 
摘    要:文章通过单因素实验和正交实验相结合的方法对微波辅助乙醇、异丙醇两种混合醇提取姜黄中姜黄素的工艺条件进行了研究。以姜黄素的提取率为考察指标,在单医素实验的基础上,通过正交实验筛选出微波辅助混合醇提取姜黄素的最佳工艺条件为:乙醇与异丙醇的体积分数均为70%,乙醇与异丙酵体积比为7:3,混合醇用量为1:10,提取功率为400w,提取时间为4min。在此条件下姜黄素含量达到4.13%。

关 键 词:姜黄素  混合醇  微波提取  正交设计

Study on the Extraction Process of Curcumin in Curcuma longa L.with Mixed Alcohol Assisted by Microwave
Zhang Li,Liu Huaijin,Huang Li,Li Yang,Peng Zhong,Gu Leilei,Du Huanyu,Yan Jianhui.Study on the Extraction Process of Curcumin in Curcuma longa L.with Mixed Alcohol Assisted by Microwave[J].Guangdong Chemical Industry,2009,36(10):14-15,43.
Authors:Zhang Li  Liu Huaijin  Huang Li  Li Yang  Peng Zhong  Gu Leilei  Du Huanyu  Yan Jianhui
Affiliation:Zhang Li,Liu Huaijin,Huang Li,Li Yang,Peng Zhong,Gu Leilei,Du Huanyu,Yan Jianhui(Department of Chemistry and Chemical Engineering,Hunan Institute of Science and Technology,Yueyang 414006,China)
Abstract:To optimize the extraction process of mixed alcohol for curcumin in Curcuma longa L. assisted by microwave,the extraction process of Curcuma longa L. was studied by single factor level test and orthogonal tests.With the extraction percentage of curcumins as the optimum index, microwave assisted extracting optimum conditions were as follows: 70 % ethanol and 70 % was opropyl alcohol as extraction solvent, the volume ratios of mixed ethanol and isopropyl alcohol was 7 : 3, the use leve of mixed alcohol was 1 : 10, the microwave assisted extraction time was 4 rain and the power was 400 W. The content of curcumin was 4.13 % in the process.
Keywords:curcumin  mixed alcohol  microwave extraction  orthogonal design  
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