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| 杠柳根皮化学成分研究 | |
| 引用本文： | 王磊,殷志琦,张雷红,叶文才,张晓琦,沈文斌,赵守训.杠柳根皮化学成分研究[J].中国中药杂志,2007,32(13):1300-1302. |
| 作者姓名： | 王磊 殷志琦 张雷红 叶文才 张晓琦 沈文斌 赵守训 |
| 作者单位： | 1. 中国药科大学,天然药物化学教研室,江苏,南京,210038 2. 中国药科大学,天然药物化学教研室,江苏,南京,210038;暨南大学,中药及天然药物研究所,广东,广州,510632 3. 暨南大学,中药及天然药物研究所,广东,广州,510632 4. 中国药科大学,分析测试中心,江苏,南京,210009 |
| 摘 要： | 目的：对杠柳根皮的化学成分进行研究。方法：采用色谱技术进行分离,通过NMR等谱学方法确定化合物的结构。结果：分离并鉴定了8个化合物,分别为异香草醛(1),香草醛(2),4-甲氧基水杨酸(3),(24R)-9,19-cycloart-25-ene-3β,24-diol(4),(24S)-9,19-cycloart-25-ene-3β,24-diol(5),cycloeucalenol(6),β-香树脂醇乙酸酯(7),α-香树脂醇(8)。结论：化合物1～6为首次从杠柳中分离得到,并首次从杠柳属植物中分离得到环阿尔廷型三萜化合物4～6。 |
| 关 键 词： | 杠柳 化学成分 |
| 文章编号： | 1001-5302（2007）13-1300-03 |
| 收稿时间： | 2006-10-23 |
| 修稿时间： | 2006-10-23 |
Chemical constituents from root barks of Periploca sepium |
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| WANG Lei; YIN Zhi-qi; ZHANG Lei-hong; YE Wen-cai;; ZHANG Xiao-qi; SHEN Wen-bin; ZHAO Shou-xun.Chemical constituents from root barks of Periploca sepium[J].China Journal of Chinese Materia Medica,2007,32(13):1300-1302. | |
| Authors: | WANG Lei; YIN Zhi-qi; ZHANG Lei-hong; YE Wen-cai;; ZHANG Xiao-qi; SHEN Wen-bin; ZHAO Shou-xun |
| Affiliation: | 1. Department of Phytochemistry, China Pharmaceutical University, Nanjing 210038, China; 2. Institute of Traditional Chinese Medicine and Natural Products, Jinan University, Gucmgzhou 510632, China; 3. Center of Instrumental Analysis , China Pharmaceutical University, Nanjing 210009 , China |
| Abstract: | OBJECTIVE: To investigate the chemical constituents of the root barks of Periploca sepium. METHOD: Column chromatographic techniques were used to isolate the chemical constituents. NMR and MS methods were employed for their structural elucidation. RESULT: Eight compounds were isolated and identified as isovanillin (1), vanillin (2), 4-methoxysalicylic acid (3), (24R)-9, 19-cycloart-25-ene-3beta, 24-diol (4), (24S)-9, 19-cycloart-25-ene-3beta, 24-diol (5), cycloeucalenol (6), beta-amyrin acetate (7) and alpha-amyrin (8). CONCLUSION: Compounds 1-6 were isolated from this plant for the first time. |
| Keywords: | Periploca sepium chemical constituents |
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