| 多枝状PdCu纳米合金的结构表征及其电催化性能研究 |
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| 引用本文： | 刘美梅,沈闽,李小燕.多枝状PdCu纳米合金的结构表征及其电催化性能研究[J].电子显微学报,2016(3):201-206. |
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| 作者姓名： | 刘美梅 沈闽 李小燕 |
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| 作者单位： | 1. 中国科学院福建物质结构研究所,福建 福州,350002;2. 福建江夏学院,福建 福州,350108 |
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| 基金项目： | 国家自然科学基金资助项目(No．21271170)． |
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| 摘 要： | 本文采用一锅法制备钯铜纳米材料（ PdCu），并对PdCu纳米颗粒形貌、成分及微观结构进行表征。 X射线衍射仪（ XRD）和透射电子显微镜（ TEM）结果表明，PdCu纳米颗粒呈单分散的复杂多枝状结构。多枝状PdCu颗粒的产率高达90％左右，其粒径大小约为（30.85±8.68） nm。乙醇的循环伏安法与计时安培法测试表明PdCu多枝合金有良好的乙醇电催化性能和循环稳定性。
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| 关 键 词： | Pd-Cu TEM XRD 良好的电催化性能 循环稳定性 |
Characterization and electrocatalytic performance of branched PdCu alloy nanocatalysts |
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| Abstract: | In this paper, a PdCu nanomaterial had been synthesized via a simple Wet Chemical method. The morphology, microstructures and chemistry of PdCu were characterized by X-ray diffraction(XRD) and transmission electron microscopy (TEM). The results showed that PdCu nanoparticles were monodisperse spherical and multibranched shapes. The yield of branched PdCu were approximately 90%. The average size of branched PdCu nanoparticles was ( 30. 85 ± 8. 68 ) nm. PdCu nanocrystals showed superior electrocatalytical performance with excellent cyclic stability. |
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| Keywords: | Pd-Cu TEM XRD superior electrical catalytical performance cyclic stability |
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