| 微波消解-端视ICP-AES法测定食用明胶中铅、铬和砷 |
| |
| 引用本文： | 鲁丹.微波消解-端视ICP-AES法测定食用明胶中铅、铬和砷[J].食品与发酵工业,2008,34(9). |
| |
| 作者姓名： | 鲁丹 |
| |
| 作者单位： | 浙江出入境检验检疫局技术中心,浙江杭州,310012 |
| |
| 摘 要： | 建立了同时测定食用明胶中铅、铬和砷的新方法。试样经微波消解后用端视电感耦合等离子体原子发射光谱(ICP-AES)法同时测定。对仪器的工作参数进行了优化和选择。铅、铬和砷的检出限分别为0.002,0.000 8,0.004 mg/L;定量限分别为0.066,0.026,0.13 mg/kg。相对标准偏差为0.89%～2.71%,回收率为94.0%～106.0%。该法操作简便、快速,结果准确,适用于食用明胶中铅、铬和砷的快速测定。
|
| 关 键 词： | 微波消解 端视ICP-AES 食用明胶 铅 铬 砷 |
Determination of Pb, Cr and As in Edible Glutin by Microwave Digestion-Axial View ICP-AES |
| |
| Lu Dan.Determination of Pb, Cr and As in Edible Glutin by Microwave Digestion-Axial View ICP-AES[J].Food and Fermentation Industries,2008,34(9). |
| |
| Authors: | Lu Dan |
| |
| Abstract: | A new method for the simultaneous determination of Pb,Cr,and As in edible glutin was established.Samples were digested with microwave and determined by axial view ICP-AES.The plasma parameters were optimized and selected.The detection limits of Pb,Cr and As were 0.002、0.000 8 and 0.004mg/L.The LOQ was 0.066、0.026 and 0.13 mg/kg.The relative standard deviations was 0.89%~2.71%.The recovery was 94.0 %~ 106.0 %.The method was simple,rapid,accurate and suitable for determination of Pb,Cr and As in edible glutin. |
| |
| Keywords: | microwave digestion axial view ICP-AES edible glutin Pb Cr As |
| 本文献已被 维普 万方数据 等数据库收录！ |
|
