| 火焰原子吸收光谱法测定大青盐中微量钾、钙和镁的含量 |
| |
| 引用本文： | 刘晓芳,萨力塔娜提,徐鸿,尹丽,李革.火焰原子吸收光谱法测定大青盐中微量钾、钙和镁的含量[J].中国药房,2012(15):1389-1391. |
| |
| 作者姓名： | 刘晓芳 萨力塔娜提 徐鸿 尹丽 李革 |
| |
| 作者单位： | 新疆维吾尔自治区食品药品检验所 |
| |
| 基金项目： | “十一五”国家科技支撑计划项目子课题(2006BAI55B02-09) |
| |
| 摘 要： | 目的:建立测定大青盐中钾、钙和镁含量的方法。方法:采用标准加入法,用火焰原子吸收光谱法测定大青盐中微量钾、钙和镁的含量。结果:钾、镁的进样浓度均在0.4～10.0mg.L-1,钙在0.4～30.0mg.L-1范围内遵循朗伯比尔定律;钾、钙、镁的平均加样回收率分别为109.6%、101.8%、94.7%,RSD分别为2.43%、2.81%、5.00%(n均为9)。结论:该方法专属性强、简便易行、灵敏度高,可用于矿物药大青盐中微量钾、钙和镁的限量控制。
|
| 关 键 词： | 大青盐 钾 钙 镁 火焰原子吸收光谱法 含量测定 |
Determination of Potassium,Calcium and Magnesium in Halitum by Flame Atomic Absorption Spectrometry |
| |
| LIU Xiao-fang,Salitanati,XU Hong,YIN Li,LI Ge.Determination of Potassium,Calcium and Magnesium in Halitum by Flame Atomic Absorption Spectrometry[J].China Pharmacy,2012(15):1389-1391. |
| |
| Authors: | LIU Xiao-fang Salitanati XU Hong YIN Li LI Ge |
| |
| Affiliation: | (Xinjiang Uygur Autonomous Region Institute for Food and Drug Control,Urumqi 830002,China) |
| |
| Abstract: | OBJECTIVE:To establish the method for the content determination of potassium,calcium and magnesium in halitum.METHODS:By using standard join method,the contents of potassium,calcium and magnesium in halitum were determined by flame atomic absorption spectrometry.RESULTS:The results showed that Beer’s law was kept in the range of 0.4～10.0 mg·L-1 for potassium and magnesium and 0.4～30.0 mg·L-1 for calcium under certain conditions.Average recoveries were 109.6%(RSD=2.43%,n=9),101.8%(RSD=2.81%,n=9) and 94.7%(RSD=5.00%,n=9).CONCLUSION:The method is specific,simple and sensitive.It can be used for the limit control of potassium,calcium and magnesium in halitum. |
| |
| Keywords: | Halitum Potassium Calcium Magnesium Atomic absorption spectrometry Content determination |
| 本文献已被 CNKI 维普 等数据库收录！ |
|
