Preparation and luminescent properties of Cr3+:Al2O3 nano-powders by low-temperature combustion synthesis |
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Authors: | Xiaoyun Mi Xiyan Zhang Xuewei Ba Zhaohui Bai Liping Lu Xiaochun Wang Quansheng Liu |
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Affiliation: | 1. School of Material Science and Engineering, Changchun University of Science and Technology, No. 7989, Weixing Road, Changchun 130022, China;2. Chemistry and Chemical Engineering Institute, Qiqihar University, Qiqihar 161006, China |
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Abstract: | Cr3+:Al2O3 nano-powders were prepared through low-temperature combustion synthesis (LCS) method by using glucose as a dispersion agent for the first time. The Cr3+:Al2O3 nano-powders samples were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM) and luminescence spectrometer. XRD results showed that pure α-Al2O3 phase was obtained for the sample fired at 1100 °C for 0.5 h. TEM results indicated that nano-powders were well dispersed. Luminescence spectrum analysis results indicated that the excitation spectrum of Cr3+:Al2O3 nano-powders consisted of two bands peaking at 462 nm and 579 nm, respectively, and the emission spectrum consisted of two bands peaking at 692 nm and 668 nm, respectively. |
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