Preparation and mechanical properties of Ti3SiC2/SiC functionally graded materials

Ti₃SiC₂/SiC functionally graded materials (FGMs) were prepared via hot-pressing sintering followed by positioning impregnation. Positioning impregnation is a novel technique for local impregnation targeted at graded layers that exhibit poor sintering behaviour. The positioning impregnation process significantly densified layers with SiC volume fractions of more than 70% while only slightly affecting the densities of the other layers and preserving sufficiently weak interfaces between layers. FGMs that were hot pressed at 1600 and 1700 °C and then subjected to impregnation showed not only high flexural strengths but also zigzag load-displacement behaviour. The flexural strengths of these FGMs were 436 and 485 MPa, respectively; in comparison, the values for the FGMs without impregnation that were hot pressed at 1600, 1700 and 1800 °C were 235, 268 and 328 MPa, respectively. Moreover, the fracture toughnesses of these FGMs were 8.23 and 7.15 MPa m^1/2, respectively; in comparison, the values for the FGMs without impregnation that were hot pressed at 1600, 1700 and 1800 °C were 6.77, 7.05 and 4.65 MPa m^1/2, respectively.