| 上感冲剂质量标准研究 |
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| 引用本文： | 杨惠,高婷婷,高传忠.上感冲剂质量标准研究[J].中国实用医药,2009,4(30):22-23. |
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| 作者姓名： | 杨惠 高婷婷 高传忠 |
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| 作者单位： | 1. 安徽省铜陵市药品检验所,244100
2. 铜陵市有色职工总医院 |
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| 摘 要： | 目的建立上感冲剂质量标准。方法采用薄层色谱法对处方中的板蓝根、大青叶进行定性鉴别,用高效液相色谱法测定处方中连翘中连翘苷的含量。结果薄层色谱法阴性对照无干扰;连翘苷在14.016～70.080μg/ml。表明连翘苷在范围内呈良好的线性关系（r=0.9999,n=5）,平均回收率为98.0%,RSD=0.86%（n=9）。结论所建立的方法可准确地进行定性、定量检测,可用于该制剂的质量控制。
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| 关 键 词： | 大青叶 板蓝根 连翘苷 薄层色谱法 高效液相色谱法 |
Study on quality standard of Shanggan granules |
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| YANG Hui,GAO Ting-ting,GAO Chuan-zhong.Study on quality standard of Shanggan granules[J].China Practical Medical,2009,4(30):22-23. |
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| Authors: | YANG Hui GAO Ting-ting GAO Chuan-zhong |
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| Affiliation: | (Anhui Tongling Medicine Checking Institution, Tongling ,Anhui 244000, China) |
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| Abstract: | Objective Aim The quality specification for Shanggan granules was established.Methods Fofium isatidis and Radi isatidis were identified by TLC.The forsyth content was determinated by HPLC.Results The negative sample didn t interfere the identification of TLC.The 1inear relation was good within the range of 14.016～70.080 μg/ml（r=0.9999,n=5）for forsyth,The average recovery was 98.0%,RSD =0.86%（n=9）.Conclusion The method was simple,accurate,reliable and reproducible.It could be used in the quality contro1 of Shanggan granules. |
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| Keywords: | Fofium isatidis Radi isatidis forsyth TLC HPLC |
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