| 绿色合成丁二酰丁二酸二甲酯工艺研究 |
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| 引用本文： | 肖友军,张志军,刘燕.绿色合成丁二酰丁二酸二甲酯工艺研究[J].山西大学学报(自然科学版),2011(Z2):39-42. |
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| 作者姓名： | 肖友军 张志军 刘燕 |
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| 作者单位： | 江西理工大学材料与化学工程学院;山西大学化学化工学院; |
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| 摘 要： | 采用丁二酸二甲酯与甲醇钠反应,以丁二酸二甲酯做溶剂通过克莱森缩合和狄克曼缩合合成丁二酰丁二酸二甲酯,并通过正交试验得到绿色合成的工艺路线.
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| 关 键 词： | 丁二酰丁二酸二甲酯 克莱曼缩合 狄克曼缩合 正交试验 |
Technology Research on Green Synthesis of Dimethyl Succinylsuccinate |
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| XIAO You-jun,ZHANG Zhi-jun,LIU yan.Technology Research on Green Synthesis of Dimethyl Succinylsuccinate[J].Journal of Shanxi University (Natural Science Edition),2011(Z2):39-42. |
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| Authors: | XIAO You-jun ZHANG Zhi-jun LIU yan |
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| Affiliation: | XIAO You-jun1,ZHANG Zhi-jun1,LIU yan2(1.College of Material and Chemical Engineering,Jiangxi University of Science and Technology,Ganzhou 341000,China,2.School of chemistry and Chemical Engineering,Shanxi University,Taiyuan 030006,China) |
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| Abstract: | Dimethyl succinate and sodium methoxide,through reaction with Claisen condensation and DiKemann condensation synthesis dimethyl succinylsuccinate,in the presence of dimethyl succinate used as the reaction solven and get the green synthesis route by orthogonal test. |
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| Keywords: | dimethyl succinylsuccinate claisen condensation DiKemann condensation orthogonal test |
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