氯化氢合成炉的数值模拟分析

根据传统氯化氢合成炉特点,运用计算流体力学软件建立合成炉数学模型。通过对氯化氢燃烧工艺过程理论模拟,分析了氯化氢合成反应热分布规律。     

1 kHz步进低噪声YIG调谐微波频率综合器

低噪声微波频率综合器在现代电子系统和高性能测试系统中起着非常重要的作用,其实现方式通常以压控振荡器(VCO)和YIG调谐振荡器锁相频率合成为主。基于4~9 GHz YIG调谐振荡器,通过VCO合成小步进可变参考,使锁相环路在不降低鉴相频率的前提下,设计了完成高分辨率、低杂散的宽带低噪声YIG频率综合器。技术验证样品测试结果表明,在4~9 GHz工作带宽内频率步进为1 k Hz,相位噪声优于-95d Bc@10 k Hz,-115 d Bc@100 k Hz,其软硬件设计支持连续扫频和合成扫频功能,工作性能稳定可靠,可满足工程中本振和信号源应用需求。     

新型高精度数控交流恒流源的设计

基于直接数字频率合成技术设计了一种新型高精度数控交流恒流源系统。该系统由低频正弦信号发生器和恒流源电路组成,其中正弦信号发生器由STM32单片机搭建,恒流源电路在功率放大电路的基础上添加反馈网络,使新型恒流源具有更高的输出精度和更好的幅值稳定性。测试结果显示：该恒流源输出电流的幅值、频率、相位、输出时长可控,具有工作稳定好、精度高、噪声小的特点。     

一种超宽带线性调频信号源的设计

超宽带雷达因其距离分辨率高、抗干扰能力强、目标检测和识别能力高等优点,受到世界各国的重视。通常采用倍频器来产生超宽带信号,然而,倍频环节中存在一些影响信号质量的非理想特性。针对该问题,提出利用频谱拼接技术来产生超宽带雷达信号。采样频率越大则输出信号幅度包络失真越小。频谱拼接时间误差小于100 ns时,其主瓣比理想情况增大5%。通过频谱拼接技术能够有效解决幅度失真、高采样频率需要和拼接时间误差等问题。设计了两个直接数字频率合成器同步电路,确保两路正交基带信号同步。频谱拼接技术还能灵活控制信号带宽大小,产生较理想的超宽带线性调频信号。     

基于导航系统的低功耗全集成频率综合器设计

针对双模卫星导航接收系统对集成度、功耗和面积的需求,研究了频率综合器的电路结构和频率规划,分析了频率综合器环路的参数设计,实现了片上集成环路滤波器,版图采用MIM和MOS电容堆叠的方式节省了面积,电容电阻采用了加权的方式,使环路带宽可调.采用高速TSPC结构的D触发器构成双模预分频器,降低了整体电路的功耗.利用基于0.18 μmRF CMOS工艺实现了低功耗全集成的频率综合器,芯片面积0.88 mm2,功耗18.5 mW,相位噪声-94 dBc/Hz@100 kHz,杂散-68 dBc.测试结果证明了该电路系统参数设计和结构改进是合理和有效的,各参数性能满足系统要求.     

基于DDS与PLL的C波段全相参雷达频综设计

提出了一种直接数字频率合成(DDS)与锁相环(PLL)相结合的全相参频率合成方案。运用HMC704控制压控振荡器(VCO)设计高性能锁相本振源,将AD9910在基带产生的线性调频(LFM)脉冲调制信号经二次变频搬移到C波段,改善了输出信号的相噪和杂散,降低了系统的复杂性。实现了低相噪,低杂散,窄步进的C波段全相参雷达频综。结果表明,该频综在C波段输出LFM信号的幅度大于10dBm,频率步进为1kHz,相位噪声优于-103dBc/Hz@1kHz,各项指标均满足实际工程要求。     

C频段宽带低杂散频率合成器的设计与实现

在此介绍了小数分频锁相频率合成器的相关理论。设计一个带宽为580 MHz、杂散抑制度≤-60 d Bc、相位噪声≤-85 d Bc/Hz@10 k Hz的C频段宽带低杂散频率合成器。利用双环锁相频率合成技术和小数分频锁相技术,实现了宽带、低杂散的锁相频率合成器的设计。最后经过测试近端杂散指标≤-60 d Bc,远端杂散指标≤-70 d Bc,偏移10 k Hz的相位噪声为-89.95 d Bc/Hz,技术指标都优于设计要求。     

Full Automated Synthesis of18F-FDOPA and Preliminary PET/CT Imaging

¹⁸F-fluoro-L-dihydroxyphenylalanine (¹⁸F-FDOPA) as a dopamine neurotransmitter imaging agent has been widely used for diagnosis and therapy evaluation of Parkinson's disease, brain tumors and neuroendocrine diseases with positron emission tomography (PET) imaging in clinical setting and research. To meet the increasing clinical demand in oncology and neurology, a routine protocol for the automated synthesis of¹⁸F-FDOPA with a disposable cassette system on an imported multifunctional synthesizer was studied and discussed.¹⁸F-FDOPA was automatically synthesized via a multiple-step reaction, including fluorination, reduction, iodization alkylation and hydrolysis, following purification by using a semi-preparative high-performance liquid chromatography (HPLC) system which was built in the multifunctional synthesizer. After HPLC purification, the purified¹⁸F-FDOPA solution was collected and passed through a sterilizing filter into a collection bottle. The final¹⁸F-FDOPA injection was obtained for quality control (QC) determination. The QC indexes of the final products were detected： the injection was colorless and transparent, pH value was at 4 to 5.5, radiochemical purity >98%, radionuclide purity >99%, specific activity >1.9 GBq/μmol, K_2.2.2 content <50 mg/L, methanol content <0.01%, alcohol content <0.01%, dichloromethane content <0.01 mg/L, dimethylformamide content <15 mg/L, bacterial endotoxin test <0.100 EU/mL, sterility test 0 cfu/mL,and abnormal toxicity test was negative. PET/CT imaging of rats was performed by intravenous injection of¹⁸F-FDOPA half an hour after the intraperitoneal injection of carbidopa, PET/CT scan was performed after 100 min post-injection. The imaging of¹⁸F-FDOPA showed symmetry high uptake in the bilateral striatum of normal rats. The decay-corrected radiochemical yield of¹⁸F-FDOPA from the¹⁸F-fluoride was (63.1±3.8)% (n=10) at the end of synthesis (EOS), the radiochemical purity was no less than 98%, and the total radiosynthesis time was within 80 min. The quality control results demonstrated that the quality indexes of the final injection solution met the relevant requirements of radiopharmaceutlcals, which were well-suited for clinical application. An efficient and high reproducible automatic method for the radiosynthesis of¹⁸F-FDOPA with high radiochemical yields and good radiochemical purity is obtained and performed via a multi-step reaction on the multifunctional synthesizer.¹⁸F-FDOPA can be used for animal and human PET imaging.     

可编程模拟雷达信号源的设计

设计了一种可通过软件灵活控制的模拟雷达信号源,采用Silicon公司C8051F340微处理器芯片,控制直接数字频率合成芯片AD9858输出模拟雷达信号.文中说明了电路设计结构和软件设计方法,并对信号源的性能进行了可行性验证.     

基于DDS的激光频率高精度控制系统及其应用

在诸如激光冷却原子、光频标和冷原子干涉等实验中,通常采用压控振荡器（VCO）技术对激光移频,但是移频精度和稳定性不能满足实验要求。本文提出并研制了一种直接数字频率合成器（DDS）及其专用高精度时序控制系统用于激光的移频。DDS基于AD9852芯片,配合微控制器（MCU）控制其参数,输出经功率放大后直接驱动声光调制器以调...