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本文论述了利用气相色谱法检测石脑油中含氧化合物的方法,考察了无阀切换技术、分离模式的设计、操作条件的优化等方面的问题。提出利用多维气相色谱法,采用一根非极性柱和一根极性柱进行独立和串联分离,通过改变辅助载气压力的无阀切换方式进行柱分离,应用双FID检测器进行信号检测,数据利用Agilent的chemestation工作站采集和输出。该方法操作简单,分析时间在23 min以内,重复测定结果的相对标准偏差(RSD)小于1.5%,标准加入回收率在95~105%范围内,方法准确可靠。 相似文献
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FU Xin XIE Haibo YANG Huayong JIA Zhijian & FANG Qun . State Key Laboratory of Fluid Power Transmission Control Zhejiang University Hangzhou China . Institute of Microanalytical Systems Zhejiang University Hangzhou China 《中国科学E辑(英文版)》2005,48(3):326-337
Micro fluidic analysis technology has been developed rapidly since the 1990s. The essentials of the technology are fabricating the micron structure (usually net channels, 20―100 μm wide and 10―30 μm deep) in chips by micro processing, and analyzing the fluids of samples or reagents chemically when they are controlled to flow and to be mixed in the micro structures. The occurrence of the technology makes the miniaturiza-tion, integration and portability of chemical detecting devices possibl… 相似文献
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基于MEMS的微泵研究进展 总被引:7,自引:0,他引:7
主要介绍了基于MEMS的微泵 10年来的研究成果和研究现状。微泵是微电子机械系统(MEMS)中重要的执行器件 ,在系统中占有很重要的地位。微泵可以分为有阀泵和无阀泵两大类 ,一般来说 ,有阀泵的制造工艺和应用技术比较成熟 ,但存在加工尺寸限制和使用寿命的问题 ;无阀泵的原理新颖 ,结构相对简单 ,更适合微型化发展 ,是目前研究的热点。 相似文献
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Microchannel heat sink with high heat transfer coefficients has been extensively investigated due to its wide application prospective in electronic cooling. However, this cooling system requires a separate pump to drive the fluid transfer, which is uneasy to minimize and reduces their reliability and applicability of the whole system. In order to avoid these problems, valveless piezoelectric pump with fractal-like Y-shape branching tubes is proposed. Fractal-like Y-shape branching tube used in microchannel heat sinks is exploited as no-moving-part valve of the valveless piezoelectric pump. In order to obtain flow characteristics of the pump, the relationship between tube structure and flow rate of the pump is studied. Specifically, the flow resistances of fractal-like Y-shape branching tubes and flow rate of the pump are analyzed by using fractal theory. Then, finite element software is employed to simulate the flow field of the tube, and the relationships between pressure drop and flow rate along merging and dividing flows are obtained. Finally, valveless piezoelectric pumps with fractal-like Y-shape branching tubes with different fractal dimensions of diameter distribution are fabricated, and flow rate experiment is conducted. The experimental results show that the flow rate of the pump increases with the rise of fractal dimension of the tube diameter. When fractal dimension is 3, the maximum flow rate of the valveless pump is 29.16 mL/min under 100 V peak to peak (13 Hz) power supply, which reveals the relationship between flow rate and fractal dimensions of tube diameter distribution. This paper investigates the flow characteristics of valveless piezoelectric pump with fractal-like Y-shape branching tubes, which provides certain references for valveless piezoelectric pump with fractal-like Y-shape branching tubes in application on electronic chip cooling. 相似文献
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PZT压电薄膜无阀微泵的制备工艺及实验研究 总被引:4,自引:2,他引:2
介绍了一种基于PZT薄膜的无阀压电微泵。该微泵利用聚二甲基硅氧烷(PDMS)作为泵膜,自制的压电圆型薄膜片作为驱动部件,采用收缩管/扩张管结构,压电圆型致动片和PDMS泵膜的组合可产生较大的泵腔体积改变。在对微泵制备工艺研究的基础上,对其性能进行了实验研究,结果表明:电压和频率对流速均有显著影响。在7.5 V1、80 Hz的正弦电压驱动下,该压电微泵的最大输出流速为2.05μL/min。该文制作的微泵具有流量稳定,驱动电压较低,性能稳定可靠和易控制等优点,可满足微流体系统的使用要求。 相似文献
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提出三肋式微型气动阀这一可用于流场主动控制领域的新型微阀,通过增大逆/正向气流的损失系数比来大幅提高效率。阐述了气动阀的设计原理,对其效率高的原因进行了解释;对三肋式气动阀的流场进行数值模拟以验证设计原理,并对三角阀、气动阀的流量与效率进行计算与分析。结果表明:三肋式气动阀的效率提高到三角阀的4倍。加工了3种微阀实验件,在不可压与可压两种状态下分别进行对比实验。结果表明:在不可压状态下,三角阀的效率为3%~4%,三肋式气动阀为17%~18%;在可压状态下,三角阀的效率接近2%,三肋式气动阀约为16%。 相似文献