2002 Annual Report of the American Psychological Association.

Presents the 2002 Annual Report of the American Psychological Association. Directorate Reports, the President's Address, and Treasurer's Report are included. (PsycINFO Database Record (c) 2010 APA, all rights reserved)     

离子膜车间杜邦膜监测工作总结

通过对杜邦膜NX2002TX和旭硝子公司的F-893膜在第1年应用中运行数据的比较。证明在使用第1年内，NX2002TX膜的性能高于F-893膜。     

城市轨道交通EP2002制动系统应用研究

介绍EP2002制动系统构成和EP2002阀的种类及作用,分析EP2002制动控制逻辑及其气动原理,说明EP2002制动控制系统在城轨车辆中应用的优势。     

基于IMPACT的嵌入式汇编设计与实现

DSP的底层特性与传统的C语言特性差别很大,有DSP领域的特殊指令集,这些指令很难被编译器生成,或者根本不能被编译器生成.程序员也有需求直接访问底层特性.为了解决这个问题,通过对IMPACT的基础编译器框架进行拓展实现嵌入式汇编功能模块.     

A way to reduce environmental impact of ladle furnace slag

Abstract

In the last decades the European steel industry has made continuous efforts to reduce residues and byproducts and to increase recycling in order to reduce its environmental impact. While some steelmaking slags have been widely characterised and, to a certain extent reused, ladle furnace (LF) slag is used in different applications because of its specific properties. The main purpose of the case study presented in this paper concerns the reduction of potential LF slag environmental impacts, because of its intrinsic physicochemical properties. During the handling and cooling of LF slag, it disintegrates into a powder due to instability of the dicalcium silicate, causing an increase in dust emissions to the environment. The approach presented in this paper aims to reduce this phenomenon in order to achieve a more sustainable solution in term of reduction of powder dispersion in the environment, of costs saving and of nuisance reduction in the surroundings areas.     

Monitoring the presence of residues of tetracyclines in baby food samples by HPLC-MS/MS

Tetracyclin is a group of antimicrobial permitted in animal food production, but their concentrations in food of animal origin should not exceed 100 μg kg⁻¹ (in meat and milk). Although the detection of these substances above these limits involves fines and jail for the producer, residues of tetracyclines are still being detected in food a potential risk to consumer health, especially babies.In the past, baby foods were carefully prepared at homes. However, modern lifestyles have led to the commercialization of ready-made baby food. Generally, these products are made with vegetable and meat from different animals, such as pork, chicken or beef. The presence of tetracyclines in meat at concentrations above 100 μg kg⁻¹ is forbidden in Europe by the Regulation 37/2010. Consequently this concentration is also applicable to the portion of meat present in baby food. Even if the presence of tetracyclines is controlled regularly in meat, they should also be monitored in baby food as babies are vulnerable to such as drugs.A rapid analytical method based on high-performance liquid chromatography coupled to a tandem mass spectrometer (HPLC-MS/MS) for quantification of four tetracyclines (tetracycline, chlortetracycline, doxycycline and oxytetracycline) in baby food is presented. The tetracyclines are extracted with EDTA-McIlvaine buffer, acidified at pH 4.0, followed by liquid–liquid extraction with ethyl acetate. The final extract is analysed within 19 min on a Sunfire HPLC column from Waters. Validation was performed according to the Commission Decision 2002/657/EC. The mean accuracy was 103 μg kg⁻¹, and the mean precision, was less than 23% for all the tetracyclines. The method was tested on 31 prepared baby food samples containing vegetable and beef. The presence of oxytetracycline was detected in one of the samples at a concentration of 5 μg kg⁻¹.     

HPLC confirmatory method development for the determination of seven quinolones in salmon tissue (Salmo salar L.) validated according to the European Union Decision 2002/657/EC

A confirmatory high pressure liquid chromatographic method for the determination of seven quinolone antibiotics in tissue of Atlantic salmon (Salmo salar L.) was developed. Ciprofloxacin (CIP), danofloxacin (DAN), enrofloxacin (ENR), sarafloxacin (SAR), oxolinic acid (OXO), nalidixic acid (NAL) and flumequine (FLU) were separated on a Perfectsil ODS-2 120 (250 mm × 4 mm, 5 μm) column by gradient elution with a mobile phase consisting of 0.1% trifluoroacetic acid (pH = 1), acetonitrile and methanol at 25 °C within 22 min. Analytes were monitored at 255 nm (for the determination of OXO, NAL and FLU) and 275 nm (for CIP, DAN, ENR and SAR) by means of photodiode array detector. Examined quinolones were isolated from salmon tissue by extraction with citrate buffer solution (pH = 4.7) and purified by solid phase extraction using Oasis HLB (200 mg/6 mL) cartridges. The developed method was fully validated in terms of selectivity, linearity, accuracy, precision, stability and sensitivity according to the European Union Decision 2002/657/EC. The accuracy of the method was additionally proved by its application to certified reference material of salmon tissue (BCR® 725).     

化学反应器的定态及其稳定性分析

针对教材和专业文献中化学反应器稳定性分析方法的局限性，提出了计算机作图求解定态点的新方法，并给出全面有效的稳定性判据和分析方法，方便教学和工程应用。     

Modelling of Charpy V test rejection probability

Abstract

The purpose of this study was to develop a product design model for estimating the impact toughness of low alloy steel plates. The rejection probability in a Charpy V test is predicted with process variables and chemical composition. Joint modelling of the mean and deviation was used in order to improve the results. The proposed method is suitable for the whole production line, including all grades of steel in production and it is not restricted to a few test temperatures. Using the proposed model the product design group could have recognised most of the rejections before production. Next, the developed model will be implemented into a graphical simulation tool that is in daily use in the product planning department and already contains some other mechanical property models. The model will guide designers in predicting the related risk of rejection and in producing desired properties in the product at lower cost.     

Early accident simulating testing of radioactive material packages in road vehicles

Abstract

Beginning as early as the 1960s, concerns were voiced as to the adequacy of the package test standards imposed by the transport regulations promulgated by the International Atomic Energy Agency. One concern that was frequently raised and has continued to the present time is that the test standards do not necessarily simulate real accidents. The purpose of the crash tests described here that were done with typical packages carried in full scale vehicles was to assess the IAEA standards, their adequacy and to suggest changes to them that might be needed. It was also hoped that the tests, which were performed in the USA and in the UK, would show to regulators, to users of the regulations and to the public that current regulations already provide a very high level of safety for real world accidents. With time, much of the original information regarding these tests and their results has been lost. The few documents that remain have been surveyed and this paper presents summaries from this survey of the tests and their results.