磨料有序排布电镀砂轮的制备及其把持力研究

为解决电镀砂轮磨削加工中容屑空间不足的问题，采用点胶微粘接的方法制备了磨料有序排布的电镀砂轮，分析了磨料粘接效果和镀层力学性能。通过SEM分析了磨料/镀层/导电胶的结合界面，并进行了干磨削试验。研究结果表明，直径约为磨料粒径40%的胶点可粘接住磨料，单个胶点上粘接多颗磨料的占比小于6%；双脉冲电镀工艺制备的镀层显微硬度大于500HV，表层残余应力小于100MPa，磨料/镀层/导电胶之间的界面贴合紧密，无明显缺陷；砂轮在磨削时没有出现磨料脱落现象。     

Study on the non-uniform contact during ELID groove grinding

This paper introduces the potential feasibility that ELID (electrolytic in-process dressing) grinding replaces superfinishing in bearing manufacturing, but ELID grinding will bring new challenges. Different regions present distinguish surface profile due to the non-uniform contact in ELID groove grinding. However, few reports explaining the non-uniform contact are available. This article explores the mechanisms of the non-uniform contact during ELID groove grinding. Experiments on the non-uniform contact between bearing raceway and grinding wheel have been carried out under different conditions. The results show that non-uniform contact exists in ELID groove grinding process and it exerts influence on the profile of the raceway surface. Non-uniform contact influences the Rsk and Rku value all the time, but it influences the Ra value occasionally. Improvement strategies of eliminating the non-uniform contact are also discussed based on the experimental study.     

Effect of sintering conditions on structural and morphological properties of Y- and Co-doped BaZrO3 proton conductors

BaZrO₃-based materials doped with a trivalent cation have excellent chemical stability and relatively high proton conductivity which makes them potential proton conducting oxide materials for various electrochemical device applications such as hydrogen processing, high-temperature electrolysis, and solid electrolyte in fuel cells. However, BaZrO₃ showed poor sinterability, requiring high sintering temperatures (1700–2100 °C) with longtime sintering (20–100 h) to achieve the desired microstructure and grain growth. This sintering problem can be solved by slightly doping BaZrO₃ with a sintering aid element. Therefore, in this study, two different zirconate proton conductors: BaZr_0·9Y_0·1O_3-α (BZY) and BaZr_0·955Y_0·03Co_0·015O_3-α (BZYC) were sintered in an air atmosphere and an oxygen atmosphere for 20 h in the temperature range of 1500–1640 °C. The sinterability was evaluated by analyzing the XRD diffraction patterns, lattice constant, lattice strain, crystallite size, relative density, open porosity, closed porosity, surface morphology, grain size, and grain boundary distribution, using the XRD, SEM, EDX, and Archimedes density measurement methods. It is concluded that in an oxygen atmosphere, sintering aid Co not only improves the relative density but also produces highly dense fine particles with clear grain boundaries which are promising for electrochemical hydrogen device applications.     

Role of MgO on densification and mechanical properties in spark plasma sintered Os0.9Re0.1B2 ceramic

To promote the densification and therefore the mechanical properties of boride-based ceramics, MgO was added as sintering aid into Os_0.9Re_0.1B₂ powders for densification by using spark plasma sintering (SPS). The Os_0.9Re_0.1B₂ powders were synthesized by mechanochemical method from powder mixture of Os, Re and amorphous B. The role of MgO on densification, phase composition, microstructure and mechanical properties (hardness, fracture toughness and wear behavior) were studied by using X-ray diffraction (XRD), scanning electron microscope (SEM) with energy-dispersive spectroscopy (EDS), micro indentation and ball-on-disk tribometer. The results show that, with the introduction of MgO as sintering aid, the relative density of the Os_0.9Re_0.1B₂ ceramic samples increased. When the MgO content reached 9 wt%, the as-sintered sample is almost fully dense. No obvious regularity was found from the samples with the addition of different content of MgO. Vickers hardness values of the samples with 0, 3 wt% and 9 wt% MgO are found to be very close with each other within the experimental error (~30 GPa), while the sample with the addition of 6 wt% MgO exhibits the highest hardness of ~35 GPa. The fracture toughness of the samples is decreased slightly with the addition of MgO. The friction coefficient and wear rate of the sample with the addition of 6 wt% MgO was also found to be the lowest among all samples, which indicate best wear resistance. As a whole, with the addition content of 6 wt% MgO, the Os_0.9Re_0.1B₂ ceramic sample performs relatively excellent mechanical properties among four groups of samples.     

郴州某复杂硫化铅锌矿阶段磨浮试验研究

针对郴州某复杂硫化铅锌矿资源的性质特点,采用铅快速浮选后尾矿再磨再选的阶磨阶选工艺,较好地实现了铅锌的高效浮选回收。研究了磨矿方式、捕收剂和调整剂种类及用量等因素对该矿石浮选的影响,确定了最佳浮选条件,通过小型闭路浮选试验,得到了铅品位60.05%、回收率89.63%的铅精矿和锌品位47.01%、回收率88.14%的锌精矿。     

Simulation of Strength Distribution in Ground Ceramics by Incorporating Residual Stress Effect

Strength of ground ceramics may be affected by residual stress as well as surface flaws induced by grinding. Strength prediction for ground ceramics is convenient for mechanical design of ceramic components. In this article, a numerical procedure based on fracture mechanics was proposed to estimate strength distribution of ground ceramics by considering grinding-induced residual stress. Bending strength and residual stress of ground ceramics were measured for three grinding-conditions. By comparison of simulated results with experimental ones, it was revealed that strength characteristics in experiments were well simulated by using the proposed procedure.     

陶瓷减水剂、助磨剂、增强剂的发展现状、趋势及展望

阐述了陶瓷行业所用添加剂的分类，以及目前国际上主要生产陶瓷添加剂的厂家及主要产品，详细介绍了陶瓷坯体减水剂、助磨剂、增强剂的种类、应用、性能特点和它们与陶瓷材料的作用机理，并对陶瓷添加剂的发展前景进行了展望。     

成形磨削中砂轮修整精度的研究

成形磨削一般采用金刚石笔来修整所需要的砂轮形状，金刚石笔在安装中的位置误差将影响被加工工件的精度，本文对此误差的大小进行了分析。     

在线磨辊辊面粗糙度的实验研究

影响轧辊表面粗糙度的因素很多，为此对影响辊面粗糙度的因素进行了系统分析和实验研究，得出了轧辊和砂轮的速度、砂轮粒度、砂轮直径及磨削液等主要因素对轧辊表面粗糙度影响的一般规律。利用回归分析的方法建立了轧辊表面粗糙度的数学模型，并将计算值与实测值进行了比较，发现两者基本一致。此项研究为适时控制冷轧带钢在线磨辊辊面粗糙度提供了计算模型。     

1 000 t/d湿磨干烧生产线工艺特点和调试

湿法生产线的技术更新改造有异地新建新型干法生产线和原地改成湿磨干法生产线二种。浙江虎山集团(?)3.0 m×88.68 m湿法线的改造,经方案比较和生产原料的状况,采用了湿磨干烧方案。其中,料浆脱水采用了真空吸滤法,浇成系统采用了南京院专有技术。改造投产后,获得了优质、高产、低耗和安全生产的技改效果。