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1.
Analog Integrated Circuits and Signal Processing - We propose a power divider comprising of two parallel λ/4 coupled lines with a shared input signal line. An isolation resistor R is included...  相似文献   
2.
This is the first investigation to report the processing and properties of ultrahigh molecular weight polyethylene (UHMWPE)/functionalized activated nanocarbon (FANC) gel solutions with the aid of supercritical carbon dioxide (scCO2). The ultradrawing and ultimate tensile properties of scCO2UHMWPE and scCO2UHMWPE/FANC fibers were found to improve considerably compared to those of UHMWPE and UHMWPE/FANC fibers prepared in the conventional way. The maximum achievable draw ratio obtained for the optimal scCO2UHMWPE/FANC fibers drawn at 95°C reached 445. The highest tensile tenacity (σf) of the fully drawn scCO2UHMWPE/FANC fiber reached an extraordinary high value of 104 g/d, which is about 3.2 and 1.1 times of that of the optimal UHMWPE and UHMWPE/FANC fully drawn fibers, respectively. The σf obtained for the optimally fully drawn scCO2UHMWPE/FANC fiber is about 25 times of those of steel fibers and is the highest tensile tenacity ever reported for single‐stage drawn polymeric fibers. Considerably lower dynamic transition temperatures and evaluated thinner crystal lamellae nucleated off of extended chains or FANC nucleants were found for as‐prepared scCO2UHMWPE and scCO2UHMWPE/FANC fibers compared with UHMWPE and UHMWPE/FANC fibers, respectively. Specific surface area, morphological, and Fourier transform infrared analyses of the activated nanocarbon (ANC), acid‐treated activated nanocarbon (ATANC) and FANC nanofillers and investigation of thermal, morphological, and orientation factor properties of the as‐prepared and drawn UHMWPE, UHMWPE/FANC, scCO2UHMWPE, and scCO2UHMWPE/FANC fibers were performed to understand the remarkable ultradrawing, dynamic transition, and ultimate tensile properties obtained for scCO2UHMWPE and scCO2UHMWPE/FANC fibers. POLYM. ENG. SCI., 59:1462–1471 2019. © 2019 Society of Plastics Engineers  相似文献   
3.
Resveratrol can affect the physiology or biochemistry of offspring in the maternal–fetal animal model. However, it exhibits low bioavailability in humans and animals. Fifteen-week SD pregnant female rats were orally administered bisphenol A (BPA) and/or resveratrol butyrate ester (RBE), and the male offspring rats (n = 4–8 per group) were evaluated. The results show that RBE treatment (BPA + R30) compared with the BPA group can reduce the damage caused by BPA (p < 0.05). RBE enhanced the expression of selected genes and induced extramedullary hematopoiesis and mononuclear cell infiltration. RBE increased the abundance of S24-7 and Adlercreutzia in the intestines of the male offspring rats, as well as the concentrations of short-chain fatty acids (SCFAs) in the feces. RBE also increased the antioxidant capacity of the liver by inducing Nrf2, promoting the expression of HO-1, SOD, and CAT. It also increased the concentration of intestinal SCFAs, enhancing the barrier formed by intestinal cells, thereby preventing BPA-induced metabolic disruption in the male offspring rats, and reduced liver inflammation. This study identified a potential mechanism underlying the protective effects of RBE against the liver damage caused by BPA exposure during the peri-pregnancy period, and the influence of the gut microbiota on the gut–liver axis in the offspring.  相似文献   
4.
Many circulating cancer-related proteins, such as fibroblast growth factors (FGFs), associate with glycosaminoglycans—particularly heparan sulfate—at the cell surface. Disaccharide analogues of heparan sulfate had previously been identified as the shortest components out of the sugars that bind to FGF-1 and FGF-2. Taking note of the typical pose of l -iduronic acid, we conceived of per-O-sulfonated analogues of such disaccharides, and devised a single-step procedure for per-O-sulfonation of unprotected sugars with concomitant 1,6-anhydro bridge formation to achieve such compounds through direct use of SO3 ⋅ Et3N as sulfonation reagent and dimethylformamide as solvent. The synthesized sugars based on the oligomaltose backbone bound FGF-1 and FGF-2 mostly at the sub-micromolar level, although the tetrasaccharide analogue achieved low-nanomolar binding with FGF-2.  相似文献   
5.
There is a growing concern over the food safety issue related to increased incidence of cooking oil adulteration with recycled cooking oil (RCO). The objective of this study was to detect fresh palm olein (FPO) adulteration with RCO using fatty acid composition (FAC) and Fourier-transform infrared spectroscopy (FTIR) spectral analyses combined with chemometrics. RCO prepared in the laboratory was mixed with FPO in the proportion ranged from 1% to 50% (v/v) to obtain the adulterated oil samples (AO). FACs for FPO, RCO, and AO were determined using gas chromatography equipped with a flame ionization detector (GC-FID). The compositions of most fatty acids in RCO lied within the normal ranges of Codex standard, except for C8:0, C10:0, C11:0, C15:0, trans C18:1, and polyunsaturated fatty acids (PUFAs), C20:5. PUFAs showed a consistent decreasing trend with increasing magnitude of change with respect to increasing adulteration level and thus might be a good indicator for detecting FPO adulteration with RCO. The evaluation parameters (coefficient of determination, root mean standard error) of the FTIR-partial least square (PLS) model of palm oil adulteration with recycled oil are R2 = 0.995 and 3.25, respectively. For FTIR spectral analysis, the distinct variations in spectral regions and aberrations in characteristic bands between FPO and RCO were observed. The optimized PLS calibration model developed from normal spectral of the combined region at 3602–3398, 3016–2642, and 1845–650 cm?1 overpredict the adulteration level. On the other hand, the discriminant analysis classification model was able to classify the FPO and AO into two distinct groups. Improvement of the principles of combined techniques in authenticating AO from fresh oil is beneficial as a guideline to detect adulteration in cooking oil.  相似文献   
6.
Multimedia Tools and Applications - With the development of technology, the importance of the research on speech emotion recognition and semantic analysis has increased. The research is primarily...  相似文献   
7.
C.L. Yeh  G.T. Liou 《Ceramics International》2018,44(16):19486-19491
Fabrication of alumina-chromium carbide composites was investigated by PTFE-activated Cr2O3/Al/C combustion synthesis. PTFE was employed as not only a reaction promoter, but a carburizing agent. Three reaction systems were prepared with different contents of carbon for the synthesis of Cr23C6, Cr7C3, and Cr3C2. The amounts of PTFE were selected to ensure combustion synthesis in the SHS (self-propagating high-temperature synthesis) mode and to provide carbon in quantities of 15 and 25?mol% of the total carbon. Experimental results showed that the combustion wave velocity and temperature decreased with increasing carbon, but increased with PTFE. A correlation between combustion wave velocity and temperature contributed to determination of the activation energy Ea =?89.15?kJ/mol for the combustion reaction. The increase of PTFE also improved formation of chromium carbides. As a result, the Cr23C6– and Cr7C3–Al2O3 composites were produced with almost no impurities. Due to a loss of carbon in carbothermic reduction, the Cr3C2–Al2O3 composite was obtained with Cr7C3 as the secondary carbide. SEM micrographs and DES analyses indicated that spherical carbide grains with a size of 0.5–3.0 μm were synthesized.  相似文献   
8.
The oxygen transmission rate, average volume of free‐volume cavities (Vf) and fractional free volume (Fv) of polyamide 6,10 (PA610)/poly(vinyl alcohol) (PVA) (i.e. PA610xPVA05y, PA610xPVA08y and PA610xPVA14y) blend films reduced to minimum values when their PVA contents reached corresponding optimal values. Oxygen transmission rate, Vf and Fv values obtained for optimal PA610xPVAzy blown films were reduced considerably with decreasing PVA degrees of polymerization. The oxygen transmission rate of the optimal bio‐based PA61080PVA0520 blown film was only 2.4 cm3 (m2·day·atm)?1, which is about the same as that of the most often used high‐barrier polymer, ethylene–vinyl alcohol copolymer. Experimental findings from dynamic mechanical analysis, differential scanning calorimetry, wide‐angle X‐ray diffraction and Fourier transform infrared spectroscopy of the PA610xPVAzy blends indicate that PA610 and PVA in the blends are miscible to some extent at the molecular level when the PVA contents are less than or equal to the corresponding optimal values. The considerably enhanced oxygen barrier properties of the PA610xPVAzy blend films with optimized compositions are attributed to the significantly reduced local free‐volume characteristics. © 2017 Society of Chemical Industry  相似文献   
9.
(Ti,V)2AlC/Al2O3 solid solution composites were prepared by solid state combustion simultaneously incorporating reduction reactions of V2O5 and TiO2/V2O5 with aluminum. Two reaction systems composed of Ti–V2O5–Al–Al4C3 and TiO2–V2O5–Al–Al4C3 powder mixtures were studied. Combustion exothermicity was enhanced by increasing V2O5 and Al, which not only caused an increase in the combustion temperature and reaction front velocity, but also facilitated evolution of the (Ti,V)2AlC phase. Between two reaction systems, the Ti-containing samples were more energetic and produced (Ti1–xVx)2AlC/Al2O3 composites with x = 0.2–0.8. The degree of element substitution was reduced for the samples adopting TiO2, which yielded Al2O3-added (Ti1–yVy)2AlC with y = 0.4–0.8.  相似文献   
10.
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