行波管质量与可靠性信息管理系统的设计

本文从应用角度简要介绍了《行波管质量与可靠性信息管理系统》的研制背景，数据库的数据来源，数据结构，系统构成及功能特点。     

基于IPAT模型的河北省灰水足迹分析及预测

河北作为京津冀发展圈的重要组成部分,水质水量问题突出,因此迫切需要对其水量和水质进行研究。基于农业和工业生活两部分,选取N肥、P肥、COD为关键污染物,以水环境最大允许容量为依据,计算了河北省2004—2015年的灰水足迹,并以此为基础,对2030年单位产值造成的灰水足迹进行了预测。结果表明:(1)12年间河北省灰水足迹呈现先上升再下降的趋势,农业灰水足迹以N肥为最关键污染物,随着化肥总量和平均施肥水平的增加不断增长,年均增长率0.87%;(2)工业生活灰水足迹总体呈现增长趋势,阶段内呈现下降趋势。以2011年为界,河北省灰水足迹从由农业灰水足迹决定转变为由工业生活灰水足迹决定,且工业生活灰水足迹和第三产业产值的相关性较强;(3)通过IPAT模型分析发现,农业灰水足迹除2004,2013,2015年外,其他各年份可持续性均较差,2004—2010年工业生活灰水足迹的可持续性好于2011—2015年。未来若按照现有水平继续发展,到2030年河北省单位农业产值造成的灰水足迹将下降为0.05 m~3/元,单位工业生活产值造成的灰水足迹将下降为0.006 m~3/元。     

TiNb（Y_2O_3）长纤维增强Ti－48Al－2Cr－2Nb合金复合材料的弯曲变形与界面

研究了ＴｉＮｂ（Ｙ２Ｏ３）连续纤维增强Ｔｉ－４８Ａｌ－２Ｇｒ－２Ｎｂ合金复合材料的界面及显微组织。研究发现：复合材料的弯曲强度比基体略有提高，弹性模量和挠度有所下降。在纤维和基体之间形成一层约１０～２０μｍ厚的α２－Ｔｉ３Ａｌ性层，近界面基体组织有片层化倾向。大量变形层错带和孪晶出现及界面位错墙的形成成为塑变及强化的主要机制。     

无动力污水处理技术及其研究与应用进展

无动力水处理技术自从二十世纪九十年代才开始在我国逐步得以应用和发展。文章介绍了该技术的发展历程、基本原理和工艺特点，结合各地实践总结评价了其应用效果，并对该技术在水处理领域的应用改进提出建议和方法。     

新型实验室XFD-63单槽浮选机的研制

实验室XFD-63单槽浮选机更新换代、技术创新对实验室选矿试验工作发挥着重要作用。通过叶轮无级调速、自动曲柄摆杆刮泡机构的改进，使浮选机结构更加简化，刮泡结构新颖，选别性能优良。     

相角测量装置的同步测量精度问题

对基于全球定位系统 (GPS)、锁相环 (PLL)的相角测量装置 (PMU )主要误差因素进行了分析与仿真研究 ,结果表明 :幅值误差远小于角度误差 ;异地同步方法误差远小于同步测量环节本身的误差 ,后者主要由PMU的频率跟踪与测量、信号滤波延迟以及数值算法等环节引起 ;指出以PLL器件锁相跟踪被测信号基频时 ,在频率快速变化的情况下可能隐含的问题。最后得出 :在保证频率跟踪测量精度的前提下 ,PMU的相角测量精度可以达到 1°。     

集输管道绝缘接头强度评价方法研究

绝缘接头作为阴极保护系统的关键组件,其安全性与可靠性的研究在不断深入。由于集输系统高温、高压的特点,绝缘接头必然承受由于内压和热胀等导致的弯矩,加之其结构特点,可能会引起泄漏。为此,有必要综合考虑工况条件,研究绝缘接头可承受的安全弯矩值,并形成基于强度的评价方法。根据规范要求,结合管道强度理论,推导了绝缘接头承受弯矩范围的计算公式,提出了对应的绝缘接头强度校核与设计弯矩值选取方法;研究成果为绝缘接头安全设计与强度校核提供了参考与借鉴。     

Ketjen black carbon supported CoO@Co−N−C nanochains as an efficient electrocatalyst for oxygen evolution

We demonstrate an extremely facile in-situ pyrolysis followed by the reduction of partial Co²⁺ route to synthesize novel Ketjen black carbon (KB) supported CoO@Co?N?C (denoted as CoO@Co?NC/KB) nanochains using KB, urea and cobalt (Ⅱ) acetate as co-precursors. The as-prepared CoO@Co-NC/KB displays higher electrocatalytic activity, smaller Tafel slope and better durability for the oxygen evolution reaction than those of the benchmark commercial RuO₂ catalyst in 1.0 M KOH solution, far outperforming the control groups (i.e. CoO@Co?g-C₃N₄/KB, Co?NC/KB, CoO?NC/KB, CoO@Co/KB, CoO@Co?NC and Co₃O₄?NC/KB). The remarkable electrocatalytic performance of CoO@Co?NC/KB is primarily credited to the synergistic effect between Co and CoO species with a core-shell structure, increased active sites and considerably enhanced electronic conductivity.     

Identification of phosphoserine and phosphothreonine as cysteic acid and beta-methylcysteic acid residues in peptides by tandem mass spectrometric sequencing

Tandem mass spectrometry has long been an intrinsic tool to determine phosphorylation sites in proteins. However, loss of the phosphate moiety from both phosphoserine and phosphothreonine residues in low-energy collision-induced dissociation is a common phenomenon, which makes identification of P-Ser and P-Thr residues complicated. A method for direct sequencing of the Ser and Thr phosphorylation sites by ESI tandem mass spectrometry following beta-elimination/sulfite addition to convert -HPO4 to -SO3 has been studied. Five model phosphopeptides, including three synthetic P-Ser-, P-Thr-, or P-Ser- and P-Thr-containing peptides; a protein kinases C-phosphorylated peptide; and a phosphopeptide derived from beta-casein trypsin digests were modified and then sequenced using an ESI-quadrupole ion trap mass spectrometer. Following incubation of P-Ser- or P-Thr-containing peptides with Na2SO3/NaOH, 90% P-Ser and 80% P-Thr was converted to cysteic acid and beta-methylcysteic acid, respectively, as revealed by amino acid analysis. The conversion can be carried out at 1 microM concentration of the peptide. Both cysteic acid and beta-methylcysteic acid residues in the sequence were shown to be stable and easily identifiable under general conditions for tandem mass spectrometric sequencing applicable to common peptides.