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1.
Avneet Kaur Neha Bhardwaj Amanpreet Kaur Km Abida Tejo Prakash Nagaraja Amjad Ali Ranjana Prakash 《Journal of the American Oil Chemists' Society》2021,98(2):139-147
Epoxidized methyl esters (EMO) with their high oxirane ring reactivity, acts as a raw material in the synthesis of various industrial chemicals including polymers, stabilizers, plasticizers, glycols, polyols, carbonyl compounds, biolubricants etc. EMO has been generally quantified by the gas chromatography (GC) and high-performance liquid chromatography (HPLC) techniques. Taking into the account of the limitations of these techniques, two qHNMR-based equations have been proposed for the quantification of EMO in the mixture of EMO and methylesters (MO). The validity of the proposed method was determined using standard mixtures of MO and EMO having different molar concentrations. The developed equations have been applied on the samples of EMO prepared from oleic acid in two-step process viz., esterification followed by epoxidation. The qHNMR-based EMO quantification showed acceptable agreement with the results obtained from HPLC analysis. 相似文献
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Muhammad Ovais Sudip Mukherjee Arindam Pramanik Devlina Das Anubhab Mukherjee Abida Raza Chunying Chen 《Advanced materials (Deerfield Beach, Fla.)》2020,32(22):2000055
Tailoring personalized cancer nanomedicines demands detailed understanding of the tumor microenvironment. In recent years, smart upconversion nanoparticles with the ability to exploit the unique characteristics of the tumor microenvironment for precise targeting have been designed. To activate upconversion nanoparticles, various bio-physicochemical characteristics of the tumor microenvironment, namely, acidic pH, redox reactants, and hypoxia, are exploited. Stimuli-responsive upconversion nanoparticles also utilize the excessive presence of adenosine triphosphate (ATP), riboflavin, and Zn2+ in tumors. An overview of the design of stimulus-responsive upconversion nanoparticles that precisely target and respond to tumors via targeting the tumor microenvironment and intracellular signals is provided. Detailed understanding of the tumor microenvironment and the personalized design of upconversion nanoparticles will result in more effective clinical translation. 相似文献
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Rezvan Tavakoli Saeid Vakilian Fatemeh Jamshidi-Adegani Samaneh Sharif Abdolreza Ardeshirylajimi 《国际聚合物材料杂志》2018,67(15):873-878
In situ prolonged delivery of drugs at the site of tumor can be satisfactorily accelerated patient recovery. We compared the effect of temozolomide while incorporated by polycaprolactone nanofibers on the apoptotic behavior of U87 glioma cells. After biocompatibility evaluation of nanofibers by scanning electron microscope and 3-(4,5-dimethylthiazolyl-2)-2,5-diphenyltetrazolium bromide analysis, the apoptosis of U87 cells was evaluated using p53, Bcl2 and Bax genes expression. It was found that nanofiber-temozolomide group showed a greater ability to induce apoptosis as well as have a significantly diminished initial burst release of drug compared with other groups and have promising potential in treating cancer. 相似文献
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Ahlam Ammar Sharif 《建筑学研究前沿(英文版)》2020,9(4):837-857
Urban researchers have maintained a constant interest in the complexity and continuity of urban space usage. Some have applied actor–network theory (ANT) to investigate the heterogeneity of spaces and present them through the networks of their users’ activities. However, these accounts are predominantly limited in examining the extent to which these spaces may be heterogeneous when exploring such networks. This paper draws on recent ANT scholarship, which employs an ethnographic research conducted in a main park in a housing project at Dahiyat Al Hussein in Amman, Jordan. The findings describe the complex and unpredictable negotiations that occur within spaces by documenting the varieties and interrelations among user activity networks within this common and shared urban space. This research reveals the extent to which spaces, parks in this case, may be heterogeneous by unpacking their usage. The conclusions and insights assert the necessity of paying attention to design detail and creating designs that are responsive to evolving user activities. 相似文献
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Different top layer fabrication methods (amine-first, acid-first, spin coating), organic phase solvents (hexane, heptane, mixed hexane/heptane), acid acceptors (triethylamine, sodium carbonate, sodium hydroxide), and surfactant sodium dodecyl sulfate concentrations (0, 0.05, and 0.1 wt%) were utilized to fabricate thin film composite polyamide membranes for CO2/N2 separation. The results, according to an L9 orthogonal array of Taguchi approach, showed that employing acid-first method increases both CO2 permeance and CO2/N2 selectivity of the membranes at a feed gas pressure of 3 bars. On the other hand, sodium hydroxide, and triethylamine should be used, as acid acceptors, to maximize CO2 permeance and CO2/N2 selectivity, respectively. Moreover, the use of hexane solvent and 0 wt% surfactant led to maximum permeance, while, hexane solvent and 0.1 wt% surfactant were needed to reach the highest selectivity. The above level setting of synthesis parameters also resulted in the minimum sensitivity of the fabrication process to the noise factors effects. As shown by the analysis of variance, acid acceptor, and organic solvent types were the most influential parameters on CO2 permeance and CO2/N2 selectivity, respectively. The effects of fabrication method and surfactant concentration, as single factors, on permeation/selectivity responses were also investigated. 相似文献
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Yara Sharif 《Landscape Research》2019,44(7):872-891
ABSTRACTThis paper sheds a light on the ephemeral landscape of Palestine. Under a deliberate process of ‘erasing, peeling, cutting and pasting’, the physical and mental maps of Palestine today are rapidly changing with the Palestinians being pushed out of the scene. This colonial project has been best represented by Sari Hanafi as ‘spacio-cidal’ as it targets the landscape and consequently the narrative of those who shape it.Stemming from the need for an alternative discourse to narrate and redraw the map from a local lens, I use the village of Beit Iksa as an example to portray the spatial restructuring of the landscape. I show how ‘greening’ casts a shadow on the Israeli colonial strategies that lie beneath to alienate and ‘reinvent’ the rural scene. And yet, because for every strategy of control there is a tactic to resist, I show how through spatial interventions, I tried to rethink the rural and challenge its ideological transformation into a void; a leftover landscape shaped by time and immobility and yet is loaded with spatial potentials and open to change. 相似文献
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AbstractThis paper proposes an on-line maximum torque per ampere (MTPA)/maximum torque per voltage (MTPV) trajectory tracking method in permanent magnet synchronous machines (PMSMs) with power management. The on-line MTPA/MTPV machine current trajectory tracking algorithm is developed from PMSM model. Maximum source current and machine current are regulated to enhance hardware protection during machine current trajectory tracking. The maximum source current management is achieved by iterating within the current trajectory tracking algorithm over continuous torque command modifications based on power flow analysis, and the maximum machine current management is achieved by torque command limiting based on current angle modulation. Different from the existing techniques in literature, the proposed method has an unique feature of providing on-line regulation of source current, while maintaining on-line MTPA/MTPV trajectory tracking in PMSMs. It also provides machine and inverter overcurrent regulation to enhance their protection. In addition, the proposed method is flexible to tune and does not require off-line calibration. The effectiveness of the proposed method is confirmed by simulation results in MATLAB. 相似文献