电流密度对Ni-Fe纳米合金微观结构及性能的影响

通过电沉积制取大块Ni-Fe纳米合金,利用XRD、TEM、SEM等研究了Ni-Fe纳米合金(平均晶粒尺寸约20 nm)的微观结构和变形机制,用单向拉伸试验机(MTS810)测试单向拉伸性能,表明这种合金的抗拉强度近2 GPa,伸长率可达10.9%.Ni-Fe纳米合金对应变速率敏感较小,塑性变形导致了合金的晶粒长大,同时变形孪生和位错运动也起到一定作用.试验结果表明,纳米合金的塑性变形受晶界活动的影响.     

孔洞敏感超塑性材料变形的数值分析

本文用两种数值方法,非线性长波分析和刚粘塑性有限元方法研究了孔洞敏感的超塑性材料在单向拉伸和园板涨形中的不均匀变形和断裂过程。分析表明,这种过程是不均匀几何失稳与内部孔洞长大的结合与相互作用的结果。材料的应变速率敏感性指数与孔洞长大速率通过不同的变形机理图控制着这种过程。叠加的静水压力能够改变孔洞敏感材料的断裂模式,从常压下没有宏观颈缩的孔洞断裂到无内部孔洞的外部颈缩断裂。     

塑性和超塑性材料m-n-δ关系的简化表达式

以Hart的微分型本构关系为基础,本文推导出了一个既包含应变硬化效应(n)又包含应变速率敏感效应(m)的m-n-δ关系式δ=[1/(1-(1-α(0))~(1/m))]~m×e~n-1当n=0时,它吻合于Ghosh和Ayres的现代分析,当m=0时,吻合于Considère的经典分析.该公式的计算结果和实验结果一致.     

Surface morphology and photoluminescence properties of ZnO thin films obtained by PLD

ZnO thin films on Si(111) substrate were deposited by laser ablation of Zn target in oxygen reactive atmosphere, Nd-YAG laser with wavelength of 1 064 nm was used as laser source. XRD and FESEM microscopy were applied to characterize the structure and surface morphology of the deposited ZnO films. The optical properties of the ZnO thin films were characterized by photoluminescence. The UV and deep level (yellow-green) light were observed from the films. The UV light is the intrinsic property and deep level light is attributed to the existence of antisite defects (Ozn). The intensity of UV and deep level light depends strongly on the surface morphology and is explained by the surface roughness of ZnO film. A strongly UV emission can be obtained from ZnO film with surface roughness in nanometer range.     

冷变形低碳马氏体钢的回火塑性

研究回火温度对15钢冷变形低碳马氏体塑性的影响.获得板条马氏体的试样经大量冷拔变形后在200～600℃进行了回火处理并测试了抗拉强度和伸长率.结果表明,随回火温度的提高拉伸强度连续降低,且伸长率在200～500℃范围内始终保持不变,当回火温度超过500℃后伸长率才开始急剧上升.而未冷变形的低碳马氏体钢在同温度范围回火时其伸长率随回火温度的提高连续增长.透射电镜分析结果表明,这种冷变形低碳马氏体的回火特性是,由于马氏体再结晶晶界上大量析出渗碳体所致.     

A SIMPLIFIED EXPRESSION OF m-n-δ RELATIONS FOR MATERIALS WITH PLASTICITY OR SUPERPLASTICITY

以Hart的微分型本构关系为基础,本文推导出了一个既包含应变硬化效应(n)又包含应变速率敏感效应(m)的m-n-δ关系式δ=[1/(1-(1-α(0))~(1/m))]~m×e~n-1当n=0时,它吻合于Ghosh和Ayres的现代分析,当m=0时,吻合于Considère的经典分析.该公式的计算结果和实验结果一致.     

沉积温度对ZnO薄膜结构及发光性能的影响

利用Nd-YAG激光器(波长为1064nm,频率为10Hz)做光源,采用纯金属锌靶,以Si(111)为基体在有氧的气氛中通过激光烧蚀锌靶表面来制备氧化锌薄膜,研究基体温度对ZnO薄膜结构及发光性能的影响.通过XRD和AFM原子力显微镜来表征氧化锌薄膜的结构和表面形貌,其光学性质由光致发光谱来表征.结果表明:在450-550 ℃的条件下沉积的ZnO薄膜具有c-轴择优取向,500℃时c-轴取向最明显.具有c-轴取向的ZnO薄膜具有强的紫外光发射和弱的绿光发射,发光中心在518nm处的黄绿光发射主要归因于电子从导带底部到氧位错缺陷OZn能级之间的跃迁.     

Influence of Laser Coating on Microstructure and Properties of an Al-Si Alloy

The microstructure and wear resistance of acast Al-Si alloy coated with metal and rare earthelements and treated by the laser rapidmelt-solidification(LRMS)are studied in the pres-ent work.Optical and SEM micrographic analysesshowed that a superfine microstructure was ob-tained,and the hardness was remarkably enhancedby the LRMS treatment.Wear test showed that therapid melt-solidified microstructure had higherwear resistance than that treated by ordinary solidsolution treatment.     

钢铁表面黑色转化膜处理技术

黑色转化膜技术是目前较为先进的钢铁表面处理技术 ,本文试验研究了一种新工艺 ,提出了TB值的概念 ,通过控制TB值即可控制处理液的质量 ,获得性能优良的转化膜。此工艺性能可靠 ,可操作性强 ,并可应用于激光热处理前的预处理。