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Ti2AlC bulk material was synthesized by hot pressing of mixture powders of TiC, Ti, Al and active carbon. The phase compositions of resultant product at different temperature were detected by X-ray diffractometer. The microstructures of the samples were observed by SEM. Finally, the mechanical properties and thermal properties of the sample at 1 400 ℃ were measured. The results show that high purity Ti2AlC material with little Ti3AlC2 can be synthesized by hot pressing 0.5TIC/1.5Ti/1.0A1/0.5C at 1 400 ℃. Ti2AlC exhibits high mechanical properties and metallic electrical properties. Its fractm'e toughness is 7.0 MPa·m^1/2, its flexural strength is 384 MPa at room temperature, and its electrical conductivity is 2.56 × 10^6 Ω^-1·m^-1 at room temperature. 相似文献
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放电等离子烧结工艺制备Ti2AlC材料的研究 总被引:4,自引:0,他引:4
以元素粉钛、铝、碳为原料,采用放电等离子烧结工艺在1100℃的温度下成功地制备了高纯、致密Ti2AlC材料。合成材料的x-射线衍射(XRD)和扫描电镜(SEM)分析的结果表明:多晶体Ti2AlC形貌为板状结晶,晶粒大小平约为20μm,厚度在3—5μm。 相似文献
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采用热压工艺以Ti、Al、Si元素粉和活性炭为原料,分别以2.0Ti/1.1Al/1.0C(摩尔比)及以0.1和0.2mol的Si取代Al,合成了Ti2AlC/Ti3AlC2块体材料.通过建立Ti2AlC、Ti3AlC2和掺Si的计算模型,计算了平均原子净电荷和平均共价键键级.结果表明:以元素粉2.0Ti/1.1Al/1.0C为原料在1450℃热压60min合成只含有非常少量Ti3AlC2的Ti2AlC材料;当Si取代Al达到0.2mol时,作用非常明显,表现为使同一温度下Ti3AlC2含量增加而Ti2AlC含量减少.另外,应用掺Si后对原子净电荷和共价键键级的影响解释了实验结果. 相似文献
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