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1.
Simultaneous surface modification by 3‐chloropropyl and methyl groups on the same Si atoms resulted in hydrophobic and highly
ordered mesoporous silica with a very high surface area. 13C and 29Si MAS NMR spectra indicate homogeneous grafting of chloropropyl and methyl groups in the silica matrix and this organically
modified Ti‐MCM‐41 shows outstanding catalytic performance in the epoxidation of cyclododecene using tert‐butyl hydroperoxide
as oxidant.
This revised version was published online in July 2006 with corrections to the Cover Date. 相似文献
2.
Mazumdar Debasis Mitra Soma Ghosh Kuntal Bhaumik Kamales 《Pattern Analysis & Applications》2021,24(3):1403-1425
Pattern Analysis and Applications - The pattern of spatial contrast discontinuities in natural images has been analysed in the present work, and based on it, a new adaptive model of the... 相似文献
3.
Krishanu Sarkar Mahasweta Nandi Manirul Islam M. Mubarak Asim Bhaumik 《Applied Catalysis A: General》2009,352(1-2):81-86
Phenyl functionalized 2D-hexagonal mesoporous silica material has been synthesized by cationic/non-ionic mixed surfactant templating route. The phenyl group of this mesoporous material is further functionalized via nitration and then reduction of that nitro group to amino functionality, followed by Schiff base condensation and heterogenization of a palladium(II) complex, yielded an ortho-metalated palladium(II) complex anchored in a ordered mesoporous silica matrix. This supported metal complex acts as an efficient catalyst in the Suzuki cross-coupling reaction and shows high selectivity for the bi-aryl products. 相似文献
4.
Simultaneous sequestration of nitrate and phosphate from wastewater using a tailor‐made bacterial consortium in biofilm bioreactor 下载免费PDF全文
Pallavi Mukherjee Chaitali Chanda Moumita Bhaumik Madhurima Ghosh Jaweria Sharmin Poulami Datta Srimoyee Banerjee Parthasarathi Barat Ashoke Ranjan Thakur Lalit Mohan Gantayet Indranil Mukherjee Shaon Ray Chaudhuri 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》2018,93(5):1279-1289
5.
SA Lelièvre VM Weaver JA Nickerson CA Larabell A Bhaumik OW Petersen MJ Bissell 《Canadian Metallurgical Quarterly》1998,95(25):14711-14716
What determines the nuclear organization within a cell and whether this organization itself can impose cellular function within a tissue remains unknown. To explore the relationship between nuclear organization and tissue architecture and function, we used a model of human mammary epithelial cell acinar morphogenesis. When cultured within a reconstituted basement membrane (rBM), HMT-3522 cells form polarized and growth-arrested tissue-like acini with a central lumen and deposit an endogenous BM. We show that rBM-induced morphogenesis is accompanied by relocalization of the nuclear matrix proteins NuMA, splicing factor SRm160, and cell cycle regulator Rb. These proteins had distinct distribution patterns specific for proliferation, growth arrest, and acini formation, whereas the distribution of the nuclear lamina protein, lamin B, remained unchanged. NuMA relocalized to foci, which coalesced into larger assemblies as morphogenesis progressed. Perturbation of histone acetylation in the acini by trichostatin A treatment altered chromatin structure, disrupted NuMA foci, and induced cell proliferation. Moreover, treatment of transiently permeabilized acini with a NuMA antibody led to the disruption of NuMA foci, alteration of histone acetylation, activation of metalloproteases, and breakdown of the endogenous BM. These results experimentally demonstrate a dynamic interaction between the extracellular matrix, nuclear organization, and tissue phenotype. They further show that rather than passively reflecting changes in gene expression, nuclear organization itself can modulate the cellular and tissue phenotype. 相似文献
6.
S. K. Bhaumik 《Transactions of the Indian Institute of Metals》2010,63(2-3):297-299
Analysis of engineering failures is a complex process. It is a task that requires information from personnel having expertise in many areas. From the information gathered, a failure analyst needs to discover what was fundamentally responsible for the failure, termed as “root cause”, and to determine the sequence of events that led to the final failure. Root cause analysis not only helps in finding solutions to the immediate problem, but also provides valuable guidelines as to what needs to be done to prevent recurrence of similar failures in future. However, experience suggests that most failure analyses fall short of this goal. Also, it is seen that a significant number of failure analysts incorrectly use the term “root cause“ when what they really establish is the primary cause of failure or simple physical cause. Is this because the definition of “root cause“ not understood adequately? The author examines this aspect through a few service failure cases. 相似文献
7.
Siddharth Gupta Anagh Bhaumik Ritesh Sachan Jagdish Narayan 《JOM Journal of the Minerals, Metals and Materials Society》2018,70(4):450-455
This article provides insights pertaining to the first-order phase transformation involved in the growth of densely packed Q-carbon and nanodiamonds by nanosecond laser melting and quenching of diamond-like carbon (DLC) thin films. DLC films with different sp3 content were melted rapidly in a controlled way in super-undercooled state and quenched, leading to formation of distinct nanostructures, i.e., nanodiamonds, Q-carbon, and Q-carbon nanocomposites. This analysis provides direct evidence of the dependence of the super-undercooling on the structural evolution of Q-carbon. Finite element heat flow calculations showed that the super-undercooling varies monotonically with the sp3 content. The phenomenon of solid–liquid interfacial instability during directional solidification from the melt state is studied in detail. The resulting lateral segregation leads to formation of cellular filamentary Q-carbon nanostructures. The dependence of the cell size and wavelength at the onset of instability on the sp3 content of DLC thin films was modeled based on perturbation theory. 相似文献
8.
Fe(3)O(4) coated polypyrrole (PPy) magnetic nanocomposite was prepared via in situ polymerization of pyrrole monomer for the removal of highly toxic Cr(VI). Structure and morphology of the prepared nanocomposite were characterized by attenuated total reflectance Fourier transform infrared spectroscopy (ATR-FTIR), X-ray diffraction pattern, Field emission scanning electron microscopy (FE-SEM) and high resolution transmission electron microscopy (HR-TEM). Electron spin resonance (ESR) studies confirmed that the nanocomposite is magnetic in nature. Up to 100% adsorption was found with 200mg/L Cr(VI) aqueous solution at pH 2. Adsorption of Cr(VI) on the surface of the adsorbent was confirmed by the ATR-FTIR and X-ray photoelectron spectroscopy (XPS). XPS studies also suggested that ion exchange and reduction on the surface of the nanocomposite may be the possible mechanism for Cr(VI) removal by the PPy/Fe(3)O(4) nanocomposite. Adsorption results showed that Cr(VI) removal efficiency by the nanocomposite decreased with an increase in pH. Adsorption kinetics was best described by the pseudo-second-order rate model. Isotherm data fitted well to the Langmuir isotherm model. Thermodynamic study revealed that the adsorption process is endothermic and spontaneous in nature. Desorption experiment showed that in spite of the very poor recovery of the adsorbed Cr(VI); the regenerated adsorbent can be reused successfully for two successive adsorption-desorption cycles without appreciable loss of its original capacity. 相似文献
9.
Partha Bhaumik Shuqiang Zhang Pulak Chowdhury Sang-Soo Lee Jong Hyun Lee Biswanath Mukherjee 《Photonic Network Communications》2014,28(1):4-18
This paper gives an overview of software-defined optical networks (SDONs). It explains the general concepts on software-defined networks (SDNs), their relationship with network function virtualization, and also about OpenFlow, which is a pioneer protocol for SDNs. It then explains the benefits and challenges of extending SDNs to multilayer optical networks, including flexible grid and elastic optical networks, and how it compares to generalized multi-protocol label switching for implementing a unified control plane. An overview on the industry and research efforts on SDON standardization and implementation is given next, to bring the reader up to speed with the current state of the art in this field. Finally, the paper outlines the benefits achieved by SDONs for network operators, and also some of the important and relevant research problems that need to be addressed. 相似文献
10.
Swapan K. Das Mahasweta Nandi Saurav Giri Asim Bhaumik 《Microporous and mesoporous materials》2009,117(1-2):362-367
A new mesoporous iron(III) borate material has been synthesized hydrothermally by using supramolecular assembly of cationic (cetyltrimethylammonium bromide, CTAB) or anionic (sodiumdodecyl sulfate, SDS) surfactant as structure directing agent (SDA) during co-condensation of Fe(III) and H3BO3 under controlled pH condition. Powder X-ray diffraction, N2 sorption, HRTEM, FE-SEM-EDS, AAS, FT-IR and UV–Vis spectroscopic tools, Mössbauer and magnetization measurements are used to characterize the nanostructure, porosity, morphology, chemical composition and magnetic properties. Template molecules can be removed from the as-synthesized material by two consecutive HCl–EtOH extraction and the template-free sample showed good surface area with a peak pore width of ca. 2.6 nm. Spectroscopic results suggested the octahedral coordination of Fe(III) in the FeBO3 framework. Magnetic measurements suggested the coexistence of antiferromagnetic core and the glassy magnetic behavior. The glassy magnetic behavior is ascribed to the dominant surface magnetism for mesoporous FeBO3. Acid catalytic properties of this material in liquid phase benzylation of mesityline and anisole have been studied. 相似文献