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1.
Koji Morita Byung-Nam Kim Hidehiro Yoshida Keijiro Hiraga Yoshio Sakka 《Journal of the European Ceramic Society》2018,38(6):2588-2595
Carbon contamination from the carbon paper/dies during spark-plasma-sintering (SPS) processing was examined in the MgAl2O4 spinel. The carbon contamination sensitively changes with the heating rate during the SPS processing. At the high heating rate of 100 °C/min, the carbon contamination having organized structures occurred over almost the entire area from the surface to deep inside the SPSed spinel disk. In contrast, at the slow heating rate of 10 °C/min, the carbon contamination having disordered structures occurred only around the surface area. The carbon phases transform into high pressure CO/CO2 gases by post-annealing in air and lead to pore formation along the grain junctions. The pore formation significantly occurs at the high heating rate due to the large amount of the contaminant carbon phases. This suggests that if once the carbon contamination was formed in the materials, it is very difficult to remove the carbon phases from the materials. 相似文献
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M Tanaka T Hakuto M Akatsuka E Morimoto T Hama M Morimoto Y Hiraga M Hyodo 《Canadian Metallurgical Quarterly》1993,42(6):883-887
We injected botulinum toxin to treat hemifacial spasm, and investigated the effects and the patient's impression of this treatment. Average duration of improvement lasted about 3.5 months in both the initial treatment group and the recurrent group. However the patients in the recurrent group received fewer units of botulinum toxin than those in the initial treatment group. Except for local paralysis that disappeared within a month, there were very few complications. Most patient were satisfied with this treatment. We conclude that the treatment of hemifacial spasm with botulinum toxin is both simple and useful. 相似文献
4.
Effect of Ultrasonication on the Microstructure and Tensile Elongation of Zirconia-Dispersed Alumina Ceramics Prepared by Colloidal Processing 总被引:1,自引:0,他引:1
Tohru S. Suzuki Yoshio Sakka Keishi Nakano Keijiro Hiraga 《Journal of the American Ceramic Society》2001,84(9):2132-2134
To obtain dense, fine-grained ceramics, fine particles and advanced powder processing, such as colloidal processing, are needed. Al2 O3 and ZrO2 particles are dispersed in colloidal suspensions by electrosteric repulsion because of polyelectrolyte absorbed on their surfaces. However, additional redispersion treatment such as ultrasonication is required to obtain dispersed suspensions because fine particles tend to agglomerate. The results demonstrate that ultrasonication is effective in improving particle dispersion in suspensions and producing a homogeneous fine microstructure of sintered materials. Superplastic tensile ductility is improved by ultrasonication in preparing suspensions because of the dense and homogeneous fine microstructure. 相似文献
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Crack propagation velocity in delayed failure under superposed repeating load, (, was compared with that under static load, (Two peaks appear on the relation between decreasing rate of crack propagation velocity, and frequency, ?, both under sinusoidal and square load. By changing the ratio of holding time at maximum stress intensity factor to that at minimum stress intensity factor in square load, it was deduced that the existence of two peaks on the 1 ? β vs curve was caused by an asymmetric interaction between hydrogen atoms and cyclic moving of the position with triaxial tensile stress at crack tip. Moreover, the relation between 1 ? β and under the positive or negative saw tooth load could be well explained by the interaction model. 相似文献
7.
Silica-doped (SiO2 = 0 - 1.0 wt%) 3Y-TZP (3 mol % yttria-doped tetragonal zirconia polycrystal) ceramics are prepared from hetero-coagulated aqueous suspension by colloidal processing. Consolidation of the suspension was carried out by pressure filtration at 10 MPa followed by cold isostatic pressing (CIP) at 400 MPa. Consolidated compacts are densified to a relative density over 99% by sintering at 1573 K for 2 h. The formation of glass pockets at grain boundary multiple junctions was observed by SEM for ≥0.5 wt % silica-doped samples. Electrical conductivity measurements were performed to evaluate the modification of grain-boundaries by silica. The apparent grain boundary conductivity decreased with an increase in silica content and became nearly constant above 0.3 wt % of silica, while the bulk conductivity was constant with silica content. 相似文献
8.
Kiyoyuki Shimizu Tomohito Sunagawa Keijiro Arimura Hideshi Hattori 《Catalysis Letters》1999,63(3-4):185-188
Cyclohexane isomerization to methylcyclopentane over sulfated zirconia is markedly enhanced in the presence of isopentane
which acts as a hydride transfer agent to facilitate the slow step of hydride transfer from cyclohexane to isopropyl cation.
This was revealed by deuterium tracer studies.
This revised version was published online in July 2006 with corrections to the Cover Date. 相似文献
9.
Toshiko Mizokuro Hiroyuki Mochizuki Nobutaka Tanigaki Takashi Hiraga 《Thin solid films》2008,516(9):2411-2415
We report selective doping of vapor of yellow dye, ferrocenedimethanol into exposed (UV-irradiated) areas of novolac resin films. When vapor of the dye was contacted with micro-patterned resin films containing both exposed and unexposed areas, the dye was doped only into the exposed areas, resulting in fabrication of micro-pattern containing the dye. On the contrary, ferrocene and other ferrocene derivatives were doped both exposed and unexposed areas of the resin. A contact angle measurement of aqueous drops on each dye indicated that the chemical affinity between hydroxyl groups of ferrocenedimethanol and exposed areas of the novolac resin will enhance selective doping of the dye into the exposed areas. 相似文献
10.
Nobukata H. Takagi S. Hiraga K. Ohgishi T. Miyashita M. Kamimura K. Hiramatsu S. Sakai K. Ishida T. Arakawa H. Itoh M. Naiki I. Noda M. 《Solid-State Circuits, IEEE Journal of》2000,35(5):682-690
We report a fast-programming, compact sense and latch (SL) circuit to realize an eight-level NAND flash memory. Fast programming is achieved by supplying optimized voltage and pulsewidth to the bit lines, according to the programming data. As a result, all data programming is completed almost simultaneously, and 0.67-MB/s program throughput, which is 1.7 times faster than conventional program throughput, is achieved. The compact layout of the SL circuit is made possible by four 3-bit latches sharing one unit of the read/verify control circuit. Using these techniques, we fabricated a 144-Mb, eight-level NAND flash memory using a 0.35-μm CMOS process, resulting in a 104.2-mm2 die size and a 1.05-μm2 effective cell size 相似文献