Synthesis of Ta C and Ta_2C from tantalum and graphite in the laser-heated diamond anvil cell

The pressure dependence of the onset of the formation of Ta C and Ta2 C from the elements has been investigated by in situ X-ray diffraction and pyrometry.Ta C has been synthesized by the reaction of Ta and graphite at pressures between 8.6 and 14.3 GPa and at temperatures up to 2,300 K using a laser-heated diamond anvil cell. The products were characterized by X-ray diffraction. Ta and graphite begin to react around 1,100 K at ambient pressure conditions, and the reaction temperature increases with increasing pressure. A linear extrapolation of these data is consistent with recent observations of the formation of Ta C at 90 GPa and 3,600 K. We show that diffusion of carbon into tantalum significantly changes the lattice parameter of up to 2 % in the pressure range of up to19 GPa. In some experiments, Ta2 C was formed concomitantly. The experimentally determined bulk modulus of Ta2 C is B0;exp：= 286（5） GPa. Other tantalum carbide phases were not observed.     

基于LIF技术的煤矿水源识别系统应用

本文主要叙述LIF(激光诱导荧光光谱分析)技术的基本原理以及在水源识别中的应用,重点分析LIF技术的系统构成和主要模块的选择设计。通过该系统对某矿的送检水样和标准水样进行荧光实验,得到水样的荧光光谱图。传统的水源识别主要依据水中代表离子的离子浓度进行分析,但是从荧光光谱分析水中代表离子的离子浓度难度较大。本文提出一种较为简单且实用的方法由荧光光谱进行水源的精确识别,即使用相应分析软件分别测量未知水样与标准水样的欧氏距离,得出未知水样的精确分类。对未知水样的水源识别验证了该系统的可行性,解决了当前煤矿无法对突水情况进行实时在线监测的难题,对于煤矿的安全生产具有重要意义。     

Identification of proteinaceous binding media for the polychrome terracotta army of Emperor Qin Shihuang by MALDI-TOF-MS

A proteinaceous binding media for the polychrome terracotta army of Emperor Qin Shihuang has been identified using matrix-assisted laser desorption/ionization time-of-flight mass spectrometry(MALDI-TOF-MS).Methods for the preparation of the model samples and the elimination of interferences have been evaluated,as well as ageing processes.A method involving the complexation of EDTA in combination with dialysis was used to eliminate any interference in the polychrome layers taken from the historical samples.The model samples were aged by being buried in loess to replicate the ageing process of the historical samples as closely as possible.The optimum conditions for the extraction and subsequent enzymatic hydrolysis of the extracted protein were investigated.Under the optimized conditions,the‘‘peptide mass fingerprints’’of the proteinaceous binding media from the historical and model samples were determined by MALDITOF-MS.The results revealed that animal glue was used as the binding media for the polychrome layers of Emperor Qin Shihuang’s terracotta army.It also shows that animal glue used as binding media has a long history in China.     

Experimental investigation on upstream-injection interaction with a scramjet cavity flameholder

The study has evaluated the coherent structures and the velocity field of gaseous transverse jet upstream of a scramjet flameholder in a supersonic turbulent flow. The high spatiotemporal resolution coherent structures of the jet plume/wakes and the cavity shear layer were obtained by utilizing the nanoparticle-based planar laser scattering technique. Compared to the no upstream injection case, the cavity shear layer downstream of the jet shows significant mass exchange with mainstream. The particle image veloc- imetry velocity field and the velocity profiles demonstrated that the interaction intensity of the cavity shear layer with the upstream injection is further enhanced as the injection stagnation pressure increases.     

偏振旋转光反馈半导体激光混沌系统时延特征的隐藏

半导体激光混沌系统的时延特征为混沌通信攻击者重构非法接收机提供了线索,隐藏系统输出的时延特征能够提高通信的安全性。基于单模半导体激光器的理论模型,构建了偏振旋转光反馈半导体激光系统的动力学方程,利用自相关函数及时延特征峰相对高度,数值研究了该系统输出的时延特征。结果表明,在激光器合适的参数条件下,波片快轴方向在30°和60°附近一定范围内,反馈系数较小及偏置电流较大时,时延特征容易被隐藏。     

钛宝石飞秒激光系统及其应用

目前最为成熟的飞秒激光系统是基于啁啾脉冲放大技术（CPA）的太瓦级钛宝石飞秒激光系统。本文以东莞理工学院光电子技术实验室的钛宝石飞秒激光系统为例,主要介绍飞秒激光系统的组成和一些主流应用,为飞秒激光系统的搭建与商业化提供了可参考的路线和方向。     

舰艇雷达望远镜瞄准线和火炮膛线平行度调校

为了更好地提高舰艇雷达望远镜瞄准线和火炮膛线的平行度,本文提出了一种采用专利激光自动安平水准仪,校炮镜,方管前置镜,在舰艇上调校的方案。该专利产品安平精度为20″,基尺寸小,便于安装,调试灵活方便,能够解决由于舰艇上雷达,望远镜和火炮相距十几米远,该雷达,望远镜控制火炮困难的问题。从而实现雷达,望远镜瞄准轴线和火炮膛线的平行度。     

3D打印产业化难在哪

国外很多产品是定制化、个性化的,产量不是很,可以直接使用3D打印设备进行生产。而中国市场则更欢大规模制造生产出来的物美价廉的产品,对定制化、个化产品的接受程度有限,这在一定程度上制约了3D打印国内的应用和发展。     

激光投影显示的核心技术--多晶格激光屏的设计

随着现代科学技术的发展,在军用显示和民用高端显示领域对显示图像的清晰度、亮度的要求也越来越高,而传统的阴极射线投影显示管已经不能满足超高分辨率和高亮度投影显示这种迫切的要求.在大屏幕显示方面,一般是40英寸～50英寸(101.6～127cm)左右,投影对外围光线的要求太高.尽管出现了油膜光阀等技术,但是对比度低还是其致命的弱点.     

时尚科技

正能在几乎全黑的环境里拍摄的相机如果你认为低光摄影技术将在未来迅猛发展,那你必是还不了解这台新相机。这是一款麻省理工的研究者研发的新相机,它能够在只有极少量光子存在的情况下拍摄出物体清晰的影像。该技术是用可见激光的超低强度脉冲去扫描目标物体。激光将脉冲扫向制定位置,被反射回的单程光子会被高度灵敏的固态探测器记录下来。然后,激光会继续前进,反射过程就会重复进行。每一个被照到的位置都会给最终影像添上一个图素。该团队预期这个设备可以用于拍摄在高光下易损的物质,特别是生物结构,比如眼睛。有趣的是这项技术开辟了在不被侦查到的情况下获取图像的可能性,谁会不想要一台隐形相机呢?