Influence of accelerated ageing on methacrylate‐based denture resins heterogeneity as viewed by ESR‐spin‐probe method

The electron‐spin‐resonance (ESR) spin‐probe method, was used to study the heterogeneity of denture resins based on poly(methyl methacrylate). Results for three resins processed by microwave energy, conventional curing and cold curing (depending on the curing procedure and exposed to ageing in various environmental conditions) were compared. All three cured resins were stored over the same time (1200 h) in distilled water at ambient temperature and in artificial saliva at 348 K. The temperature‐dependent ESR spectra of a spin probe dispersed in the denture resins are analyzed in terms of line‐shapes and line‐widths. The appearance of two spectral components was taken as an indication of resin heterogeneity. The results reveal that the cold‐cured resin has a lower local density in comparison with microwave and conventionally cured resin. The amount of residual monomer also contributes to the local motion of polymer segments. The change of denture resins exposed to ageing is influenced both by the structure of the original resin and the ageing conditions. Restricted motion of a spin probe incorporated into the acrylic resins exposed to accelerated ageing suggests additional crosslinking of polymer chains. The differences are observed for all the investigated resins, but the highest change is observed with the cold‐cured resin. The ESR results are accompanied by T_g and T_m measurements. Copyright © 2005 Society of Chemical Industry     

Reconstruction of Mandibular Defect with Porous β-TCP/BMG Artificial Bone

1Introduction Reconstructivesurgeryisoneofthehottestre searchedsubjectsthatdealingwithbonedefects.Thetra ditionalmethodisimplantationoffreshautograftbonebe causeofitsnon immunoreactiveproperty.Butautologousbonewasnotabundantinsomecases.Sowefoundbeta trica…     

Formation of composites fabricated by exothermic dispersion reaction in A1-TiO2-B2O3 system

The formation of aluminum matrix composites fabricated by exothermic dispersion reaction in A1-TiO2-B2O3 system was investigated. The thermal analysis results show that the reactions are spontaneous and exothermic. The Gibbs free energy of α-Al2O3 is the lowest among all the combustion products, followed by TiB2 and Al3Ti. It is noted that when the B2O3/TiO2 mole ratio is below 1, the reaction products are composed of particle-like α-Al2O3, TiB2 and rod-like Al3Ti. The α-Al2O3 crystallites, resulting from the reaction between A1 and TiO2 or B2O3, are segregated at the grain boundaries due to a lower wettability with the matrix. SEM micrographs show that rod-like Al3Ti phase distributes uniformly in the matrix. When the BEO3/TiO2 mole ratio is around 1, the Al3Ti phase almost disappears in the composites, and the distribution of α-Al2O3 particulates is improved evidently.     

Preparation and Compressive Stress Effect of Polymer Matrix RE-Fe Giant Magnetostrictive Composite

Polymer matrix RE-Fe giant magnetostrictire composite （GMPC） was prepared using bonding and magnetic field forming technique, and magnetostriction of samples was measured for different compressive stress. The experimental results show thai there is certain compressive effect in GMPC. And the influence of compressive stress on magnetostriction of sample was investigated. It offers essential reference for application and device design of GMPC.     

General Solution for the Dynamic Modeling of Parallel Robots

In this paper, we present a general method to calculate the inverse and direct dynamic models of parallel robots. The models are expressed in a closed form by a single equation in which all the elements needed are expressed. The solution is given in terms of the dynamic models of the legs, the dynamics of the platform and some Jacobian matrices. The proposed method is applied in this paper on two parallel robots with different structures. Categories (2), (3).     

Average consensus in networks of dynamic agents with switching topologies and multiple time-varying delays

In this paper, we discuss average consensus problem in undirected networks of dynamic agents with fixed and switching topologies as well as multiple time-varying communication delays. By employing a linear matrix inequality method, we prove that all the nodes in the network achieve average consensus asymptotically for appropriate communication delays if the network topology is connected. Particularly, several feasible linear matrix inequalities are established to determine the maximal allowable upper bound of time-varying communication delays. Numerical examples are given to demonstrate the effectiveness and the sharpness of the theoretical results.     

A parallel and scalable algorithm for ADI method with pre-propagation and message vectorization

It is hard to implement the ADI method in an efficient way on distributed-memory parallel computers. We propose “P-scheme” which parallelizes a tridiagonal linear system of equations for the ADI method, but its effectiveness is limited to the cases where the problem size is large enough mainly because of the communication cost of the propagation phase of the scheme.

In order to overcome this difficulty, we propose an improved version of the P-scheme with “message vectorization” which aggregates several communication messages into one and alleviates the communication cost. Also we evaluate the effectiveness of message vectorization for the ADI method and show that the improved version of the P-scheme works well even for smaller problems and linear and super-linear speedups can be achieved for 8194 × 8194 and 16,386 × 16,386 problems, respectively.     

几种OLED有源驱动电路中像素单元电路的分析

在有机电致发光器件两管单元有源驱动电路的基础上．分析了几种四管单元电流控制型和电压控制型的驱动电路，它们都能补偿TFT阈值电压的漂移．但都有各自的优缺点：前者能准确地调节显示的灰度，但它的响应速度慢；后者的响应速度快，但不能准确地调节显示的灰度。     

MSP-G320240DBCW-211N大规模点阵式LCD与PIC单片机接口技术

介绍了大规模点阵式液晶显示器MSP-G320240DBCW-211N的特点及其与PIC18F6620单片机的接口技术，提出了应用过程中可能遇到的问题和解决方法．给出相关的C程序设计并在研制的智能光电检测仪器上得以成功地应用。     

Fracture toughness of thermoset composites reinforced by perfectly bonded impenetrable short fibers

The fracture toughness of brittle thermoset resins could be improved significantly by perfectly bonded tough, short fibers through both crack trapping and bridging effects. In this paper, the crack trapping effect was studied through the analysis of the change of strain energy associated with the crack propagation across a regular array of fibers, and the bridging effect was discussed based on the Andersson–Bergkvist model. The fracture resistance increases with the fiber volume fraction, and is independent of the elastic properties of the matrix, the crack length, and the cross-sectional diameter of the fibers.