取样光栅周期中等效啁啾的实验研究

在Moire取样Bragg光纤光栅（SBG）的理论基础上，首次通过用相位模板旋转和2次曝光的方法，得出了带有取样啁啾的SBG的各个Fourier级数的等效啁啾率。实验数据和理论值的误差小于9%。     

长江采砂监管系统的设计与研究

文章阐述了建立长江采砂监管系统的必要性，以及依据《长江河道采砂管理条例》和采用GIS、GSM、GPS等技术建立该系统的解决方案，使用该系统可以对采砂的船舶位置，产量，时段进行实时的监控，根据船舶运行轨迹，采砂规划数据库，许可证数据库评价采砂船的违规情况，使长江采砂真正达到科学、合理，有序的效果。     

~(131)I-Lym-2单克隆抗体实验研究

不同浓度的~(131)I-Lym-2 MoAb与ARH-77和CEM细胞进行结合试验,结果表明:随浓度增大,结合值均升高;实验组裸鼠模型9只获得动力学数据。实验组和对照组注射~(131)I-Lym-2 MoAb后144h解剖,进行生物学分布(％D/g)测定,实验组肿瘤为16.88±12.64,肌肉为0.72±0.56。结果表明,~(131)I-131-Lym-2MoAb对临床B细胞淋巴瘤的放射免疫分析、显像有良好的效果。     

用各向异性介质构造的一维光子晶体的特性分析

本文根据单轴晶体的传输矩阵，研究了一种由各向异性介质周期排列构成的一维光子晶体，分析了在不同入射角度和折射率条件下，该周期结构的反射和偏振的光学特性。分析结果表明，各向异性介质在折射率比值较大或与高折射率同性介绍结合使用，可获得较宽的禁带，并可实现在可见光范围内的全偏振全角度反射。     

GAO Feng~1,LI Wei~2,TANG Zon

tific Experiment Center of Guangxi Medical University,Nanning 530021,China)Objective:To investigate the mutation pattern of adenomatous polyposis coli(APC),Kirsten-ras(K-ras) and p53 genes in sporadic colorectal cancer tissues.Meth     

北京谱仪端盖簇射计数器工作气体的研究

为使北京谱仪端盖族射计数器更好地工作在自猝灭流光ＳＱＳ模式下，提高其能量分辨以及线性等指标，用Ａｒ，ＣＯ２，Ｌｓｏｂｕｔａｎｅ三元工作气体对探测器的工作性能进行了仔细研究，找出了一适合于主雇地数器的工作气体，此外，还研究了异丁的纯度对探测器性能的影响。     

An IR study on ion-specific and solvent-specific swelling of poly(N-vinyl-2-pyrrolidone) gel

Swelling degrees of poly(N-vinyl-2-pyrrolidone) (PVP) gel were measured in aqueous salt solutions and in water/organic solvent mixtures to find marked ion- and solvent-specificities. In order to investigate any correlation of those specificities with hydration or solvation of PVP, IR spectra band of the CO group was monitored by means of ATR method both for PVP gel and the relevant solution systems. Dependence of the peak frequency on the swelling ratio suggested that hydration of PVP carbonyl group in deswollen gel systems is different from that in the corresponding solution systems. In the solution systems, PVP carbonyl band showed a high-wavenumber shift for deswollen systems, which can be well correlated with changes in water proton charge through ionic hydration and with Gutmann's acceptor number of organic solvents. In the deswollen gel systems, the CO band showed a low-wavenumber shift, suggesting a strong hydration or doubly hydrated state. This unexpected behavior was interpreted by assuming an intermolecular hydrogen bond of two carbonyl groups intermediated by water molecules.     

In situ polyurethane/silica composite formation via a sol‐gel process

Polyurethane acrylate anionomer (PUAA)/silica composite gels were prepared by the sol‐gel reaction of tetraethoxysilane (TEOS) and methacryloxypropyl trimethoxysilane (MPTS) incorporated to PUAA gels by using a swelling method. The formation and structure of composites were confirmed by FTIR, X‐ray diffraction, and SEM. As a result, we found that silica components in composites are located within the ionic domains of their gels and interacted with PUAA via hydrogen bonding. This drastically enhanced the mechanical properties of the composites. Mechanical properties are also improved by MPTS, because MPTS improves the dispersibility and adhesion of silica components in PUAA/silica composite gels. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 84: 2327–2334, 2002     

Formation and investigation of epoxy intumescent compositions modified by active additives

Results are reported of research on intumescent composites based on epoxy resin cross‐linked with polyethylene polyamine and containing ammonium polyphosphate and such modifying additives as calcium borate, manganese dioxide, nickel, and chromium, containing tubulenes as gas‐formers and carbonization stimulators. The changes in composition and physicochemical properties of modified compositions under conditions of heat and fire were investigated by X‐ray photo‐electron spectroscopy, atomic force microscopy, and local force spectroscopy. Ammonium polyphosphate mainly stimulates carbonization processes on the inner surface of a bubble being formed during foam coke formation. The introduction of metal‐containing tubulenes leads to the formation of fire‐retardant and low flammability‐compositions with high coke and carbon structures content. The use of calcium borate in the compositions considerably increases the strength of foam coke being formed. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 85: 1477–1483, 2002     

DSC and DMTA characterization of ternary blends

The phase behavior of ternary blends made of poly(epichlorohydrin) (PECH), poly(vinyl acetate) (PVAc) and poly(methyl methacrylate) (PMMA) has been investigated by differential scanning calorimetry (DSC) and dynamic mechanical thermal analysis (DMTA). DMTA measurements have been shown to be more sensitive than DSC for the detection of a second phase, for the determination of the composition of each phase, and the distribution of PECH in each of them. About 70% PECH was required to obtain a single narrow T_g in the ternary system, which suggests a single homogeneous phase in the limit of sensitivity of DMTA. This study also emphasizes the importance of the composition of the immiscible polymer pair (i.e. the PVAc/PMMA pair in the PECH/PVAc/PMMA system), in addition to the thermodynamic interaction parameters, for controling the phase behavior of ternary systems.