用热分析仪检测球化率的实践

对球铁球化处理后判断球化效果的几种检测方法进行了比较。设计了一种双通道热分析系统，并进行了检测球化率的实验，结果表明：热分析法得到的球化率数据与金相检查得到的数据有密切的相关性，而两者与声速球化分析的结果相关性则较差。双通道热分析法不但可以对球化与否进行判断，还可以进行具体球化率和球墨大小的评定。     

热压变形对灰口铸铁石墨形态的影响

研究了灰口铸铁(HTl50)在900℃大压下量塑性变形后石墨的分布形态，结果表明：随着压下量的增加，石墨片逐渐趋于平行分布；变形过程中发生了碳的回溶，同时伴随着石墨片的断裂；石墨片体积分数及片间距随压下量的增加而逐渐减少。     

微合金化蠕墨铸铁玻璃模具材质的研究

介绍了微合金化蠕墨铸铁玻璃模具材质的组织、力学性能及热物性，探讨了影响其性能的诸多因素。结果表明：这种材质具有较高的综合性能指标，具有良好的使用性能和显著的经济价值和社会效益。不仅适于与玻璃模具，还可广泛地应用于冶金、塑料和橡胶行业。     

石墨电极的研究与实践

介绍了石墨材料的有关性能、石墨组合电极的结构形式和其在生产现场中的应用情况及注意事项，并将石墨组合电极的性能特点与传统的钢质电极进行了对比，从而达到推广应用的目的。研制了与以往启动装置完全不同的石墨启动电极，为盐炉启动技术的发展，提供了新的途径。     

蠕墨铸铁在铁道车辆制动系统中的应用研究

在分析车辆制动器摩擦温度场的基础上 ,研究蠕墨铸铁在铁道车辆制动系统中的使用性能 ;研究结果表明 ,在车辆制动器服役条件下 ,摩擦速度与接触压力的提高 ,摩擦副的摩擦系数显著降低 ,磨损率显著增加 ;在所研究的不同石墨形态的铸铁中 ,蠕墨铸铁不但具有低而稳定的磨损率 ,而且具有高而稳定的制动性能 ,是制造车辆制动器部件的合理选材。     

掺杂石墨/Cu钎焊接头残余应力的分布特征及中间层的作用

利用有限元方法,模拟分析了掺杂石墨/Cu钎焊接头残余应力的分布特征。分析结果表明,对接头有害的较大残余应力分布在石墨棱角距离焊缝约0.8mm处的狭小区域;降低连接温度、减少连接时间及增加钎焊压力均有利于减小接头残余应力,优化接头的界面应力状态;中间层的加入在一定程度上缓和了接头的残余应力。从缓和效果来看,Cu比Mo作中间层好,而Cu/Mo复合中间层的缓和效果最好,是较理想的中间层材料。     

Influence of expandable graphite on fire resistance and water resistance of flame-retardant coatings

Expandable graphite (EG) coating and ammonium polyphosphate-pentaerythritol-melamine (APP-PER-MEL) coating were prepared. Thermal degradation and char formation of the coatings were investigated by differential thermal analysis (DTA), thermogravimetry (TG), X-ray diffraction (XRD), scanning electron microscopy (SEM) and X-ray photoelectron spectroscopy (XPS). The results have shown that the anti-oxidation and fire-resistant properties of expandable graphite coating containing EG with size of 74 μm are better than those of APP-PER-MEL coating. The static immersion test was applied to study water resistance of the coatings, and the fire protection test and mechanical test were used to analyse heat insulation and mechanical properties of coatings before and after water immersion. The fire-resistant and mechanical properties of APP-PER-MEL coating were severely damaged by water immersion, whereas EG coating containing 8.5% EG with size of 74 μm could retain the good fire resistance even after 500 h water immersion.     

同质焊缝球墨铸铁焊条的研制

研制了一种适合于球墨铸铁与球墨铸铁以及球墨铸铁与结构钢焊接的专用球墨铸铁焊条，通过试验确定了球墨铸铁焊条的合金成分并给出了比较合理的焊芯和焊条药皮化学成分。采用该焊条对球墨铸铁焊接时，可以达到同质焊缝要求。测试结果表明，焊缝金属的化学成分、金相组织均满足焊接球墨铸铁的要求，焊缝的硬度在190～230HB之间，焊缝中石墨球化稳定，焊条具有良好的焊接工艺性能。     

高炉用石墨砖的现状及问题

介绍了近年来我国高炉用石墨砖的进展和存在的问题，提出了高炉用石墨砖的改进方向。     

Microwave assisted ultrafast synthesis of graphene oxide based magnetic nano composite for environmental remediation

We have successfully synthesized multi-layer graphene oxide and graphene oxide based magnetic nanocomposite (M/GO) by microwave-assisted modified Hummers’ method for removal of toxic lead (Pb²⁺) and cadmium (Cd²⁺) ions from aqueous solution. The X-ray diffraction spectra of synthesized graphene oxide and M/GO confirm increased interlayer spacing along c-axis. Raman spectra revealed the good quality of synthesized GO and M/GO. The wrinkles were seen in the SEM images of synthesized graphene oxide. The presence of conjugated double bond (CC) and carbonyl (CO) were confirmed by using the UV–Vis spectroscopic spectra. Brunauer–Emmett–Teller (BET) analysis showed high (126 m²/g) surface area M/GO composite which accounts for large number of active binding sites for the adsorption of heavy metal ions. The adsorption studies revealed that Pb²⁺ ions were efficiently adsorbed on GO sheets. Interestingly, M/GO showed better adsorption for cadmium ions.