Synthesis and electrochemical properties of Th-doped LiMn2O4 powders for lithium-ion batteries

To improve the cycle performance of eco-friendly and cost-effective spinel LiMN2O4 as the Li secondary batteries, the Th-doped LiThxMn1-xO4 spinel powers were synthesized by solid-state method. The starting materials, Li2CO3,MnO2 and Th(NO3)4·4H2O, were mixed uniformly using a traditional ball milling, which resulted in a uniform particle size distribution in the mixed powers. Tests of X-ray diffraction, SEM, impedance spectra and charge-discharge were carried out for LiThxMn1-xO4 cathode materials. Results show that the synthesized LiTh0.01Mn1.99O4 material exhibits standard spinel structure, regular particle morphology and excellent property of charge-discharge for big current. The capacity retention of the material modified by doping Th is more than 85.1% of the first discharge specific capacity of 111.5 mAh·g -1 after 20 cycles at the current rate 1C, while the pristine LiMN2O4 is only 57% of the first discharge specific capacity of 110.2 mAh·g-1 after the same cycles at the same current rate.     

甲型肝炎病毒(L-A-1株)基因型分析

目的 分析甲肝病毒基因型,为确定我国甲肝的分子流行病学及疫苗的安全性和免疫原性奠定基础。方法 采用抗原捕获聚合酶链反应（AC/PCR）,依据国际上甲肝病毒分型标准,扩增VP1/2A结合处的168个核苦酸（nt2909～3264）。结果 经生物信息学软件分析,得出L-A-1株病毒属于甲肝病毒基因IB亚型。结论 在我国有IA和IB两个亚型甲肝病毒流行。     

双电层电容器用沥青焦基活性炭的制备工艺条件对其孔结构及电化学性能的影响

以沥青焦为原料，KOH为活化剂在不同的工艺条件下制备了双层电容器用活性炭电极材料。分别考察了活化剂用量、活化时间、以及加入Cu、Ni催化活化等工艺条件对活性炭孔结构及作为双电层电容器电极的电化学性能的影响。结果表明：在实验范围内增加KOH用量及活化时间，活性炭的比表面积和比电容增加，比电容最高达到247F／g。添加Cu、Ni催化活化后活性炭的比表面积及比电容增加，高功率放电性能明显改善。     

交流接触器温度场仿真及试验验证

将ANSYS有限元热分析应用到交流接触器热特性分析中,模仿其实际工作环境,构建交流接触器三维稳态热分析模型,确定热源、导热系数和表面散热系数,对接触器的稳态温度场进行分析;进一步改变施加的边界条件,研究不同散热方式下接触器的温度分布。最后对CJX2-0910型交流接触器进行温升试验,将温度场的仿真结果与试验结果比较,误差较小,表明所建立热分析模型的可行性。研究结果对接触器材料的选择、结构的设计及其性能的优化有重要意义。     

Towards subject independent continuous sign language recognition: A segment and merge approach

This paper presents a segment-based probabilistic approach to robustly recognize continuous sign language sentences. The recognition strategy is based on a two-layer conditional random field (CRF) model, where the lower layer processes the component channels and provides outputs to the upper layer for sign recognition. The continuously signed sentences are first segmented, and the sub-segments are labeled SIGN or ME (movement epenthesis) by a Bayesian network (BN) which fuses the outputs of independent CRF and support vector machine (SVM) classifiers. The sub-segments labeled as ME are discarded and the remaining SIGN sub-segments are merged and recognized by the two-layer CRF classifier; for this we have proposed a new algorithm based on the semi-Markov CRF decoding scheme. With eight signers, we obtained a recall rate of 95.7% and a precision of 96.6% for unseen samples from seen signers, and a recall rate of 86.6% and a precision of 89.9% for unseen signers.     

Reaction Coupling of Ethylbenzene Dehydrogenation with Nitrobenzene Hydrogenation

The chemical equilibrium for the coupling of ethylbenzene dehydrogenation with nitrobenzene hydrogenation, to produce styrene and aniline simultaneously, has been calculated on the basis of the Soave–Redlich–Kwong equation of state. The dehydrogenation of ethylbenzene in the presence of nitrobenzene over the catalysts -Al₂O₃, ZSM-5, activated carbon and platinum supported on activated carbon has been carried out at 400 °C. The effects of Pt loading and the pretreatment of the catalysts have been investigated. It has been revealed that the conversion of ethylbenzene can be greatly improved by the reaction coupling due to the elimination of the hydrogen produced in the reaction by the hydrogenation of nitrobenzene. Platinum supported on the activated carbon has been suggested as a suitable catalyst. The best results with ethylbenzene conversion of 33.8% and styrene selectivity of 99.2% were obtained over Pt(0.02 wt%)/AC at 400 °C. Moreover, such process is also energetically favored since the necessary process heat to drive the ethylbenzene dehydrogenation can be provided by the coupling with the exothermic nitrobenzene hydrogenation reaction.     

A study of PtRuO2 catalysts thermally formed on titanium mesh for methanol oxidation

Platinum-based catalysts, for the electro-oxidation of methanol, have been made by thermal decomposition of chloride precursors onto titanium mesh. The catalysed electrodes were successfully operated in acidic methanol electrolytes. Electrochemical characterisation has been carried out using cyclic voltammetry, electrochemical impedance spectroscopy and galvanostatic polarisations. A complete analysis of the electrochemical results showed that the preliminary performance of the catalysed titanium mesh was comparable to that achieved with carbon-supported PtRu catalysts. The catalysts formed on titanium mesh by thermal decomposition also exhibited dimensional stability. Catalysed titanium mesh therefore appears to be a promising alternative to carbon-supported catalysts for certain fuel cell applications.     

一种32位浮点型处理器的励磁控制器设计

针对同步发电机励磁控制系统在控制精度和控制稳定性方面存在的不足,通过对国内外励磁控制系统发展状况的分析,提出了一种基于32位浮点型处理器的数字式励磁控制系统.该系统通过将先进的交流采样算法和DSP的优异性能相结合,实现了励磁控制器的深度数字化;通过对同步发电机系统关键模拟量的采集与计算,得出适用于当前工况下触发脉冲角度α.试验验证了该设计能很好地解决发电机励磁控制系统中的稳定性问题.     

15%恶霉灵防治水稻立枯病药效试验

田间试验表明，15％恶霉灵水剂6～8ml／m^2，对水稻立枯病的防效可达82.3％，病指防效可达89.4％，明显好于对照药剂。而且对水稻安全，能够提高秧苗素质。     

卧螺离心机共直流母线双电机双变频驱动

介绍了卧螺离心机差转速自动控制共直流母线变频调速系统的结构,分析了工作原理和节能效果,介绍了直流母线的两种并接方法。