工艺参数对磨削硅晶圆亚表面损伤裂纹的影响

为研究粗磨硅晶圆亚表面微裂纹,采用截面显微观测法,实验研究了粗磨工艺下砂轮进给速率、砂轮转速和硅晶圆转速对晶圆亚表面裂纹的影响.结果表明:磨削后晶圆亚表面斜线裂纹和折线裂纹占70%,中位裂纹、分叉裂纹和横向裂纹占30%,裂纹形状与工艺参数的关系不大.裂纹深度从晶圆圆心向外逐渐增大,〈110〉晶向裂纹深度稍大于〈100〉晶向.裂纹深度随砂轮进给速率增大单调增加,随砂轮转速增大单调减小.裂纹深度与晶圆转速之间的关系复杂,晶圆转速增大时,裂纹深度先是减小,然后增大.提出了磨削工艺参数的优化措施.     

聚羧酸助磨剂合成及其性能

利用水泥粉磨过程中的机械力促使水解聚马来酸酐（HPMA）与聚乙二醇单甲醚（MPEG）进行酯化反应形成聚羧酸助磨剂。试验研究了HPMA、MPEG、HPMA与MPEG的混合物、HPMA与MPEG的反应合成物对水泥助磨效果以及对砂浆性能的影响。结果表明,HPMA与MPEG都有一定的助磨性,HPMA与MPEG的混合物和反应合成物具有更佳的助磨性能,且可以改善水泥砂浆的流动性能和显著提高水泥砂浆的早期强度。激光拉曼光谱测试表明HPMA与MPEG的混合物和反应合成物与水泥共同粉磨后吸附在水泥颗粒表面,具有相似的拉曼位移图谱。     

超细矿粉对混凝土界面区硫酸盐腐蚀的影响

为了研究骨料与水泥石界面区(ITZ)的组成及结构对混凝土抗硫酸盐腐蚀性能的影响,利用紫外分光光度计绘制了硫酸钠溶液浸泡混凝土试样的SO2-4浸入浓度/深度曲线,并辅以扫描电镜(SEM)和电子探针能谱(EDS)等对ITZ进行观测;同时利用XRD定量分析研究了混凝土本体相和界面相的水化产物富集的差异.结果表明:Ca(OH)2、钙矾石(AFt)等晶体富集于硫酸钠溶液浸泡后试样的ITZ,引起AFt二次结晶型的硫酸盐腐蚀破坏.在适量石膏的激发下,掺入超细矿粉(GGBS)可阻止AFt转变成单硫型水化硫铝酸钙(AFm),减少AFt二次结晶的生成,明显提高抗硫酸盐侵蚀能力,试样的同深度硫酸根浓度最低,抗硫酸盐侵蚀性能最好.     

Simulation of clinker grinding circuits of cement plant based on process models calibrated using GA search method简

Particle size distributions of obtained samples from several sampling campaigns were determined and raw data were mass balanced before being used in simulation studies.After determination of breakage function,selection function,Bond work index,residence time distribution parameters,and Whiten＇s model parameters for air separators and diaphragms between the two compartments of tube ball mills,performance of the circuits was simulated for given throughputs and feed particle size distribution.Whiten＇s model parameters were determined by GA（genetic algorithm） toolbox of MATLAB software.Based on implemented models for modeling and simulation,optimization of circuits was carried out.It increased nearly 10.5% and 15.8% in fresh feed capacity input to each tube ball mill.In addition,circulating load ratios of circuits are modified to 118% and 127% from low level of 57% and 22%,respectively,and also cut points of air separators are adjusted at 30 and 40 μm from high range of 53 and 97 μm,respectively.All applications helped in well-operation and energy consumption reduction of equipments.     

基于HHT的磨床磨削颤振特征量提取方法

针对数控磨床磨削加工过程中的颤振现象,提出一种基于希尔伯特黄变换的磨削颤振特征量提取方法。采用经验模式分解,将信号分解成具有不同特征时间尺度的固有模态函数分量,筛选合适的分量,提取其颤振特征量实时方差和瞬时能量,并将其作为判断磨削发生颤振的依据。模拟仿真结果表明：基于希尔伯特一黄变换提取的磨削颤振特征量,可以作为颤振发生的判断依据。     

微-纳米复合陶瓷超声振动磨削的塑性-脆性 转变特征研究

基于工件超声振动磨削的单磨粒运动模型,建立超声振动磨削单磨粒最大切削厚度agm ax公式;基于压痕断裂力学,给出硬脆材料超声振动磨削塑性-脆性转变临界条件,进行超声振动磨削与普通磨削对比试验,应用SEM和AFM分析陶瓷磨削表面微观形貌特征,重点研究磨削参数对其塑性-脆性转变特征的影响。研究结果表明,砂轮平均磨粒尺寸是影响塑性-脆性转变最为主要的因素,砂轮速度对其影响次之,磨削深度对塑性-脆性转变的影响最小;得出只有当agm ax小于临界切削深度agc时,才能实现硬脆材料塑性域磨削的重要结论。     

Fine grinding of thermoplastics by high speed friction grinding assisted by guar gum

High speed friction grinding has been used to grind plant and food substances in water but never been explored for grinding of thermoplastics like polylactic acid (PLA), low and high density polyethylene and polypropylene. Such grinding was investigated in this work and was made possible by using 0.5% guar gum solution instead of just water because increasing the viscosity of water reduced their settling and the speed of passing through the grinder. Tensile, flexural, and impact strengths of the plastics were studied and higher grinding efficiency of PLA could be explained by its low elongation-at-break compared to low density polyethylene, high density polyethylene, and polypropylene. The microplastics (2000–45 μm) were studied for mass and particle size distributions and by scanning electron microscopy, ¹³C CP/MAS NMR, Fourier transform infrared spectroscopy, differential scanning calorimetry, and thermogravimetric analysis. In addition, viscosity of guar gum and contact angles was measured. This new technology can produce finely ground microplastics (710–45 μm) for a variety of applications.     

Investigation of Creep Feed Grinding Parameters and Heat treatment Effects on the Nickel-base Superalloys

The Nickel base Superalloys are the most famous complicated and useable of Superalloys to make hot zone components of the gas turbines. The complicated dimensional tolerances, specially at the root of the blade show importance of grinding processes at the production of blades root. The prediction of the effect of machining parameters on the soundness of component surface strengthening for reaching to a suitable surface finishing and avoiding from crack formation at the work part during machining operation often is not easy and feasible so needs to more industrial investigation.This research is about frame 5 blade designed by GE and made from Superalloy IN738LC has been investigated. The formation of a plastically deformed and heat affected zone during grinding of Superalloy IN738LC with a high depth of cut but slow work speed (creep feed grinding) was investigated. Parameters such as work speed, depth of cut and radial dressing speed have been considered as variables and their effects have been studied. During experimental performed, the voltage and current of motor measured and power and special energy calculated.Some samples heat-treated (of the 1176℃ for 1 hr under neutral argon gas and cooling rate of 15℃/min up to 537℃ and then air cooling) to study grains recrystallization. Other samples have been created from the roots of blades and then coated by Nickel to measure boundary layer micro-hardness. The results show that increasing work speed leads to increasing the use power. Increasing the depth of cut, by increasing material removal rate, and the radial dressing speed, by decreasing power, lead to decreasing special energy. The temperature created by grinding lead to decreasing plastic deformation and boundary layer formation. When the radial dressing speed changes from 1 to 0.6μm/rev and other parameters are kept unchanged the roughness of surface increases and the special energy decreases. Sufficient dressing is very essential in limiting the width of the molten zone to few micrometers. As a result, it was found that local melting at contact spots to be a rather common mechanism during grinding of superalloys, lead to so-called white layers which can easily be observed on metallographic cross sections.     

多元醇还原制取球形钴粉

以自制 Co(OH) 2 为原料 ,乙二醇为溶剂和还原剂 ,制得了分散性很好的球形超细钴粉。研究了单位体积乙二醇中 Co(OH) 2 加入量对钴粉的粒径和形貌的影响。用SEM、XRD、BET和激光粒度分析仪测试粉体的粒子形貌、晶体结构、比表面积和粒度分布。测试结果表明多元醇还原的钴粉为球形 ,以面心立方晶体为主 ,还有微量的简单六方 ;钴粉粒度分布较窄 ,平均粒径为 0 .88μm,比表面积为 3 .46m2 /g,钴含量 >99.5 %。     

250m/s超高速磨床主轴磁浮轴承设计

本文介绍了磁浮轴承的优点，并针对一台250m/s超高速磨床主轴系统，首次进行了磁浮轴承设计，其结果对我国发展高速主轴技术有一定意义。