填充HDPE复合材料基体结晶形态的控制因素

本文以HDPE/玻璃微珠和HDPE/CaCO₃体系为研究模型,通过扫描电镜、红外光谱、偏光显微、小角激光散射和材料力学性能实验等方法考察了这两种体系的界面粘结性、填料含量、粒径及试样成型冷却速率等与其材料性能及基体结晶形态变化间的关系。实验结果表明;在复合材料试样成型过程中,因基体树脂冷却收缩而产生的界面应力可干扰基体中球晶的生长环境,应变诱导填料颗粒周围基体树脂的结晶,促使其表面伸展链晶体结构的形成,并由此而明显改变了复合材料的耐热性;复合材料的界面粘结性是产生这种应变诱导作用,并控制异相结晶的关键。     

VHF-PECVD制备微晶硅材料的均匀性及其结构特性的分析

采用VHF-PECVD技术在多功能系统(cluster tool)中制备了系列硅薄膜，研究薄膜的均匀性及电学特性和结构特性。结果表明：气压和功率的合理匹配对薄膜的均匀性有很大的影响；材料的喇曼测试和电学测试结果表明微晶硅薄膜存在着纵向的结构不均匀，在将材料应用于器件上时，必须要考虑优化合适的工艺条件；硅烷浓度大，相应制备薄膜的晶化程度减弱，即薄膜中非晶成分增多。     

Structural and electrical measurements of CdZnSe composite

TheI—Vcharacterization and the electrical resistivity of selenium rich Se₈₅Cd_15-xZn_x (x = 0, 3, 7, 11 and 15) system at room temperature have been studied. Samples were obtained using melt cooling technique. So prepared samples were then characterized in terms of their crystal structure and lattice parameter using X-ray diffraction method. The materials were found to be poly crystalline in nature, having zinc blend structure over the whole range of zinc concentration. The measurements ofI—V bdcharacteristics have been carried out at different temperatures from room to 140°C. The electrical resistivity of the samples with composition at room temperature has been found to vary between maximum 2.7 x 10⁸ Ωm and minimum 7.3 x 10⁵ Ωm and shows a maximum at 3 at. wt.% of Zn. The carrier activation energy of the samples with composition has also been determined and found to vary from 0.026 eV to 0.111 eV.     

α－Al_2O_3衬底上生长的GaN膜的光学性质

采用金属有机化学气相淀积（ＭＯＣＶＤ）方法生长了α－Ａｌ２Ｏ３衬底上外延的高质量的单晶ＧａＮ薄膜。Ｘ射线衍射光谱与喇曼散射光谱表征了ＧａＮ外延薄膜的单晶结构和单晶质量。透射光谱和光调制反射光谱定出了六角单晶ＧａＮ薄膜的直接带隙宽度和光学参数。     

A study of the static and dynamic properties of side-chain liquid crystalline polymers in low molar mass mesogens

The static and dynamic properties of solutions of a side chain polysiloxane liquid crystal polymer have been studied in a cyanobiphenyl nematic host as a function of concentration and temperature. Refractive index measurements were carried out on aligned samples and the data used to determine the macroscopic order parameter, S, using Haller's method. Photon correlation spectroscopy has been used to measure ($\text{k}{}_{22}\text{γ}{}_1$) for the pure nematic solvent and the solutions. From these measurements it appears that the static properties vary slowly and linearly with increasing polymer concentration whilst the dynamic or viscoelastic properties change markedly. This change has been attributed to γ₁, the twist viscosity, and the results have been discussed in terms of the function of the siloxane polymer backbone.     

用测井资料预测储层的润湿性

岩心电性及润湿性实验测量结果表明，润湿性对阿尔奇饱和度指数n有很大影响。通过引入相对润湿指数，发现阿尔奇饱和度指数n的对数与相润湿指数之间存在很好的线性关系，为利用饱和度指数预测储层的润湿性提供了依据。同时使用电磁波传播测井和微球形聚焦电阻率测井求出饱和度指数随地层深度的变化曲线，预测储层的润湿性。现场井资料处理结果表明，该方法能快速直观显示不同深度处储层润湿性的变化。     

硫对注入YSZ单晶的金属铂在退火过程中结晶的影响

秀卢瑟福背散射－沟道技术（ＲＢＳ－Ｃ）和Ｘ射线衍射技术（ＸＲＤ）研究了Ｐｔ和注入ＹＳＺ（Ｙ２Ｏ３稳定的ＺｒＯ２）后产生的损伤和退火过程中损伤的恢复及注入Ｐｔ的晶化，ＲＢＳ－Ｃ分析表明ＹＳＺ室温下的存在较强自退火效应，ＸＲＤ分析结果示出硫以铂的晶化产生很大影响。     

Sidechain liquid crystal polymers

Research has continued in the field sidechain liquid crystal polymers over recent years, but it is becoming clearer that this research is being directed away from the traditional technology areas of electro-optic devices and researchers are developing new and exciting applications for this novel state of matter.     

单色光石英退偏器的退偏机理及性能研究

研究了单色光石英退偏器的退偏机理；定义了退偏度作为衡量退偏器性能的物理量。从实验上在４４０～９２０ｎｍ的光谱范围测试了器件的退偏度，结果表明：只要器件的结构角适当，或者适当调节入射光束的截面大小，便可对某一单色线偏振光实现很好的退偏。     

砂土中支盘桩抗压性能试验研究

支盘桩轴向受压过程是桩与周围土体相互作用的过程,研究支盘桩桩周土体的变形破坏机理对支盘桩竖向承载力的预测具有重要的意义。通过利用粒子图像测速技术进行了一系列的室内双支盘桩模型试验,对轴向荷载作用下支盘桩桩周土体变形特性进行非介入式测量。试验结果表明,不同相对密度下的荷载－位移曲线存在明显差异,相对密度增大可以大幅度提高双支盘桩竖向承载力并有效减小桩基沉降,密砂中双支盘桩的极限承载力是松砂的两倍以上。试验中发现支盘间距对支盘桩的竖向承载力有显著影响,随着盘间距的增加,支盘桩承载力增大但承载力增长率呈现出逐渐减小的趋势。针对地基土为密实砂土时,双支盘桩的支盘间距宜取盘径的３倍。