Detection of failure sites by focused ion beam and nano-probing in the interconnect of three-dimensional stacked circuit structures

Focused ion beam (FIB) and nano-probing were applied for failure analysis of three-dimensional stacked circuits with copper through-silicon-vias between the stacked chips. The failure analysis was done after high temperature storage and thermal cycling tests. Passive voltage contrast in FIB allowed to pinpoint the open sites. FIB cross-sections showed the presence of opens at the bottom of the copper vias. The failure cause was suspected to be an interlayer particle, which was confirmed by optical profilometry. Nano-probing was used on another sample to pinpoint the failure location through the measurement of the local resistance within the daisy chains. The failure was traced out to be related with surface contamination.     

An Investigation of Vibration Reducing on a Machine Tool

In order to reduce the vibration on a machine tool, more orthogonal experiment schemes have been designed, which are based on the steel balls vibration reducing principle. After experiments the optimal reducing vibration scheme was determined. This kind of vibration reducing scheme is used in steel balls vibration absorber, which can be used to reduce vibration magnitudes of a machine tools under the working conditions, whereby improving machining precision. The suggested experiment method is of useful reference in reducing vibrations on other machine tools too.     

蒸发氧化法制备高品质活性氧化镉粉末

开发了高品质活性氧化镉粉末的制备工艺，系统地探索了工艺条件对氧化镉电池材料电化性能的影响。对样品进行了物化性能及电性能检测，结果表明，采用蒸发氧化法可制备出镍镉充电电池用高品质活性氧化镉粉末。     

High Gd Concentration GaGdN Grown at Low Temperatures

GaGdN layers were grown at temperatures below 300°C by radio-frequency plasma-assisted molecular beam epitaxy on sapphire substrates. GaGdN samples with high Gd concentration as high as 12.5% were obtained by lowering the growth temperature. X-ray diffraction results showed no obvious secondary phase, which means that the phase separation can be suppressed by the growth at low temperatures. All samples, including those grown at room temperature, showed ferromagnetic characteristics. Photoluminescence emission was observed, though spectra exhibit broad and sharp luminescence bands related to many kinds of defects. It is suggested that electrons coming from defects, especially, nitrogen vacancy, stabilize ferromagnetism, and that the carrier-induced ferromagnetism occurs in the low-temperature-growth GaGdN.     

牵引一制动型液力变矩器原始特性研究

 基于束流理论建立了牵引一制动型液力变矩器原始特性参数计算数学模型．对以D430型液力变矩器为原
型设计的牵引一制动型液力变矩器进行了原始特性参数计算，并将计算结果同D430型液力变矩器原始特性参数进
行了比较分析，结论合理． 对设计牵引一制动型液力变矩器具有一定的指导意义．     

新型水力泵排液工艺

酸化或压裂是改造油气层措施中常规的也是最有效的方法之一。问题是酸化或压裂结束后,采取何种工艺及时返排出残酸,减少残液二次沉淀对油层的污染。同时常规TCP(油管传输负压射孔)+DST(地层测试器)二联作测试工艺在遇到低压、低渗等非自喷油层时,要想取准油层产能、压力,收集到有代表性产液样品资料,困难很大。针对以上问题,大港油田钻采院研制了新型水力喷射泵,该泵可与酸化、压裂及射孔+测试等工艺配套使用,在实现一趟施工管柱同时完成几项工作的同时,利用喷射泵深抽、连续强排的技术特点,取得了较好效果。     

三种套管接头抗压缩性能研究

针对套管接头抗压缩强度问题，使用全尺寸实物试验的方法对几种不同钢级、不同螺纹形式的套管接头的抗压缩强度进行了对比试验，并借助材料力学和有限元方法对试验结果进行了分析。实物试验中出现了管体失稳和接箍跳扣两种套管接头压缩失效形式。试验结果和分析结果表明，N80、P110钢级材料的压缩屈服强度高于拉伸屈服强度；偏梯形螺纹套管接头的压缩屈服强度比同钢级、同壁厚特殊扣螺纹套管接头低6.7%～7.7%；上扣是否到位，直接影响套管接头部分的抗压缩能力，上扣不到位的特殊螺纹套管接头的抗压缩性能甚至低于偏梯形螺纹接头。同时指出，为了保证上扣质量，不应使用浮动上扣方法，管柱设计中应进行抗压缩强度设计。     

香豆胶衍生物的化学结构及稳定性研究

将市售商品溶于水,用异丙醇沉析提纯,溶于0.1 mol/L NaNO3纯水溶液中,经0.5μm滤膜过滤后用水相凝胶渗透色谱法(GPC)测定,测得香豆胶(FG)、羟丙基香豆胶(HPFG)、阳离子香豆胶(CFG)的数均、重均相对分子质量Mn、Mw分别为:1.19×105、3.36×105,8.52×104、2.85×105,9.33×104、2.87×105。用甘露聚糖链在碱性条件下醚化时发生降解,解释两种改性FG的相对分子质量较FG低而多分散性(Mw/Mn)较FG高的测试结果。认为商品FG的1%水溶液黏度(1300 mPa.s)高于商品HPFG和CFG(分别为705和610 mPa.s)的原因是前者相对分子质量较高且残渣含量也较高(~10%,后二者为1%~2%)。HPFG的取代度为0.12,根据文献发表的13C-NMR数据确认HPFG分子链上羟丙基取代位置为C6。讨论了香豆胶(半乳甘露聚糖)的化学结构。热重分析法测定的热稳定性,HPFG高于CFG,CFG又高于FG。图6表3参13。     

红外多元探测器的噪声仿真研究

分析了红外多元探测器的噪声来源，建立各种噪声的公式。并以“L”型探测器为例分析其噪声的信号形式有三种：白噪声、正弦噪声、分形噪声。采用MATLAB语言对分析结果进行了仿真。     

UV法测定聚甲基丙烯酸酯纳米粒中胰岛素的包封率

建立一种简便易行的测定聚甲基丙烯酸酯胰岛素纳米粒中游离胰岛素含量方法.用Nanosep OD100C33超滤膜分离纳米粒和游离药物,在276 nm处测定药物的吸光度,建立胰岛素含量测定方法,并对线性、回收率、精密度等指标进行考察,最后测定各种胰岛素和载体比例混合的纳米粒的包封率.结果发现,该超滤膜能较好地分离纳米粒和游离的药物,在0.11～1.10 u/mL范围内,药物在276 nm的吸光度和浓度存在良好的线性关系(r=0.999 8),线性方程为A=0.868 8C-0.001 6,高、中、低3种浓度的回收率和精密度良好.该方法操作简单、结果可靠,可用于胰岛素纳米粒中药物包封率的测定.