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The effects of functionalized multi‐walled carbon nanotubes (MWCNTs) on thermal and chemorheological behaviors of an epoxy‐based nanocomposite system were investigated. Chemical functionalization of MWCNTs by acid modification (A‐MWCNTs) and chemical amidation (D‐MWCNTs) was confirmed using Fourier transform infrared spectroscopy and thermogravimetric analysis. It was found that the D‐MWCNTs had a significant effect on the chemorheological behaviors of the epoxy‐based nanocomposite. Compared to the epoxy/A‐MWCNT nanocomposite, the epoxy/D‐MWCNTs nanocomposite showed a significant increase in gel time, as obtained from isothermal rheology measurements. Also, the storage modulus of the diglycidylether of bisphenol F (DGEBF)/D‐MWCNTs nanocomposite was higher than that of the DGEBF/D‐MWCNTs nanocomposite and gradually increased with an increase of frequency. This could be interpreted by the relatively strongly interconnected structure of the D‐MWCNTs in the DGEBF epoxy resin, which arises from the functionalized alkyl groups of the D‐MWCNTs in dispersion phases with the DGEBF epoxy resin. Copyright © 2012 Society of Chemical Industry 相似文献
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Bombi Lee Jinhee Park Sunoh Kwon Mijung Yeom Bongjun Sur Insop Shim Hyejung Lee Suk Hoo Yoon Dong-Myong Jeong Dae-Hyun Hahm 《Food science and biotechnology》2012,21(3):723-729
The aim of this study was to investigate the effects of sowthistle (Ixeris dentata, IXD) on development and expression of nicotine-induced locomotor sensitization and underlying neuronal activation reflected by c-Fos expression in rats. Rats were pretreated with IXD 30 min before a daily injection of nicotine during an 8-day development phase and then challenged with nicotine after a 6-day withdrawal period. In another set of experiments, same IXD doses were administered once 30 min before nicotine challenge. Daily IXD treatment during development phase was not effective in blocking nicotine-induced locomotor sensitization in rats. However, a single IXD treatment after the development and withdrawal periods of nicotine sensitization significantly alleviated sensitized locomotor behavior on day 15. These behavioral results were coincident with significant inhibition of nicotineinduced c-Fos expression in the nucleus accumbens. These results indicated that IXD pretreatment significantly blocked the expression, but not the development of nicotine-induced locomotor sensitization in rats. 相似文献
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ABSTRACT: A vacuum-sealed miniature X-ray tube based on a carbon nanotube field-emission electron source has been demonstrated. The diameter of the X-ray tube is 10 mm; the total length of the tube is 50 mm, and no external vacuum pump is required for the operation. The maximum tube voltage reaches up to 70 kV, and the X-ray tube generates intense X-rays with the air kerma strength of 108 Gy * cm2 min1. In addition, X-rays produced from the miniature X-ray tube have a comparatively uniform spatial dose distribution. 相似文献
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This study investigates the (de)mobilizing influences of political (dis)agreement in the news and in political discussion on political attitudes and participation in new information environments. Results demonstrate the mediating functions of political ambivalence in that exposure to proattitudinal news reduces ambivalence and thereby promotes political participation, whereas exposure to counter-attitudinal news increases ambivalence and thereby discourages participation. Importantly, the effect of exposure to counter-attitudinal news on ambivalence was moderated by heterogeneous discussion networks on social network sites, such that the combination of exposure to counter-attitudinal news and to heterogeneous discussion networks amplifies ambivalence additively, and thereby augments the tendency toward demobilization. These results are interpreted as suggesting that changing media contexts may lead to complex roles of news and political discussion. 相似文献
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This paper investigates the spalling properties of high-strength concrete in order to improve the residual compressive strength and spalling resistance in specimens subjected to 3 h of unloading fire conditions. This study consists of three series of experiments with eighteen different specimens varying in fiber type and content, finishing material and simultaneous fiber content and lateral confinement. They were fabricated to a 300 × 300 × 600 mm mock-up size. Results of the fire test showed that the control concrete was explosive, while the specimens that contained more than 0.1 vol% of polypropylene (PP) and polyvinylalcohol (PVA) fibers were prevented from spalling. One specimen, finished by a fire endurance spray, exhibited even more severe spalling than the control concrete. The specimen containing 0.1 vol% of PP fiber and using a confining metal fabric at the same time, showed the most effective spalling resistance; in particular, the residual compressive strength ratio was even higher than that of the control concrete before the fire test. It was demonstrated that adding fibers in concrete prevented the spalling occurrence and confining metal fabric around the main bars of concrete specimens can secure the strength of structures during the conditions of elevated temperature. 相似文献
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Kyeong‐Yong Park Jinyong Lee Seong Jun Park Jung‐Nyoung Heo Hwan Jung Lim 《Advanced Synthesis \u0026amp; Catalysis》2015,357(18):3917-3926
A series of 1,2‐ and 1,4‐dihydroquinolines has been successfully prepared. The Pd‐catalyzed intramolecular N‐arylation of Z‐enamines, formally prepared by the Horner–Wadsworth–Emmons olefination, proceeded efficiently to furnish the cyclized products. Depending on the cyclization conditions, substituted 1,4‐dihydroquinolines and further isomerized 1,2‐dihydroquinolines were independently obtained in high yields with an excellent control of isomerization of the double bond.