Effect of constraint on fracture behavior of welded 17mn4 and aisi304 steels

In this study, 17Mn4 (P295GH) pressure vessels steel and AISI304 stainless steel were welded with ER309L austenitic consumable. In experimental part of the study, tensile tests were conducted on welded plates and variation of hardness values along specimen was measured. J-integral fracture toughness values were investigated for different crack locations. In order to determine the regions where plastic deformation did not take place due to constraint, uni-axial tensile test was performed on welded tensile specimen after attaching strain gauges. In numerical part of the study, finite element (FE) analyses were conducted by fixing 2-D models precracked on different locations by using ANSYS software. In these models, stress triaxiality and plastic deformation characteristics around crack tip were determined for each crack locations after stress — strain analyses. The limitation on the extension of plastic deformation at diffusion line causes extra increase in stress triaxiality at crack tip.     

Automated verification of access control policies using a SAT solver

Managing access control policies in modern computer systems can be challenging and error-prone. Combining multiple disparate access policies can introduce unintended consequences. In this paper, we present a formal model for specifying access to resources, a model that encompasses the semantics of the xacml access control language. From this model we define several ordering relations on access control policies that can be used to automatically verify properties of the policies. We present a tool for automatically verifying these properties by translating these ordering relations to Boolean satisfiability problems and then applying a sat solver. Our experimental results demonstrate that automated verification of xacml policies is feasible using this approach. This work is supported by NSF grants CCF-0614002 and CCF-0716095.     

Kinetics and equilibrium studies for the adsorption of Acid Red 57 from aqueous solutions onto calcined-alunite

The adsorption of Acid Red 57 (AR57) onto calcined-alunite was examined in aqueous solution in a batch system with respect to contact time, pH and temperature. The first-order, pseudo-second-order kinetic and the intraparticle diffusion models were used to describe the kinetic data and the rate constants were evaluated. The experimental data fitted very well the pseudo-second-order kinetic model and also followed the intraparticle diffusion model up to 90 min. The Langmuir and Freundlich adsorption models were applied to describe the equilibrium isotherms and the isotherm constants were also determined. The equilibrium data are successfully fitted to the Langmuir adsorption isotherm. The Langmuir isotherm constant, K(L), was used to evaluate the changes of free energy, enthalpy and entropy of adsorption for the adsorption of AR57 onto calcined-alunite. The results indicate that calcined-alunite could be employed as low-cost material for the removal of acid dyes from textile effluents.     

Level of intrinsic motivation of distance education students in e‐learning environments

According to researches, motivation that initiates and sustains behaviour is one of the most significant components of learning in any environment. Accordingly, level of intrinsic motivation triggers and sustains the interest of the open and distance education students when it comes to learning on their own in e‐learning environments. Despite a comprehensive literature regarding the motivation of those learning in traditional learning environments, the number of studies addressing the motivation of open and distance education students in e‐learning environments is not sufficient. In this context, this study aims at determining the level of intrinsic motivation of open and distance education students. Thus, data were collected from 1,639 distance education students in 22 programmes, through Intrinsic Motivation in e‐Learning Questionnaire developed and validated to that end. Analyses carried out indicate that the level of intrinsic motivation of open and distance education students is high in e‐learning environments, but there is not a statistically significant difference by gender, programme structure (graduate/undergraduate), instruction type (distance–blended), and academic disciplines.     

A Cost-Efficient and Simple Plant Oil DNA Extraction Protocol Optimized for DNA-Based Assessment of Product Authenticity

DNA-based assays offer precision in ascertaining the species/cultivar origin of agro-food products. Yet, obtaining DNA of sufficient quality and quantity is the main challenge while performing DNA-based food authentication analyses. The aim of the present work was to standardize a cost-efficient, easy-to-apply, yet effective plant oil DNA isolation protocol that allows reliable downstream PCR-based analyses. Because capillary electrophoresis (CE) separation of species/cultivar discriminating genomic fragments is a widely adopted approach in food genomics, a CE system was utilized in order to assess the performance of the proposed cetyl trimethyl ammonium bromide (CTAB)-based protocol. A plastid intergenic spacer and a nuclear olive gene were used as targets in order to evaluate the amplificability of DNA extracted with the CTAB-based protocol. The plastid barcode not only allowed assessing the reproducibility of PCR amplifications from the extracted oil DNA samples (olive, hazelnut, corn, rapeseed, cottonseed, and soybean oils) but also proved successful in discriminating all tested oil crop species based on amplified fragment length polymorphisms. Moreover, the barcode assay proved successful in correctly identifying the tested olive oil: cottonseed oil blends as admixtures of the two oil species. Thus, it was also feasible to demonstrate the potential of the barcode sequence as a discriminatory analyte to detect adulteration in plant oils. In addition, application of a CAPS (cleaved amplified polymorphic sequence) assay designed to genotype a nuclear SNP (single nucleotide polymorphism) marker resulted in the successful identification of the two single-cultivar olive oils included in the study. As a result of the present work, it was feasible to standardize a reliable and cost-efficient DNA extraction protocol that works well with both unrefined (olive and hazelnut) and refined (corn, rapeseed, cottonseed, and soybean) oils.     

Considerations about synchrophasors measurement in dynamic system conditions

This paper focuses on some concepts that are to be considered to ensure interoperability of phasor measurement units (PMU) during dynamic phenomena. Interoperability of devices in dynamic system conditions is needed to allow accurate analysis and, in the near future, control of phenomena like power system oscillations. The paper emphasizes the need to extend the IEEE standard to ensure the measurement latency and accuracy are known during field measurements. It also introduces a sequential logic aiming at providing the user with more robust measurements, together with more information about the measurement quality.     

Supercritical liquefaction of common reed (Phragmites australis) with alkali catalysts

Milled Phragmites australis was liquefied in organic solvents with and without catalyst in a cylindrical reactor at temperatures of 533, 553, and 573 K under supercritical conditions. The liquefied compounds were extracted with diethyl ether and benzene using an extraction procedure. The product yields without catalyst in supercritical methanol, ethanol, and acetone were found to be 55.4%, 64.4%, and 73.5% at 573 K respectively. The highest conversion to liquid products was obtained in supercritical acetone with 10% sodium hydroxide as catalyst at the same temperature in the catalytic runs. Main chemical compounds present in the liquid products obtained in ethanol without catalyst and acetone with sodium hydroxide catalyst at 573 K were analyzed and characterized by gas chromatography–mass spectrometry (GC-MS).     

Platelet‐to‐lymphocyte ratio better predicts inflammation than neutrophil‐to‐lymphocyte ratio in end‐stage renal disease patients

Neutrophil‐to‐lymphocyte ratio (NLR) was introduced as a potential marker to determine inflammation in end‐stage renal disease (ESRD) patients. Recently, platelet‐to‐lymphocyte ratio (PLR) and NLR were found to positively correlated with inflammatory markers including tumor necrosis factor‐α (TNF‐α) and interleukin (IL)‐6 in cardiac and noncardiac patients. Data regarding PLR and its association with inflammation are lacking in hemodialysis (HD) and peritoneal dialysis (PD) patients. Hence, we aimed to determine the relationship between PLR, NLR, and inflammation in ESRD patients. This was a cross‐sectional study involving 62 ESRD patients (29 females, 33 males; mean age, 49.6 ± 14.6 years) receiving PD or HD for ≥6 months in the Dialysis Unit of Necmettin Erbakan University. PLR, NLR, C‐reactive protein, TNF‐α, IL‐6 levels were measured. PLR, NLR, serum high sensitive C‐reactive protein, IL‐6, and TNF‐α levels were significantly higher in PD patients when compared with HD patients. ESRD patients with PLR ≥ 140 had significantly higher NLR, IL‐6, and TNF‐α levels when compared to patients with PLR < 139. In the bivariate correlation analysis, PLR was positively correlated with NLR, IL‐6, and TNF‐α in this population. When we compared the association of PLR and NLR with IL‐6 (r = 0.371, P = 0.003 vs. r = 0.263, P = 0.04, respectively) and TNF‐α (r = 0.334, P = 0.008 vs. r = 0.273, P = 0.032, respectively), PLR was found to be superior to NLR in terms of inflammation in ESRD patients. Simple calculation of PLR can predict inflammation better than NLR in ESRD patients.     

A note on histamine levels in Turkish style fermented sausages

The histamine contents of Turkish style fermented sausages were determined on 46 samples of five different brands obtained from retail stores in Van in Turkey. Histamine was found in all samples in the range 19.64-87.47 mg/kg (mean 32.13 mg/kg). Histamine levels in the brands differed significantly (P<0.01). The results suggest that the histamine levels in the sausages were not hazardous in terms of public health although they may be a potential risk to sensitive individuals.