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91.
Saikat Mandal Sujatha K. Arumugam Renu Pasricha Murali Sastry 《Bulletin of Materials Science》2005,28(5):503-510
In this paper, we describe the synthesis of silver nanocrystals within aqueous foams as a template. More specifically, we
show that aqueous Ag+ions may be electrostatically complexed with the anionic surfactants aerosol OT (sodiumbis-2-ethylhexyl-sulfosuccinate, (AOT) and sodium dodecyl sulphate (SDS)) in a highly stable liquid foam. After drainage of the
foam, the silver ions are reducedin
situby introducing sodium borohydride into the foam by capillary flow. This leads to the formation of silver nanoparticles of
spherical, tape-and sheet-like morphology in the foam. The structure of the foam is extremely complex and presents reaction
sites of different spatial extent. The differences in foam reaction-site geometry are believed to be responsible for the morphology
variation in the silver nanoparticles observed. The silver nanoparticles are observed to be extremely stable in solution suggesting
that the AOT or SDS molecules stabilize them. This approach appears promising for application in large-scale synthesis of
nanoparticles and may be readily extended to other chemical compositions. 相似文献
92.
Miniaturization in electronics and rapid advances in portable devices demand lightweight, compact, high-energy density batteries. Lithium batteries offer several advantages such as higher cell voltage, higher energy density, and longer shelf life as compared to other rechargeable systems. Although the rocking-chair concept of utilizing insertion compounds as both cathode and anode hosts has made the rechargeable lithium batteries a commercial reality, cost and environmental considerations require the development of inexpensive electrode hosts such as manganese oxides for consumer applications. Innovative synthesis and processing procedures (including low-temperature, solution-based synthesis approaches to obtain amorphous and nanocrystalline oxide electrode hosts) play a key role in developing new as well as better-performing known electrode materials. 相似文献
93.
Concentration of whey protein from cheese whey effluent using ultrafiltration by combination of hydrophilic metal oxides and hydrophobic polymer 下载免费PDF全文
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Arumugam Selva Sharma Shujat Ali Devaraj Sabarinathan Marimuthu Murugavelu Huanhuan Li Quansheng Chen 《Comprehensive Reviews in Food Science and Food Safety》2021,20(6):5765-5801
The versatile photophysicalproperties, high surface-to-volume ratio, superior photostability, higher biocompatibility, and availability of active sites make graphene quantum dots (GQDs) an ideal candidate for applications in sensing, bioimaging, photocatalysis, energy storage, and flexible electronics. GQDs-based sensors involve luminescence sensors, electrochemical sensors, optical biosensors, electrochemical biosensors, and photoelectrochemical biosensors. Although plenty of sensing strategies have been developed using GQDs for biosensing and environmental applications, the use of GQDs-based fluorescence techniques remains unexplored or underutilized in the field of food science and technology. To the best of our knowledge, comprehensive review of the GQDs-based fluorescence sensing applications concerning food quality analysis has not yet been done. This review article focuses on the recent progress on the synthesis strategies, electronic properties, and fluorescence mechanisms of GQDs. The various GQDs-based fluorescence detection strategies involving Förster resonance energy transfer- or inner filter effect-driven fluorescence turn-on and turn-off response mechanisms toward trace-level detection of toxic metal ions, toxic adulterants, and banned chemical substances in foodstuffs are summarized. The challenges associated with the pretreatment steps of complex food matrices and prospects and challenges associated with the GQDs-based fluorescent probes are discussed. This review could serve as a precedent for further advancement in interdisciplinary research involving the development of versatile GQDs-based fluorescent probes toward food science and technology applications. 相似文献
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99.
V. Arumugam S. Barath Kumar A. Joseph Stanley 《Russian Journal of Nondestructive Testing》2011,47(12):858-864
Acoustic emission is one of the powerful techniques that can be used for in situ structural health monitoring of composite
laminates. One of the main issues of AE is to characterize the different damage mechanisms from the detected AE signals. Unsupervised
Pattern recognition has been one of the techniques used for the identification of a specific failure mode in composites from
Acoustic emission data. Cross ply composite laminate of size 300 × 300 mm is fabricated using Vacuum bag molding. ASTM D3039
Standard tensile specimens are cut from the laminate and these specimens are subjected to uni axial tensile test under Acoustic
Emission monitoring. Fast Fourier transform analysis (FFT) and Short Time Fast Fourier Transform (STFFT) analysis are performed on the Wave forms of the AE hit data obtained during the conduct of tensile test to characterize
the failure modes in crossply specimens. Fast Fourier Transform enabled calculating the frequency content of each damage mechanism.
In this paper Fuzzy C Mean clustering is performed for the AE parameters obtained from the test and the efficiency of this
technique is being investigated using FFT AND STFFT analysis. 相似文献
100.
The electrochemical performances of Nd0.6Sr0.4Co0.5Fe0.5O3−δ–Ag composite cathodes have been investigated in intermediate temperature solid oxide fuel cells. The Nd0.6Sr0.4Co0.5Fe0.5O3−δ–Ag cathodes prepared by ball milling followed by firing at 920 °C show the maximum performance (power density: 0.15 W cm−2 at 800 °C) at 3 wt.% Ag. On the other hand, the Nd0.6Sr0.4Co0.5Fe0.5O3−δ–Ag composite cathodes with 0.1 mg cm−2 (0.5 wt.%) Ag that were prepared by an impregnation of Ag into Nd0.6Sr0.4Co0.5Fe0.5O3−δ followed by firing at 700 °C (but the electrolyte–Nd0.6Sr0.4Co0.5Fe0.5O3−δ assembly was prepared first by firing at 1100 °C) exhibit much better performance (power density: 0.27 W cm−2 at 800 °C) than the composite cathodes prepared by ball milling, despite a much smaller amount of Ag due to a better dispersion and an enhanced adhesion. AC impedance analysis indicates that the Ag catalysts dispersed in the porous Nd0.6Sr0.4Co0.5Fe0.5O3−δ cathode reduce the ohmic and the polarization resistances due to an increased electronic conductivity and enhanced electrocatalytic activity. 相似文献