交流变频钻井泵试验台的研制

针对大功率、超高压（52MPa）钻井泵的试验问题，设计了采用交流变频控制技术，提高试验能力的试验台架。该试验台架体现了实用性、可操作性、高效节能、环保性；电气传动部分采用具有国际先进水平、成熟技术的交流变频调速系统，实现无级调速；机械传动部分采用单级双速变速箱，试验范围广；电控系统可完成对钻井泵各种参数在线监控和测定。     

担载型含稀土三组份体系在二氧化碳甲烷化反应中的催化性能

用浸渍法制备了一系列氧化锆担载的含稀土Ⅷ族金属催化剂，对其在二氧化碳甲烷化过程中的催化活性作了研究，并用漫反射紫外可见光谱，ＦＴＩＲ等手段对催化剂作了表征。结果表明，含稀土新型催化剂具有催化活性高，目标产物选择性好等优点；稀土主要以氧化物形式存在于催化剂表面，参与对氢及表面含碳物种的吸附及活化；含稀土三组份催化剂的活性与所添加稀土三价离子的４ｆ电子数有关。     

Stability analysis and antiwindup design of uncertain discrete-time switched linear systems subject to actuator saturation

This paper investigates the stability analysis and antiwindup design problem for a class of discrete-time switched linear systems with time-varying norm-bounded uncertainties and saturating actuators by using the switched Lyapunov function approach.Supposing that a set of linear dynamic output controllers have been designed to stabilize the switched system without considering its input saturation,we design antiwindup compensation gains in order to enlarge the domain of attraction of the closed-loop system in the presence of saturation.Then,in terms of a sector condition,the antiwindup compensation gains which aim to maximize the estimation of domain of attraction of the closed-loop system are presented by solving a convex optimization problem with linear matrix inequality(LMI)constraints.A numerical example is given to demonstrate the effectiveness of the proposed design method.     

Preparation and properties of close-packed composite materials

Monodisperse silica particles of about 0.3m diameter are suspended in methacrylate monomer using a carefully selected dispersant. Many steric dispersants are hydrocarbon chains with a reactive end-group. These are not effective as dispersants for silica in moderately polar solvents, such as esters and the methacrylate monomers. Good dispersion was obtained with a methacrylate polymer terminated by a chlorosilane end group. Settling or centrifugation of these unagglomerated dispersions gives well-packed particle beds. Polymerization of the surrounding monomer produces composite materials with high packing fractions and a high degree of regularity. Moduli and strengths of these composites are reported.     

Adsorption characteristics of hexadecyl ammonium with different numbers of carbon chains in montmorillonite and the structure of the prepared composites

Journal of Porous Materials - The dynamics and thermodynamics of adsorption of hexadecyl ammonium with different numbers of carbon chains in montmorillonite (Mt) with different layer charge density...     

AN EXPERIMENTAL-NUMERICAL METHOD FOR MEASURING CRACK PROPAGATING VELOCITIES UNDER STRESS WAVE LOADING

An experimental-numerical method for measuring dynamic crack propagating velocities under stress wave loading is established in this paper. The experiments of the three-point bend specimen are done on the improved Hopkinson bar. Deflection of loading point, dynamic load and instantaneous crack length are measured, then crack propagating velocities are calculated. Experiments on 40Cr steel show that the results given by this method have a good agreement with that obtained by the resistance fracture gage method. Therefore this method is feasible for measuring crack propagating velocities under high loading rate and will have wide application.     

TiO2/MOFs的制备及污染物降解现状

TiO2是较为成熟的半导体光催化材料,但因TiO2分散性差、量子利用率低、比表面积小、难回收等问题难以工业化.多孔金属有机框架(MOFs)的引入可增强TiO2/MOFs复合材料的光吸收性能,提高电子-空穴对分离效率和提高回收率.基于TiO2/MOFs制备时前驱体添加顺序不同,综述了TiO2/MOFs的3种制备方法(即Ship-in-a-bottle法、Bottle-around-ship法、One-pot法)及TiO2/MOFs光催化机理与性能影响因素,并探讨不同MOFs与TiO2结合的作用机理.最后,对TiO2/MOFs存在的问题提出建议.