In this article, we deal with sparse high-dimensional multivariate regression models. The models distinguish themselves from ordinary multivariate regression models in two aspects: (1) the dimension of the response vector and the number of covariates diverge to infinity; (2) the nonzero entries of the coefficient matrix and the precision matrix are sparse. We develop a two-stage sequential conditional selection (TSCS) approach to the identification and estimation of the nonzeros of the coefficient matrix and the precision matrix. It is established that the TSCS is selection consistent for the identification of the nonzeros of both the coefficient matrix and the precision matrix. Simulation studies are carried out to compare TSCS with the existing state-of-the-art methods, which demonstrates that the TSCS approach outperforms the existing methods. As an illustration, the TSCS approach is also applied to a real dataset.
The effect of cerium addition on the catalytic performance of propane dehydrogenation over PtSnNa/ZSM-5 catalyst has been investigated by reaction tests and some physicochemical characterization such as XRD,BET,TEM,XPS,NH 3-TPD,H 2 chemisorption,TPR and TPO techniques.It has been found that with suitable amount of cerium addition,the platinum dispersion increased,while the carbon deposition tended to be eliminated easily.In these cases,the presence of cerium could not only realize the better distribution of metallic particles on the support,but also strengthen the interactions between Sn species and the support.Additionally,XPS spectra confirmed that more amounts of tin could exist in oxidized form,which was advantageous to the reaction.In our experiments,PtSnNaCe(1.1 wt%)/ZSM-5 catalyst exhibited the best catalytic performance.After running the reaction for 750 h,propane conversion was maintained higher than 30% with the corresponding selectivity to propylene of about 97%. 相似文献
In this paper, we study the second‐order perturbed Hamiltonian systems where is a parameter, is positive definite for all but unnecessarily uniformly positive definite for , and W is either asymptotically quadratic or superquadratic in x as . Based on variational methods, we prove the existence of at least two nontrivial homoclinic solutions for the above system when small enough. 相似文献
Supergiant vesicles are useful for investigating the interactions between lipid memebranes and collodial particles or macromolecules. Producing supergiant vesicles using the electroformation method lead to extraordinary findings in this work. The glyoxylic acid modified aluminum (GA-Al) electrode was prepared by the electro-reduction in an oxalic acid solution. High yield of supergiant vesicles with diameters >100 µm are successfully formed on a GA-Al electrode under an alternative current (AC) electric field. In contrast to platinum and indium tin oxide, which have been mainly used so far, this GA-Al electrode is preferable for the electroformation of egg phosphatidylcholine (EggPC) supergiant vesicles. 相似文献
A dispersive liquid–liquid microextraction procedure coupled with GC‐MS is described for preconcentration and determination of banned aromatic amines from textile samples. Experimental conditions affecting the microextraction procedure were optimized. A mixture of 30 μL chlorobenzene (extraction solvent) and 800 μL ACN (disperser solvent), 5 min extraction time, and 5 mL aqueous sample volume were chosen for the best extraction efficiency by the proposed procedure. Satisfactory linearity (with correlation coefficients >0.9962) and repeatability (<9.78%) were obtained for all 20 aromatic amines; detection limits attained were much lower than the standardized liquid–liquid method. The proposed method has advantages of being quicker and easier to operate, and lower consumption of organic solvent. 相似文献
A cooperative thermal decomposition route to large-scaled star-shaped α-MnS nanocrystals, which show novel magnetic properties, i.e., a high blocking temperature (275 K) and a large coercive field (1573 Oe), is reported. 相似文献