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杜仲药材有效成分与环境因子的灰色关联度分析 总被引:2,自引:2,他引:2
目的: 运用灰色关联度法分析影响杜仲皮和叶中4种有效成分含量产地差异性的主要环境因子. 方法: 利用HPLC同时测定10个产地10年生杜仲皮和叶中桃叶珊瑚苷、京尼平苷酸、绿原酸、松脂醇二葡萄糖苷的含量,流动相分别为乙腈(A)-0.1%磷酸水(B)梯度洗脱(0~25 min,5%~13%A;25~45 min,13%~15%A;45~80 min,15%~21%A),流动相乙腈(A)-0.1%磷酸水(B)梯度洗脱(0~20 min,5%~12%A;20~35 min,12%~13%A;35~45 min,13%~19%A;45~65 min,19%~25%A),检测波长均为210 nm.检测杜仲生长地土壤的全氮、全磷、全钾、碱解氮、速效磷、速效钾、有机质及pH,获得土壤因子数据,运用灰色关联度法对4种有效成分与气候及土壤因子的相关性进行分析. 结果: 10个产地同一生长年限杜仲皮、叶中4种有效成分的含量存在较大差异.碱解氮、速效钾、有机质、年平均相对湿度、年平均最高气温对4种成分在杜仲不同组织中的影响较大. 结论: 杜仲不同组织部位中4种有效成分含量与环境因子的灰色关联度分析明确了主导环境因子,为合理施肥及环境调控来提高杜仲次生代谢产物的含量提供参考,为杜仲的适宜种植区选择及其道地性产生原因分析提供实验依据. 相似文献
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菖蒲挥发油及其主要成分动态变化的研究 总被引:3,自引:1,他引:2
对东北产菖蒲的根、根茎及叶三部分挥发油及挥发油的主要成分的含量随季节、产地的变化情况进行了考察。结果表明:6月份为菖蒲的最佳采收季节;不同产地相同药用部位挥发油的主要成分化学结构类型相同。 相似文献
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环境生态因子对药用植物皂苷成分的影响 总被引:2,自引:1,他引:1
分析药用植物生长过程中主要的环境因子对药用植物皂苷成分的影响.分别从药材产地、药材采收期、光照和温度、栽培措施几个方面举例分析各个环境因子对药用植物皂苷成分的影响,分析其中的机制,寻找相关因子对药用植物皂苷成分影响的理论依据.药用植物产地、采收季节、生长年限、生长过程中的光照和温度及其栽培中的水肥管理等因素对药用植物皂苷成分都产生了很大的影响,这些现象具有一定的理论依据.优质药材的生产需考虑其栽培适宜区,确定合理的采收时间,同时在栽培过程中科学的栽培措施是提高药材产量和有效成分含量的有效手段.对药用植物采取适当的短期胁迫是优化栽培条件,提高药材质量的好方法. 相似文献
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《江西中医药》2015,(8)
目的:比较不同产地、不同采收期枫香树叶中异槲皮苷和山奈酚-3-O-芸香糖苷的含量。方法:采收相同产地下不同采收期和相同采收期下不同产地的枫香树叶,称重、晒干,并用HPLC法测定异槲皮苷和山奈酚-3-O-芸香糖苷的含量。结果:24批枫香树叶,同一采收期中江西余江、江西鹰潭、江西弋阳三个产地的枫香树叶异槲皮苷和山奈酚-3-O-芸香糖苷的总含量均较高;同一产地的8个采收期中,以5,6,7月份采收的枫香树叶异槲皮苷和山奈酚-3-O-芸香糖苷的总含量较高,12月份采收的异槲皮苷和山奈酚-3-O-芸香糖苷的总含量最低。结论:不同产地、不同采收期枫香树叶中异槲皮苷和山奈酚-3-O-芸香糖苷的含量存在明显差异,应注意生长环境和采收季节对枫香树叶药材质量的影响。 相似文献
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目的建立了飞龙掌血Toddalia asiatica根皮、茎皮高效液相色谱法指纹图谱,并运用相似度评价软件对指纹图谱进行相似度对比,从而为促进飞龙掌血综合利用提供理论依据。方法采用乙腈-0.1%磷酸水溶液梯度系统,C18柱(200mm×4.6 mm,5μm)色谱柱,测定波长269 nm,体积流量1.0 m L/min。通过对10批不同产地不同季节采收的飞龙掌血根皮与10批不同产地不同季节的茎皮对比研究,从而建立飞龙掌血的指纹图谱,并计算相似度。结果不同产地及不同季节采集的飞龙掌血根皮与茎皮共有峰的相对保留时间相对一致,但相对峰面积差异较大,说明产地和采收季节的不同会导致相关物质活性成分的量有一定的差异。结论飞龙掌血根皮与茎皮指纹图谱相似度大于0.9,其组成高度相似。 相似文献
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目的建立微波消解-电感耦合等离子体质谱(ICP-MS)直接稀释测定脉络宁注射液中25种矿物质元素(Mg、Ca、Fe、Cu、Zn、Mn、Al、B、Ba、Co、Cr、K、Li、Mo、Na、Ni、P、Pb、Sr、Th、Ti、V、As、Cd和Hg)的方法。方法分别对微波消解条件和测试条件进行考察;样品经微波消解后,采用电感耦合质谱仪测定25种矿物质元素,并对测定方法学进行考察。结果确定最佳消解条件为3步缓慢升温:400 W 80℃升温10 min,保留5 min;600 W 120℃升温10 min,保留5 min;900 W 200℃升温20 min,保留20 min;25种矿物质元素在各自的线性范围内线性关系良好,r≥0.999 6,精密度、稳定性和重复性试验的RSD均符合定量分析要求;加标回收率为94.7%~106.1%,RSD在0.34%~2.79%。脉络宁注射液中检测出Mg、Ca、Fe、Cu、Zn、Mn、Al、B、Ba、Co、Cr、K、Li、Mo、Na、Ni、P、Pb、Sr、Th、Ti、V,未检出As、Cd和Hg。结论该方法简便、迅速、准确,适用于脉络宁注射液中25种矿物质元素的同时测定。 相似文献
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O. Mastalier 《Deutsche Zeitschrift für Akupunktur (in deutscher Sprache / in German)》2013,56(4):26-29
The disturbance and instability of laterality are obstacles to diagnostics and therapy. Correction prior to starting therapy is required. They also predispose toward defined health problems and unspecific diseases. Numerous research activities provide evidence of the relevance of undisturbed laterality in diagnostics and therapy. Techniques of testing and therapeutic corrections will allow for optimized therapy success. 相似文献
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Chen Han-ping 《针灸推拿医学(英文版)》2014,(5):I0003-I0004
The Journal of Acupuncture and Tuina Science, a journal with an international scope (IS SN 1672-3597, CN 31-1908/R, Bimonthly), is embodied by 'Springer Verlag' Database, Index Copernicus (IC) and Chinese Scientific and Technical Paper and Citations Data (CSTPCD). You can search full text on http://www, springerlink, com/content/1672 -3597. 相似文献
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正Beverages based on Ilex paraguariensis A.St.-Hil.are used in the south Brazil and other Latin American countries located at the so-called southern cone.It is known as chimarro or mate in south and southeast Brazil,tererêin 相似文献
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This paper deals with an interdisciplinary study covering historic, botanical, phytochemical, pharmacological and clinical aspects of rhubarb and related species, to lay stress on the correlation between plant phylogeny, chemical constituents and purgative activity.
It was found that the official rhubarbs were exclusively restricted in the Sect. Palmata e.g. Rheum palmatum R. palmatum var. tanguticum R. officinale; the following criteria may serve as their standard, viz., the presence of sennoside derivatives and rhein, the occurrence of the reduced form of rhein and aloe-emodin, the leaves with any kind of palmate incision. Comprehensive multivariate analyses showed that there is a very close relationship between the leaf incision, existence of sennosides or rhein and purgative activity. 相似文献
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H. Brandt B. Hauswald H. Langer J. Gleditsch Th. Zahnert 《Deutsche Zeitschrift für Akupunktur (in deutscher Sprache / in German)》2008
Background
At present, the state-of-the-art medication in treating idiopathic taste disorder (gustatory dysfunction) is zinc. If zinc medication was unsuccessful, not tolerated or if it is contraindicated the persons affected can hardly be helped.Objectives
In a randomized placebo-controlled clinical trial an attempt was made to determine the efficacy of acupuncture.Methods
The treatment group was treated with acupuncture needles, the placebo group with an inactive acupuncture-laser. Endpoints of the study were changes in the taste test, the quality of life and the severity of symptoms of depression (BDI) as well as mood changes (ZMS). Satisfaction with the success of the respective therapy was also evaluated. Data were collected before and after therapy and again for the treatment group 10 weeks after completion of the treatment period.Findings
Treatment with real acupuncture showed a significant improvement in gustatory function as well as a significant improvement in psychological symptoms. Greater satisfaction with the treatment results was evident in the treatment group. The treatment results of acupuncture remained stable over a period of ten weeks after completion of the treatment.Conclusion
Acupuncture was effective in the therapy of idiopathic taste disorders and therefore it is an effective alternative when zinc medication is not tolerated or unsuccessful. But it is also suitable as a therapy of first choice. Acupuncture can be considered as an extension of the therapeutic spectrum in the difficult treatment of taste disorders. 相似文献18.
Background
Experimental and clinical studies postulate a neurobiological mechanism of acupuncture by modulating central pain systems, neurohormones and -transmitters. It seems to be quite likely that the autonomic nervous system (ANS) plays an important mediating role in this neuromodulation.Aim
In measuring heart rate variability (HRV), as a non-invasive approach to the ANS-function, the object of this study was to monitor probable acupuncture-induced changes of autonomic balance. The innovative technology of laser-needle acupuncture offers for the first time a stimulation method which fulfils the demands on a placebo-controlled acupuncture trial not requiring controversial sham acupuncture.Method
19 healthy voluntary subjects underwent 3 treatments in randomized sequence, consisting of placebo-, 1-point- (PC 6) and simultaneous 3-point- (PC 6, LR 3, SI 3) laser-needle-stimulation over 20 minutes. Before, during and after placebo-/verum laser-needle acupuncture, HRV-data for normalized HF(high frequency)- and LF(low frequency)-Power (nHF, nLF) and their quotient nLF/nHF obtained by power spectrum analysis (FFT), were measured and analyzed statistically at 5 different time points (ANOVA repeated measures, p < 0,05).Results
During both verum applications, the 1-point- (PC 6) as well as the simultaneous 3-point- (PC 6, LR 3, SI 3) laser-needle stimulation, significant changes of the ANS-activity were found in comparison to the placebo application. The most significant modification of HRV was an increase of nHF (p < 0,05 (PC 6), p < 0,0001 (PC 6, LR 3, SI 3)) as an expression of growing vagal activity during acupuncture.Conclusion
Laser-needle acupuncture causes in 1-point-stimulation (PC 6) as well as in simultaneous 3-point-stimulation (PC 6, LR 3, SI 3) significant changes in HRV in comparison to placebo application. HRV-monitoring seems to be a suitable approach in exploration of acupuncture-induced changes of ANS and could possibly be established in combination with laser needle acupuncture as a standard for further scientific and clinical acupuncture investigations which are greatly needed. 相似文献19.
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目的采用HPLC梯度洗脱法同时测定沉香化滞丸中沉香四醇、柚皮苷、橙皮苷、新橙皮苷、和厚朴酚、大黄素、厚朴酚、木香烃内酯、去氢木香内酯、大黄酚、大黄素甲醚11种成分。方法采用Thermo Syncronis C18色谱柱(250 mm×4.6 mm,5μm),流动相为水-乙腈,梯度洗脱:0~10 min,20%乙腈;10~20 min,20%~40%乙腈;20~24 min,40%乙腈;24~26 min,40%~52%乙腈;26~30 min,52%乙腈;30~31 min,52%~90%乙腈;31~35 min,90%乙腈;35~40 min,90%~100%乙腈;40~43min,100%乙腈;43~45min,100%~20%乙腈;检测波长215nm,体积流量1.0m L/min,柱温30℃,进样量20μL。结果各成分在43 min内分离良好,沉香四醇、柚皮苷、橙皮苷、新橙皮苷、和厚朴酚、大黄素、厚朴酚、木香烃内酯、去氢木香内酯、大黄酚、大黄素甲醚的线性范围分别为1.4~13.6、10.0~200.0、31.5~315.0、1.0~120.1、1.8~50.6、0.93~10.1、1.8~30.0、0.2~40.3、1.8~18.1、1.7~25.0、0.45~10.70μg/mL;样品中各成分的平均回收率均在98.90%~100.87%;11种成分精密度RSD在0.55%~1.54%;供试品溶液在30 h内稳定性良好,RSD在0.75%~1.94%;重复性RSD在0.39%~1.73%。6批次样品中沉香四醇、柚皮苷、橙皮苷、新橙皮苷、和厚朴酚、大黄素、厚朴酚、木香烃内酯、去氢木香内酯、大黄酚、大黄素甲醚质量分数分别为92.0~201.0、511.5~9 033.0、5 475.0~12 635.5、54.5~5 095.5、192.0~2 137.5、117.0~391.5、106.5~1 281.5、13.0~136.5、93.5~199.0、177.0~1 207.0、33.5~251.5μg/g。结论本方法准确、快速、简便,重复性好,精密度高,适用于沉香化滞丸中多种活性成分的定量分析。 相似文献