Effects of filler size,water, and alcohol on hardness and laboratory wear of dental composites

Three UEDMA/TEGDMA (50:50 by weight) based dental composites were made, each with filler loadings of 53 vol.%. The three composites contained silane‐treated filler particles with average particle diameters of 1.5, 3.0, or 10.0?μm. Twelve specimens per composite were mounted on wear wheels and run through 200,000 cycles in an ACTA wear machine. Six of these specimens per material were worn in slurries consisting of 30?g ground Millet seed shells and 120?g ground rice mixed with 275?mL water. The remaining six specimens were worn in similar 25% ethanol‐water slurries. The composite wear profiles were recorded with a profilometer and used to calculate the wear. Hardness values of the composites were also measured both before and after storage for 2 weeks in either water or in a 25% ethanol–water solution. The wear and hardness values from the measurements were analyzed using ANOVA. The wear analysis showed that the finer composites (1.5?μm filler diameter) wore the least and the coarsest composites (10?μm filler diameter) the most. The wear was significantly higher in the ethanol–water slurry than in the water slurry. The hardness value of the coarsest composite decreased more than the finest composite during storage in water or 25% ethanol–water. The hardness decrease was most pronounced in the alcohol solution.     

Three-body wear of dental resin composites reinforced with silica-fused whiskers.

OBJECTIVE: Recent studies used silica-fused whiskers to increase the strength and toughness of resin composites. This study investigated the three-body wear of whisker composites. It was hypothesized that the whisker composites would be more wear resistant than composites reinforced with fine glass particles, and the whisker-to-silica filler ratio would significantly affect wear. METHODS: Silica particles were mixed with silicon nitride whiskers at seven different whisker/(whisker + silica) mass fractions (%): 0, 16.7, 33.3, 50, 66.7, 83.3, and 100. Each mixture was heated at 800 degrees C to fuse the silica particles onto the whiskers. Each powder was then silanized and incorporated into a dental resin to make the wear specimens. A four-station wear machine was used with specimens immersed in a slurry containing polymethyl methacrylate beads, and a steel pin was loaded and rotated against the specimen at a maximum load of 76 N. RESULTS: Whisker-to-silica ratio had significant effects (one-way ANOVA; p < 0.001) on wear. After 4 x 10(5) wear cycles, the whisker composite at whisker/(whisker + silica) of 16.7% had a wear scar diameter (mean +/- sd; n = 6) of (643 +/- 39) microm and a wear depth of (82 +/- 19) microm, significantly less than a wear scar diameter of (1184 +/- 34) microm and a wear depth of (173 +/- 15) microm of a commercial prosthetic composite reinforced with fine glass particles (Tukey's multiple comparison). SEM examination revealed that, instead of whiskers protruding from the worn surface, the whiskers were worn with the composite surface, resulting in relatively smooth wear surfaces. SIGNIFICANCE: Silica-fused whisker reinforcement produced dental resin composites that exhibited high resistance to wear with smooth wear surfaces. These properties, together with the strength and fracture toughness being twice those of current glass particle-reinforced composites, may help extend the use of resin composite to large stress-bearing posterior restorations.     

Water and abrasive effects on three-body wear of composites.

The degrees of in vitro three-body wear resistance of a hybrid, a small-particle, and a microfilled composite were determined after water storage for up to 24 months. The hybrid composite was the most wear-resistant, while the microfilled composite showed the most wear. The hybrid composite showed no loss of wear resistance as a result of water storage. The small-particle composite showed a decrease in wear resistance after water storage only when tested with silicon carbide abrasive. The wear resistance of the microfilled composite decreased following water storage when tested with either a soft (CaCO3) or a hard (SiC) abrasive. For all composites, the soft abrasive was not capable of causing preferential wear of the polymer matrix, as observed on in vivo specimens. Instead, the filler particles became flattened, with minimal loss of interparticle substance. The hard abrasive did cause preferential wear of the matrix. All composites absorbed water and leached silicon during water storage, indicating that the filler-polymer bond was attacked by hydrolytic degradation. Scanning electron microscopic evaluation of the three-body wear specimens indicated that the in vitro wear method did not duplicate in vivo wear conditions (e.g., the hard abrasive caused excessive wear and chipping of the filler particles in vitro, a pattern that was not usually observed in vivo). Filler-polymer de-bonding was observed on in vivo specimens of all the composites, while it was found only on the in vitro microfilled composite specimens. These findings suggest that filler dislodging is a complex process that cannot be simulated with the in vitro wear method used in this study, not even after prolonged water storage.     

Effect of filler fraction and filler surface treatment on wear of microfilled composites.

OBJECTIVES: The aim of this study was to determine the effect of filler content and surface treatment on the wear of microfilled composites. METHODS: Four microfilled composites with different filler contents (A=20, B=25, C=30, and D=35 vol.%) were made with a light-cured resin (Bis-GMA/UDMA/TEGDMA). The surface treatment of the colloidal silica in each varied: F=functional silane, NF=non-functional silane, U=untreated. Silux Plus served as a control. Specimens were made in steel molds and cured in a light curing unit Triad II (40s/side). Abrasion and attrition wear were evaluated in vitro in a wear tester (OHSU oral wear simulator) with an abrasive slurry (poppy seeds + PMMA) and a human enamel antagonist. The average of five specimens was computed and compared using a ANOVA/Tukey's test at P < or = 0.05. The surface of the wear patterns and the distribution of filler particles were examined using a scanning electron microscope and digital imaging. RESULTS: As filler volume increased, wear was reduced regardless of filler treatment. Amounts of wear for specimens C and D were significantly lower than specimens A and B. Composites with functional silane treated microfiller (Group F) produced significantly less wear than those with non-functional microfiller (Group NF) at 30 and 35 vol.%, and less than the untreated microfiller (Group U) at 30 vol.%. Scanning electron microscopy of specimens of group NF showed large filler agglomerates (size > 1 microm) in the resin matrix, while specimens of group F and U showed fewer agglomerates. Digital imaging analysis revealed small filler clusters (size < or = 1 microm) in the resin matrix of all specimens. SIGNIFICANCE: Wear resistance of microfilled composites is enhanced by higher filler volumes irrespective of surface treatment, but good filler/matrix adhesion is needed to minimize wear.     

In vitro contact wear of dental composites.

OBJECTIVE: The aim of this study is to determine the in vitro two-body contact wear mechanisms of three medium filled composites and compare these with a highly filled composite previously investigated. MATERIALS AND METHODS: Three commercial dental composites with filler mass fraction loading of 75-76% were evaluated. Two of the composites contained Ba-B-Al-silicate glass fillers and fumed silica with different particle sizes and distributions. One of these composites contained a fairly uniform distribution of filler particles ranging in size from 1 to 5 microm, whereas the particle size distribution in the second composite was bimodal consisting of small (less than 1 microm) and large (about 10 microm) particles. The third composite contained Ba-Al-silicate glass and silica with a filler particle size of approximately 1 microm. The composite disks were tested for wear against harder alumina counterfaces. Wear tests were conducted in distilled water using a pin-on-disk tribometer under conditions that represented typical oral conditions (sliding speed of 2.5 mm/s and contact loads ranging from 1 to 20 N). The wear tracks were analyzed by scanning electron microscopy (SEM) and Fourier transform infrared (FTIR) spectroscopy to elucidate the wear mechanisms. The chemical composition of the water solution collected after the tests was determined using an inductively coupled plasma-mass spectrometer (ICP-MS) to detect possible chemical changes, e.g. dissolution of trace elements due to submersion or wear. The wear results were compared with those reported in an earlier study on a highly filled composite containing predominately alumino-silicate glass fillers and alumina at a filler loading of 92%. RESULTS: The differences in two-body wear rates between the three medium filled composites were not statistically significant (p<0.05) indicating that the variations in filler particle size and slight differences in chemical composition of the glass fillers do not affect the in vitro wear rates of these composites. Wear rates of these medium filled composites, however, were significantly lower than the highly filled composite (p<0.05). SEM, FTIR and ICP-MS analyses suggested that wear in the medium filled composites occurs by a complex set of processes involving tribochemical reactions between filler particles and water, formation of surface films containing a mixture of filler fragments and reaction products, and film delamination, as well as dissolution of the reaction products. SIGNIFICANCE: This study reveals that subtle changes in the filler particle size and small differences in filler composition do not significantly affect the two-body wear behavior of medium filled composites. However, the chemistry of filler particles plays an important role in altering the wear performance of composites when significant changes are made in the chemical composition of the fillers and when the filler loading is increased.     

The effect of a leucite-containing ceramic filler on the abrasive wear of dental composites.

OBJECTIVES: The aim of this study was to evaluate abrasive wear of a dental composite based on a leucite-containing (KAlSi2O2 ceramic filler, and to compare it with the wear of a composite based on commonly used aluminum barium silicate glass filler. METHODS: IPS Empress (Ivoclar-Vivadent) ingots were ball milled, passed through an 800 mesh (ASTM) sieve, and used as the leucite ceramic filler. Experimental composites were prepared by mixing the silane-treated fillers with the resin monomers. The resin consisted of 70 wt% Bis-GMA and 30 wt% TEGDMA containing camphorquinone and DMAEMA as the photoinitiator system. Glass-based composites were also prepared using silane-treated aluminum barium silicate glass fillers and the same resin system. TetricCeram, a commercially available dental composite, was used as control. Spherical specimens of the composites were then prepared and kept in water for 2 weeks to reach equilibrium with water. An abrasive wear test was performed using a device designed in our laboratory and weight loss of the specimens was measured as an abrasion parameter after each 50 h. SEMs were taken from worn and fractured surfaces. Degree-of-conversion of the composites was measured using FTIR spectroscopy. Vickers surface microhardness, flexural strength, and flexural modulus of the composites were also measured. The data were analyzed and compared using ANOVA and Tukey HSD tests (significance level=0.05). RESULTS: The results showed that there were significant differences among the abrasive wear of the composites (p<0.05). The ranking from least to most was as: leucite-based composite相似文献   

Chemical softening and wear of dental composites

The purpose of this work was to determine the influence of chemical food-simulating liquids on the wear of various commercial dental composite restoratives. In many cases, pre-conditioning the restoratives in these liquids for one week produced swelling of the polymer matrix and considerable surface damage. The resulting degradation reduced the hardness and enhanced the wear as measured by a pin-and-disc apparatus. Four kinds of commercial composites were investigated: a conventional quartz-filled, a strontium-glass-filled, a visible-light-activated, and a microfilled composite. The liquids employed were heptane and several aqueous solutions of ethanol with solubility parameters, delta, ranging from delta = 1.5 to 4.8 X 10(4) J1/2m-3/2. With all restoratives, the decline in hardness during pre-conditioning maximized at about delta = 3 X 10(4), which corresponds to a 75% ethanol solution. The wear behavior was considerably more complicated and variable, as discussed in the text. For the most part, the increase in wear rate from pre-conditioning corresponded to the fall in hardness. A notable exception was for the strontium-glass-filled composite pre-conditioned in pure water. Here the wear was enhanced considerably, with no decrease in hardness. In this case, the degradation mode is assumed to be different from the others in that it is attributed to stress corrosion of the glass filler.     

Curing light intensity effects on wear resistance of two resin composites

This in vitro study evaluated the wear resistance of resin composite polymerized using four different light-curing systems. For this, a well-defined cylindrical cavity preparation (4.0 mm in diameter x 3.0 mm in depth) was made in a ceramic block (n=4 per material/light condition). Uncured material, either a universal hybrid composite (Herculite XRV) or a flowable hybrid composite (Revolution Formula 2), was packed and light-cured from the top surface only with one of the four light-curing units: 1) a conventional quartz-tungsten-halogen light, 2) a soft-start light, 3) an argon-ion laser or 4) a plasma-arc curing light. After storing the specimens in deionized water at 37 degrees C for 24 hours, the excess cured material was ground through successive grits up to a final 1200-grit SiC abrasive. The specimens were placed in deionized water at 37 degrees C for an additional 24 hours. Wear simulation was performed using a four-station Leinfelder-type three-body wear device. A slurry of water and unplasticized polymethylmethacrylate beads, simulating an artificial food bolus, was placed on the surface of each resin-composite-restored ceramic block. The entire cycling procedure was carried out 400,000 times. Impressions of each resin composite surface were taken with polyvinylsiloxane and epoxy replicas were made. Wear analyses were conducted by generating tracings across the worn surface of epoxy replicas using profilometer scans. For the universal hybrid composite and the flowable hybrid composite, the lowest wear occurred in specimens that were cured using the conventional quartz-tungsten-halogen light, and the highest wear was detected on those specimens made using the argon-ion laser. For both resin composites, the mean wear for specimens cured using the argon-ion laser was significantly higher than that of the specimens cured with the three other lights, which were statistically similar.     

Influence of curing rate on softening in ethanol, degree of conversion, and wear of resin composite

PURPOSE: To investigate the effect of curing rate on softening in ethanol, degree of conversion, and wear of resin composites. METHOD: With a given energy density and for each of two different light-curing units (QTH or LED), the curing rate was reduced by modulating the curing mode. Thus, the irradiation of resin composite specimens (Filtek Z250, Tetric Ceram, Esthet-X) was performed in a continuous curing mode and in a pulse-delay curing mode. Wallace hardness was used to determine the softening of resin composite after storage in ethanol. Degree of conversion was determined by infrared spectroscopy (FTIR). Wear was assessed by a three-body test. Data were submitted to Levene's test, one and three-way ANOVA, and Tukey HSD test (alpha = 0.05). Results: Immersion in ethanol, curing mode, and material all had significant effects on Wallace hardness. After ethanol storage, resin composites exposed to the pulse-delay curing mode were softer than resin composites exposed to continuous cure (P< 0.0001). Tetric Ceram was the softest material followed by Esthet-X and Filtek Z250 (P< 0.001). Only the restorative material had a significant effect on degree of conversion (P< 0.001): Esthet-X had the lowest degree of conversion followed by Filtek Z250 and Tetric Ceram. Curing mode (P= 0.007) and material (P< 0.001) had significant effect on wear. Higher wear resulted from the pulse-delay curing mode when compared to continuous curing, and Filtek Z250 showed the lowest wear followed by Esthet-X and Tetric Ceram.     

Relative wear of flowable and highly filled composite

STATEMENT OF PROBLEM: By decreasing the proportion of filler, flowable composites are easy to adapt to small cavity preparations. However, the wear resistance of flowable composites is a clinical concern, as improved wear has been related to increased filler percentage. PURPOSE: The purpose of this study was to compare wear for flowable composites and comparable heavily filled materials. MATERIAL AND METHODS: Wear by attrition and abrasion (microm) of microfilled flowable (Heliomolar Flow) and heavily filled microfill (Heliomolar HB) was measured and compared to a microhybrid flowable (Tetric Flow) and a heavily filled microhybrid (Tetric HB). There were 5 specimens, 2 mm thick and 15 mm in diameter, in each group. The Oregon Health Sciences University oral wear simulator was used to produce abrasive wear and attrition for all specimens. Abrasion and attrition of the substrates were measured using a profilometer. Data were subjected to a 3-way analysis of variance for the 3 main factors: composite type, filler load, and wear type (alpha=.05) RESULTS: Composite wear rates were significantly influenced (P <.01) by both the type of wear and the filler amount. Abrasive wear occurred less than wear by attrition, and the heavily filled composites experienced less wear than the flowable composites. CONCLUSIONS: Results of this in vitro study suggest that highly filled microhybrid composites may have greater wear resistance for contact-supporting posterior restorations. However, in small noncontact restorations where longevity may be dictated by abrasion, flowable microfilled resins may be adequate.     

Effects of occlusal and brushing forces on wear of composite resins

Effects of occlusal and brushing forces on the wear of composite resins were investigated using three different wear tests: simulated occlusal wear test, toothbrush wear test, and combined wear test which carried out toothbrush wear test and occlusal wear test alternately. Test specimens were prepared from four commercial composite resins. Worn volume and maximum worn depth were measured under different occlusal forces (40 N and 80 N) and brushing forces (1.5 N and 3 N) in the three wear tests. Worn surfaces were observed using a SEM. In all the three wear tests, both higher occlusal and brushing forces resulted in significantly greater worn volume and higher maximum worn depth. The effects of occlusal force on worn volume and maximum worn depth varied with different composites, indicating that the four tested composites showed different wear behaviors under different occlusal forces and brushing forces. It was suggested that their different wear behaviors most probably stemmed from the differences in their filler systems.     

In Vitro Wear of Nano-Composite Denture Teeth

PURPOSE: Few laboratory tests have been able to substantiate and quantify the wear resistances of polymeric denture teeth. This study evaluated the relative wear resistance of several types of denture teeth using an in vitro wear testing device. MATERIAL AND METHODS: Four different types of denture teeth [nano-filled (Veracia) and micro-filled composites (SR-Orthosit, Endura, Duradent, Surpass), cross-linked acrylic (SR-Postaris, Genios-P, Creapearl, Vitapan Physiodens, Premium 8, Integral), and a conventional acrylic (Biotone)] were used. The flattened buccal surface of each denture tooth was subjected to the evaluation of Knoop hardness (n=5) and localized wear for 100,000 cycles (n=10). Wear values were determined in micrometers using a profilometer. The data for the hardness, wear depth, and worn surface areas were individually analyzed by one-way ANOVA. RESULTS: Knoop hardness values (KHN) ranged from 28.2 to 29.8 for micro-filled composite, 18.9 to 21.6 for cross-linked acrylic, 22.7 for nano-composite, and 18.6 for conventional acrylic teeth. All micro-filled composite teeth were significantly harder than other teeth (p <0.0001). The wear depth values were 90.5 microm for the nano-composite, 69.8 to 93.0 microm for the micro-filled composite, 80.8 to 104.0 microm for the cross-linked acrylic, and 162.5 microm for conventional acrylic teeth. The worn surface areas were 5.1 mm2 for the nano-composite, 2.6 to 3.6 mm2 for the micro-filled composite, 4.4 to 5.7 mm2 for the cross-linked acrylic, and 10.1 mm2 for conventional acrylic teeth. The wear values of the acrylic control were significantly different from all other denture teeth (p <0.001). CONCLUSION: The nano-composite tooth was harder and more wear resistant than the acrylic teeth but not significantly different from most of the cross-linked and micro-filled composite teeth tested.     

Wear and mechanical properties of composite resins consisting of different filler particles

To investigate the effects of different fillers and their contents on the wear of composite resins, four composites (CS: non-porous spherical silica, AS: porous spherical silica, AZ: porous spherical zirconium silicate, and IS: non-porous irregular-shaped silica) were experimentally prepared using different fillers (CS, AZ, AS and IS). Simulated occlusal wear and toothbrush wear were evaluated for these composites and their worn surfaces were observed. The mechanical properties (flexural strength, elastic modulus and hardness) of these composites were determined to examine the relationships between wear and these mechanical properties. CS showed the highest occlusal wear, but the lowest toothbrush wear among four composites. AS and AZ had lower occlusal wear than CS and IS, while their toothbrush wear was higher than CS and close to that of IS. All composites showed increase in the occlusal wear as filler content increased. CS and IS showed decrease in the toothbrush wear as the filler content increased, whereas AS and AZ did not. The occlusal wear surfaces of CS and IS had concavities, while those of AZ and AS were relatively smooth with flattened filler. The toothbrush wear surfaces of CS and IS revealed the extrusion of filler from resin matrix, whereas those of AZ and AS were smooth with flattened filler. The toothbrush wear of CS and IS decreased as the mechanical properties increased, whereas those of AS and AZ did not. The occlusal wear of all composites increased as the mechanical properties increased, which would not reflect effects of these mechanical properties.     

Hardness and fracture toughness of four commercial visible light-cured composite resin veneering materials

summary Four commercial visible light (VL)-cured composite resin veneering materials with a dentine shade were examined for their Knoop hardness and fracture toughness. Composite specimens were classified into three groups. The first group was cured by VL only, the second group was cured by VL and postcured by VL and the third group was cured by VL and post-cured by heat. It became evident that one composite containing four-functional urethane monomer had both hardness and fracture toughness greater than those of the other three composites containing two-functional urethane monomer. The filler content (vol%) in the composite tended to be linearly proportional to both hardness and fracture toughness. Post-curing by VL and heat were proven to effectively increase both hardness and fracture toughness of once light-cured composites. These results suggest that the clinical performance (e.g. wear resistance and colour stability) of VL-cured composite resin veneering materials might be improved with the aid of post-curing.     

Wear and mechanical properties of nano-silica-fused whisker composites

Resin composites must be improved if they are to overcome the high failure rates in large stress-bearing posterior restorations. This study aimed to improve wear resistance via nano-silica-fused whiskers. It was hypothesized that nano-silica-fused whiskers would significantly improve composite mechanical properties and wear resistance. Nano-silicas were fused onto whiskers and incorporated into a resin at mass fractions of 0%-74%. Fracture toughness (mean +/- SD; n = 6) was 2.92 +/- 0.14 MPa.m(1/2) for whisker composite with 74% fillers, higher than 1.13 +/- 0.19 MPa.m(1/2) for a prosthetic control, and 0.95 +/- 0.11 MPa.m(1/2) for an inlay/onlay control (Tukey's at 0.95). A whisker composite with 74% fillers had a wear depth of 77.7 +/- 6.9 mum, less than 118.0 +/- 23.8 microm of an inlay/onlay control, and 172.5 +/- 15.4 microm of a prosthetic control (p < 0.05). Linear correlations were established between wear and hardness, modulus, strength, and toughness, with R = 0.95-0.97. Novel nano-silica-fused whisker composites possessed high toughness and wear resistance with smooth worn surfaces, and may be useful in large stress-bearing restorations.     

Effects of three food-simulating liquids on the roughness and hardness of CAD/CAM polymer composites

ObjectiveImplant-supported frameworks constructed from high-performance polymer CAD/CAM composites are exposed to liquids from the oral environment and routine care maintenance. Therefore, this study investigated the effect of food-simulating liquids (FSLs) on surface properties of three CAD/CAM polymer composite blocks.MethodsThe composites investigated were (i) a carbon fibre-reinforced composite (CarboCAD 3D dream frame; CC), (ii) a glass fibre-reinforced composite (TRINIA; TR), and (iii) a reinforced PEEK (DentoKeep; PK). The filler contents were determined by thermo-gravimetry. The surface properties were roughness, Vickers hardness (HV), properties measured by Martens force/depth indentation, namely: hardness (HM), modulus (E_IT) and creep (C_IT). Property measurements were made at baseline on polished specimens and then, where possible, after 1- and 7-days storage at 37 ℃ in three different media: water, 70% ethanol/water and MEK (methyl ethyl ketone). Specimens were selected for light and scanning electron microscopy. Statistical analysis was performed by two-way repeated measures ANOVA, one-way ANOVA, and multiple comparison tests (α = 0.05).ResultsThe baseline roughness and hardness (HV, HM) and modulus (E_IT) correlated approximately with filler content (wt%), with the fibre-reinforced composites being rougher, harder and stiffer than PK. At baseline, roughness (Sa) ranged from 0.202 to 0.268 µm; HV from 23.1 to 36.9; HM from 224.5 to 330.6 N/mm²; E_IT: from 6 to 9.8 GPa. After ageing in 70% ethanol and MEK, more pronounced roughness and hardness changes were observed than in water. MEK caused greater deterioration for the FRC than 70% ethanol, while PK specimens showed slight changes in 70% ethanol.SignificanceStorage media adversely affected the surface and mechanical properties of each CAD/CAM composite. However, during ageing, the reinforced PEEK showed greater relative stability in these properties. Nevertheless, the deterioration may indicate the need for full protection by a veneer material on each surface of an implant-supported framework.     

8种复合树脂磨耗性能和硬度的研究

目的体外测定8种复合树脂的体积磨损量和硬度,评价其耐磨耗性能。方法选择Durafill VS、Filtek A110、Charisma、Ceram-X、Filtek Z350、FS-2、Filtek P60和Tetric Ceram HB 8种复合树脂,分别制备8mm×6mm×2mm的树脂片,并用自凝树脂包埋,测定表面硬度（维氏）。将试样固定在往复滑动球-片式磨耗试验机上,以萤石粉糊剂作为磨耗介质,磨耗3万次后用三维形貌扫描仪测定复合树脂表面磨痕的体积,统计学分析复合树脂的硬度与其体积磨损量的相关性及各个复合树脂体积间磨损量的差异,SEM观察分析磨损面。结果 8种复合树脂的硬度顺序为：P60≈Z350〉A110≈Tetric HB〉FS-2≈Ceram-X〉Charisma〉Durafill。Z350的磨损量最小（0.68±0.05）mm3,其次是P60（1.11±0.06）mm3,随后是Charisma（1.50±0.17）mm3、Durafill（1.64±0.49）mm3、FS-2（1.75±0.32）mm3及A110（1.84±0.37）mm3,Ceram-X（2.09±0.36）mm3和Tetric HB（2.56±0.48）mm3的磨损量较大。所测复合树脂的硬度与其体积磨损量之间无相关性（r=-0.55）。结论复合树脂的耐磨耗性能与其硬度无关,而与不同材料品牌关系密切。     

Chewing pressure vs. wear of composites and opposing enamel cusps.

The effects of various chewing pressures on the wear of composites and enamel were assessed in vitro. Standardized composite discs (8 mm in diameter, 2 mm in height) were made of a fine-particle hybrid (FPH), a coarse-particle hybrid (CPH), and a homogeneous microfilled composite (HMC). The composite specimens were chemically degraded by immersion in 75% ethanol for 24 h, brushed for 30 min, and then thermocycled 300 times (5-55-5 degrees C) while being occlusally loaded 120,000 times at 1.7 Hz, with chewing forces of 25, 50, 75, and 100 N. Standardized human enamel cusps with a uniform contact area of 0.384 mm2 served as antagonists in the chewing machine. Wear of the composites and enamel cusps, their combined wear, and the increase of the enamel contact surfaces were quantified. An increase in chewing pressure significantly enhanced the wear of both composite and enamel in all groups except for the antagonists opposing a HMC. The FPH was most wear-resistant to in vitro chewing pressures in the range of 6.58 to 19.74 MN/m2, the CPH at 26.32 MN/m2, while the HMC was the most enamel-friendly of the three composites tested. The FPH composite had the least disintegration in the occlusal contact area. The ranking of the composites generally varied at the different chewing pressures with respect to the three types of quantified wear--that is, composite wear, enamel wear, and total wear.     

Hardness and compressive strength of indirect composite resins: effects of immersion in distilled water

The aim of this study was to evaluate the effect of ageing in distilled water on the hardness and compressive strength of a direct composite resin Z100, a feldspatic porcelain (Noritake) and three indirect composites (Artglass, Solidex and Targis). For the Vickers hardness tests, five disk-shaped specimens (2 x 4 mm) of each material were prepared according to the manufacturers' instructions. The hardness tests were conducted using a Vickers diamond indentor. Compressive strength measurements were recorded on cylindrical specimens with a diameter of 6 mm and a length of 12 mm. The compression tests were carried out with a constant cross-head speed of 0.5 mm min(-1) on a mechanical test machine. For each material, 10 specimens were tested after 7 days of dry storage at 37 +/- 1 degrees C and 10 specimens were tested after water storage at 37 +/- 1 degrees C for 180 days. Noritake porcelain specimens showed higher hardness values than the composites. Among the composite materials, Z100 promoted the highest VHN values, regardless of the ageing periods. The results showed that Solidex and Z100 had the highest compressive strength values. Ageing in water reduced the hardness for all composites, but had no long-term effect on the compressive strength.