Fretting fatigue properties of plasma nitrided AISI 316 L stainless steel: Experiments and finite element analysis

This study investigates the effects of thickness, hardness and composition of modified layer on the plain and fretting fatigue properties of the nitrided 316 L steel plasma nitrided under various processing conditions. Fretting fatigue behaviour of untreated and nitrided material is also analysed with the finite element method. Experimental and theoretical fatigue life results are compared. The result indicates that the nitriding process improved the fretting fatigue properties of 316 L stainless steel. The experimental test results are close to theoretical fretting fatigue life results, thus it yields that the established model in the numerical analysis is consistent in this regard.     

The effect of fretting on the fatigue behaviour of plasma nitrided stainless steels

The plain fatigue and fretting fatigue behaviour of a plasma nitrided dual phase stainless steel known as 3CR12 and an AISI 316 austentic stainless steel have been studied in the present work, using a modified Wohler rotating-bending configuration. Test specimens were produced at two nitriding temperatures, namely 400 and 520 °C, representing low temperature and conventional nitriding temperature, respectively. The test results demonstrate that both nitriding processes can enhance the plain fatigue limit of these steels by approximately 10-25%, with the high temperature process being slightly more effective. Under fretting fatigue conditions, the beneficial effect of plasma nitriding is even more significant and the fretting fatigue limit is increased between 50 and 100% for 3CR12 and at least 50-150% for the AISI steel as the nitriding temperature is raised from 400 to 520 °C.     

An experimental study on bending fretting fatigue characteristics of 316L austenitic stainless steel

Bending fretting fatigue tests of 316L austenitic stainless steel plates against 52100 steel cylinders have been carried out under same normal load and varied bending loads. Tests of plain bending fatigue were carried out as a control group. The S-N curves of the bending fatigue were made. The results indicated that there was an obvious drop of life under the condition of bending fretting fatigue due to higher local contact stress. A dislocation model of micro-crack nucleation mechanism, as a manner of zig-zag mode, was created to explain the nucleation of fretting fatigue cracks.     

The effect of hydrogen gas environment on fretting fatigue strength of materials used for hydrogen utilization machines

The objective of this study is the characterization of the fretting fatigue strength in a hydrogen gas environment. The test materials were a low alloy steel SCM435H, super alloy A286 and two kinds of austenitic stainless steels, SUS304 and SUS316L. The test was performed in hydrogen gas at 0.12 MPa absolute pressure. The purity of the hydrogen gas was 99.9999%. The fretting fatigue limit was defined by the fretting fatigue strength at 30 million cycles. For all materials, the fretting fatigue strength in the hydrogen gas environment increased in the short-life region. However, the fretting fatigue strength in the hydrogen gas environment decreased in the long-life region when exceeding 10 million cycles except for SCM435H, while there was no reduction in the fretting fatigue strength in air between 10 and 30 million cycles. The reduction rate was 18% for A286, 24% for SUS304 and 7% for SUS316L. The tangential force coefficient in the hydrogen gas environment increased when compared to that in air. It can be estimated that this increase is one of the causes of the reduced fretting fatigue strength found in a hydrogen gas environment. In order to discuss the extension of the fretting fatigue life in hydrogen gas observed at the stress level above the fretting fatigue limit in air, continuous measurement of the fretting fatigue crack propagation was performed in a hydrogen gas environment using the direct current potential drop method. As a result, it was found that the extension of the fretting fatigue life was caused by the delay in the start of the stable crack propagation.     

Effect of Plasma Nitriding Environment and Time on Plain Fatigue and Fretting Fatigue Behavior of Ti–6Al–4V

Plasma nitriding was performed on Ti–6Al–4V fatigue test samples at 520°C in two environments (nitrogen and nitrogen–hydrogen mixture in a ratio of 3:1) for two time periods (4 and 18 h). Plain fatigue and fretting fatigue tests were conducted on unnitrided and plasma nitrided samples. Plasma nitriding degraded lives under both plain fatigue and fretting fatigue loadings. The samples nitrided in nitrogen exhibited superior lives compared with the samples nitrided in the nitrogen–hydrogen mixture, possibly due to the relatively higher hardness (and presumably lower toughness) of the nitrided layer of the samples nitrided in the nitrogen–hydrogen mixture environment. For those samples nitrided in the nitrogen–hydrogen mixture, those nitrided for 18 h exhibited superior lives compared with those nitrided for 4 h. This trend was observed for samples nitrided in nitrogen gas at lower stress levels only; the converse was true at higher stress levels of 550 MPa and 700 MPa under plain fatigue loading. However, under fretting fatigue loading, the plasma nitriding time did not influence the lives significantly.     

Elevated temperature fretting fatigue of Ti-17 with surface treatments

Fretting fatigue of Ti-17/Ti-8-1-1 contacts at 316 °C is examined experimentally. Different surface treatments are analyzed, including coatings, lubrication, and levels of shot peening. The evolution of friction is examined for a range of surface treatment. Fretting fatigue life for baseline specimens are obtained for a range of load parameters to determine loads that yield fretting fatigue lives of approximately 100,000 cycles. This applied load level was maintained constant for the different combinations of surface treatments to investigate the influence of surface treatment on fretting fatigue life. The Cu-Ni-In and Al-Br coatings and MoS₂ and Everlube lubricants are removed early in the fretting fatigue experiment; hence these surface treatments had little effect on fretting fatigue life. Shot peening increases fretting fatigue lives by about 60%. Block loading experiments show that minor cycles reduce fretting fatigue life.     

新的多轴非比例加载低周疲劳寿命估算公式

利用对 3 16L不锈钢多轴非比例加载低周疲劳的试验结果 ,对现有的多轴低周疲劳寿命估算方法进行讨论 ;基于 3 16L不锈钢非比例加载低周疲劳的微观机理 ,选择最大剪应变以及应变路径的非比例度作为损伤参量 ,建立基于临界面方法的新的非比例加载低周疲劳寿命估算公式 ;利用新的非比例加载低周疲劳寿命估算公式对寿命的预测结果表明 ,新的寿命估算公式对剪切型破坏的 3 16L与 3 16LN不锈钢及拉伸型破坏的 3 0 4不锈钢非比例加载低周疲劳寿命预测精度比现有的临界面方法高     

钢丝微动疲劳裂纹萌生寿命预测研究*

钢丝微动疲劳过程中,钢丝裂纹萌生特性直接影响其裂纹扩展特性,进而制约钢丝微动疲劳寿命,因此开展钢丝微动疲劳裂纹萌生寿命预测研究具有重要意义。基于有限元法、摩擦学理论和断裂力学理论,运用Smith-Watson-Topper（SWT）多轴疲劳寿命准则建立考虑磨损的钢丝微动疲劳裂纹萌生寿命预测模型,基于多种不同的钢丝疲劳参数估算方法对钢丝的微动疲劳裂纹萌生寿命进行了预测,并探究接触载荷、疲劳载荷、交叉角度及钢丝直径等微动疲劳参数对钢丝微动疲劳裂纹萌生寿命的影响规律。结果表明：基于中值法的预测结果最接近实际值;在微动疲劳过程中,钢丝微动疲劳裂纹萌生寿命主要与接触载荷和疲劳载荷相关。通过引入微动损伤参数建立简化的适用于钢丝绳的钢丝微动疲劳裂纹萌生寿命预测模型,通过与考虑磨损的预测模型计算结果进行对比验证了该模型的准确性。     

带有微动磨损缺口钢丝的疲劳特性

在自制的微动磨损试验机上进行钢丝的微动磨损试验,将微动磨损后的钢丝试样在液压伺服疲劳试验机上进行不同应力比和不同应力幅下的疲劳试验。结果表明,钢丝的微动磨损深度随微动时间和接触载荷的增加而增加,磨损缺口处的应力集中使其成为了裂纹萌生源,也使钢丝试样的疲劳寿命大大降低,微动磨损后钢丝试样的疲劳寿命和磨损深度呈反比关系。通过钢丝疲劳断口的SEM形貌分析了其疲劳断裂机制,断口对应不同的疲劳阶段,可分为裂纹萌生区、裂纹扩展区和裂纹瞬断区。     

中性腐蚀环境下钢丝的微动疲劳行为

在自制的微动疲劳试验机上开展中性腐蚀环境下单根钢丝的微动疲劳实验,考察在相同接触载荷下,不同振幅对钢丝的微动疲劳行为的影响,并用扫描电子显微镜观察疲劳钢丝的磨痕和断口形貌,研究钢丝微动疲劳断裂机制.结果表明:在较大的振幅下,钢丝的微动区均处于滑移状态,而在较小振幅下,钢丝的微动区从滑移状态逐渐转变为黏着状态;磨损机制主要为磨粒磨损、疲劳磨损、腐蚀磨损和塑性变形;钢丝疲劳寿命随着微动振幅的增大而减小;钢丝的疲劳断口可分为3个区域,即疲劳源区、裂纹扩展区及瞬间断裂区.     

Effect of contact load on fretting fatigue behaviour of steel wires

Abstract

The tension–tension fretting fatigue tests of steel wires were performed on a self-made fretting fatigue test equipment under contact loads ranging from 40 to 70 N and a strain ratio of 0·8. The results showed that when the contact load increased, the fretting regime of steel wires transformed from gross slip regime to mixed fretting regime. The fretting fatigue life in the mixed fretting regime was significantly lower than that in the gross slip regime. The main fretting wear mechanisms in the gross slip regime, where there were serious fretting damage and a lot of wear debris, were abrasive wear and fatigue wear. Microcracks were observed in the fretting scar of the mixed fretting regime, and the main fretting wear mechanisms were adhesive and fatigue wears. The fretting wear scar was the fatigue source region, and the fatigue fracture surface could be divided into three regions.     

微动疲劳参数对钢丝微动疲劳磨损演化的影响*

微动疲劳易引起钢丝表面磨损和横截面积损失,进而造成钢丝断裂失效并缩短钢丝绳使用寿命。不同微动疲劳参数（接触载荷、疲劳载荷、钢丝直径和交叉角度）引起差异的钢丝微动疲劳磨损特性,故研究微动疲劳参数对钢丝微动疲劳磨损演化规律影响至关重要。基于摩擦学理论和Marc仿真软件构建钢丝微动疲劳磨损模型,探究接触载荷、疲劳载荷、交叉角度和钢丝直径对钢丝微动疲劳磨损演化的影响规律。结果表明：钢丝微动疲劳磨损体积主要与接触载荷和疲劳载荷有关;疲劳钢丝的磨损深度、磨损率及磨损体积随着接触载荷的增加而增大,且不同接触载荷下疲劳钢丝磨损体积均随着循环次数的增加而呈线性增加;随疲劳载荷幅值的增加,疲劳钢丝的磨损深度、磨损率及磨损体积均呈增加趋势;在不同疲劳载荷范围下疲劳钢丝的磨损体积均随着循环次数的增加而呈线性增加;当接触载荷、疲劳载荷及钢丝间摩擦因数相同时,不同交叉角度和不同加载钢丝直径下疲劳钢丝的磨损体积相同。     

Wear analysis of materials used as orthopaedic implants

In the biomedical field, about 6% of the hip total prostheses must be replaced after 9 years. One of the main causes of the aseptic loosening may be attributed to fretting corrosion between the prosthesis and the bone cement. To understand this degradation, a fretting test between a stainless steel, 316L and PMMA has been used in Ringer solution. Fretting maps for the contact 316L/PMMA were determined in air and in Ringer solution. It has been shown that the lubricant effect of the aqueous environment shifts the gross slip/partial slip transition towards larger normal forces or lower displacements.To understand the fretting degradation behaviour of 316L against PMMA, fretting corrosion experiments have been investigated under constant applied potential. The first conclusion is that the dissipated energy is maximum at about −600 mV/SCE. The wear on PMMA does not depend on the applied potential. Moreover, the wear coefficient is lower than that in air due to the lubricant effect of the Ringer solution. Wear on 316L depends on the applied potential. The wear volume is minimum at −600 mV/SCE although the dissipated energy is maximum. The wear on 316L in Ringer solution is attributed to a dissolution process due to the local destruction of the passive film by fretting. The effect of potential on the wear of 316L may be accounted for by changes in the aqueous environment confined in the contact zone due to a restricted mass transport from the bulk solution and to the large local current densities consecutive to the destruction of the passive film. Accordingly, the wear volume on 316L is correlated to the time. Finally, the proton reduction, inside the contact, is believed to contribute significantly to the dissolution process.     

Influence of temperature on the fretting response between AISI 301 stainless steel and AISI 52100 steel

Fretting of AISI 301 stainless steel sheet in contact with AISI 52100 steel from 20 °C to 550 °C in air and argon has been studied. Transitions in the mechanical properties of 301SS and oxidative behavior of this pair have been identified as a function of temperature. Strength and ductility of 301SS is reduced from 20 °C to 250 °C, increasing susceptibility to fretting damage. Steady state friction decreases as temperature increases, reducing cyclic stresses. Wear resistance increases in this temperature range, increasing fatigue damage due to the increase in fatigue life associated with increased wear. This study aims to identify the causes of the transitions in behavior and determine the net outcome of the competing effects with regard to fatigue damage.     

Characteristics of fatigue crack initiation and fatigue strength of nitrided lCr-lMo-0.25V turbine rotor steels

To investigate the effect of nitriding layer on both fatigue crack initiation and fatigue life, turbine rotor steel (lCr-IMo-0.25V steel) specimens were nitrided by the nitemper method and then put to a rotary bending fatigue test at room and elevated temperatures. In nitriding, temperature and time were controlled to obtain a different nitrided thickness. Microstructure analysis, micro-Vickers hardness test, and scanning electron microscope observation were carried out for evaluating experiments. In results, the fatigue cracks of nitrided specimens were initiated at inclusion near the interface between nitrided layer and substrate, which showed fish-eye type appearance in fractograph. The fatigue life of nitrided specimens at every temperature was prolonged compared to that of the non-nitrided. However, there was not observable improvement in fatigue characteristics with the increase of a nitrided thickness.     

Fretting Fatigue Behavior of Cavitation Shotless Peened Ti–6Al–4V

Fretting fatigue behavior of cavitation shotless peened (CSP) titanium alloy, Ti–6Al–4V was investigated. Constant amplitude fretting fatigue tests were conducted at several maximum stress levels, σ_max, ranging from 400 to 555 MPa with a stress ratio of 0.1. Test results showed that the fretting fatigue life was enhanced by CSP treatment as compared to the unpeened specimen, but the enhancement was not as large as that from the shot-peening treatment. Residual stress measurements by X-ray diffraction method before and after fretting test showed that residual compressive stress was relaxed during fretting fatigue. Before fretting, CSP specimen had higher compressive residual stress on the surface than the shot-peened specimen. However, greater residual stress relaxation occurred in CSP specimen such that the relaxed compressive residual stress profile near the contact surface of CSP specimen was lower than that of shot-peened specimen. This lower compressive residual stress from fretting fatigue was the reason for shorter fretting fatigue life of CSP specimen as compared to shot-peened specimen at the applied stress level.     

Fretting fatigue strength of SCM435H steel and SUH660 heat‐resistant steel in hydrogen gas environment

Utilisation of hydrogen is expected to be one of the solutions against the problems of exhaustion of fossil fuels and reduction of carbon dioxide emissions. Evaluation of the materials for hydrogen utilisation machines is required. The objectives of this study are the characterisation of fretting fatigue strength of low‐alloy steel SCM435H and heat‐resistant steel SUH660, and the validation of effectiveness of nitriding in hydrogen gas environment. Fretting fatigue tests were conducted up to 3 × 10⁷ cycles. The decrease of fretting fatigue strength in hydrogen gas environment was found at the long‐life region exceeding 10⁷ cycles. The amount of the decrease of the fretting fatigue limit at 3 × 10⁷ cycles was 11% for SCM435H and 15% for SUH660. However, at the stress level above the fretting fatigue limit in air, the finite life in hydrogen gas increased more than that in air. The cause of extension of fatigue life was the delay of start of stable crack propagation. Fretting fatigue crack, which was smaller than 200 µm in length, consumed approximately 60% of the fatigue life in hydrogen gas environment. Fretting fatigue crack was steadily propagated after the test was started in air. Observations of the fretted surface showed that the fretting wear process in hydrogen gas environment was dominated by adhesion. Tangential force coefficient was higher in hydrogen gas environment than that in air. It is considered that the adhesion has a close relation to crack initiation in hydrogen gas environment, and as a result, the failure of specimen occurred at a lower stress level comparing the fretting fatigue limit in air. Copyright © 2008 John Wiley & Sons, Ltd.     

平板普通型爆破片疲劳破坏行为解析

针对爆破片服役过程中的疲劳破坏失效问题,以316L不锈钢为材料,采用试验检测结合数值模拟解析的方法对平板普通型爆破片开展相关研究。试验结果表明,平板普通型316L不锈钢爆破片的临界爆破压力P b=26.07 MPa,在0.8 P b(20.86 MPa)应力循环作用1000~8000次后,爆破压力逐步下降至21.87 MPa,在20.86 MPa恒定应力循环作用下爆破片的平均疲劳寿命为13175次。采用ABAQUS软件,针对平板普通型316L不锈钢爆破片进行静态断裂力学分析,进而结合FE_SAFE软件,可以较准确地预测不同应力水平循环作用下的疲劳寿命。相关研究为爆破片疲劳寿命预测提供了新思路,这对其安全服役有着重要意义。     

High-temperature low cycle fatigue, creep–fatigue and thermomechanical fatigue of steels and their welds

High-temperature low cycle fatigue (LCF) is influenced by various time-dependent processes such as creep, oxidation, phase transformations and dynamic strain ageing (DSA) depending on test conditions of strain rate and temperature. In this paper, the detrimental effects of DSA and oxidation in high-temperature LCF are discussed with reference to extensive studies on 316L(N) stainless steel and modified 9Cr–1Mo steel. DSA has been found to enhance the stress response and reduce ductility. It localizes fatigue deformation, enhances fatigue cracking and reduces fatigue life. High-temperature oxidation accelerates transgranular and intergranular fatigue cracking in modified 9Cr–1Mo steel and during long hold time tests in austenitic stainless steel. In welds, microstructural features such as presence of course grains in the HAZ and formation of brittle phases due to transformation of δ ferrite during testing influence crack initiation and propagation and fatigue life. Thermomechanical fatigue (TMF) studies are suggested as more closer to the actual service conditions. In 316L(N) stainless steel, TMF lives under out-of-phase cycling are found to be lower than those under in-phase conditions in the low-temperature regimes, while the converse holds good when the upper temperature encompassed the creep-dominant regime.     

Fretting fatigue behavior of Al7075-T6 at sub-zero temperature

In some fretting fatigue applications, such as aero industry, the temperature may drop well below −50 °C Fretting fatigue behavior of aluminum alloy Al7075-T6 is investigated at temperatures of 24, 0, −25 and −50 °C in this work. The results show that (i) normal fatigue life increases considerably at sub-zero temperatures up to around 85% for low working stresses and reduces to about 40% for higher working stresses; (ii) fretting fatigue life at sub-zero temperatures rises significantly up to around 220% for low working stresses and reduces to about 50% for higher working stresses; (iii) ultimate strength of material changes from −15% to 15% under the fretting fatigue test conditions; and finally (iv) some parameters such as mechanical properties and fatigue behavior of material at low temperatures, contact load relaxation, crack closure, oxidation and some unknown sources can be thought to be responsible for fretting fatigue behavior of Al7075-T6 at sub-zero temperatures.