9SiCr钢短时等温下贝氏体显微组织研究

借助X射线衍射分析、金相组织观察研究了9SiCr奥氏体化后的冷却速度与等温保温时间对下贝氏体相变产物的形貌、相组成和晶格常数的影响.实验结果表明,当奥氏体化后的冷却速度接近临界冷速(60 ℃/s)、等温时间大于孕育期(80 s)且在20 min以内短时等温获得非常规下贝氏体组织,其光学显微组织形态呈现由单一α相组成的短针状,晶格常数和平衡态α相不同,其值为2.874,呈现晶格膨胀状,具有马氏体转变特征.     

15Cr11Cu2Si2MoMn钢的成分设计及动力学测定

根据(GB/T 1220-1992)不锈钢标准成分范围,对兼具高强度、高韧性和高耐腐蚀性钢的组织,结合基础理论分析与软件模拟,进行成分设计,预设组织为含Cu无碳化物贝氏体组织.利用DIL-87型淬火膨胀仪对所设计试验钢在不同奥氏体化温度、保温时间和冷却速度等条件下进行膨胀试验,测定其相变动力学参数,结合光学显微镜分析其相变行为并绘制相应的相变动力学曲线.结果 表明:在连续冷却转变过程中,冷却速度为0.1～5℃/s时,试验钢的组织为贝氏体与马氏体,冷却速度小于0.1℃/s时,为珠光体、贝氏体和马氏体;等温转变过程中,当等温温度在Bs(375℃)～Bf(225℃)之间时,转变产物以贝氏体为主,在Ms(307℃)以上为贝氏体,在Ms(307℃)以下为贝氏体和马氏体.从贝氏体转变过程中来看,预设试验钢的贝氏体转变区间宽泛且Bs点较低.     

30MnNiCuMoB-RE铸钢的连续冷却相变动力学研究

采用淬火相变热膨胀仪测定了30MnNiCuMoB-RE铸钢890℃完全奥氏体化后以不同速度连续冷却时的膨胀曲线。通过金相检验和硬度测定研究了30MnNiCuMoB-RE铸钢在连续冷却过程中的相变动力学。结果表明：30MnNiCuMoB-RE铸钢在890℃完全奥氏体化后以0.01～100℃/s的速率冷却时，随着冷却速率的增大，奥氏体依次转变为铁素体、贝氏体和马氏体，铁素体转变温度区间为717～611℃,贝氏体转变温度区间为590～323℃,马氏体转变温度区间为313～168℃;从获得的连续冷却转变(CCT)曲线可知，随着冷却速率的降低，发生贝氏体相变的临界冷速为50℃/s,发生铁素体转变的临界冷速为0.5℃/s;由于钢中存在一定程度的偏析，以0.01～0.2℃/s的速率冷却时，奥氏体依次转变为铁素体和贝氏体，钢的组织不均匀；随着冷却速率的提高，钢的硬度从200 HV10提高至500 HV10。     

压应力对Cr-Mo钢连续冷却贝氏体相变的影响

采用Gleeble-1500热模拟试验机测量了Cr-Mo钢在1～90℃/s的冷却速度下奥氏体连续冷却过程中的温度-膨胀曲线,用origin软件进行数据处理,获得了实验钢的CCT曲线;同时测量了施加轴向载荷为0、40MPa、80MPa和120MPa的压应力时奥氏体连续冷却过程中的温度-膨胀曲线,冷却速度分别为50℃/s、70℃/s和90℃/s.利用杠杆定律,根据不同温度下的膨胀量计算得到贝氏体相变动力学曲线,研究了压应力对贝氏体相变动力学和贝氏体相变温度的影响.结果表明,在以冷却速度为50℃/s和70℃/s连续冷却时,压应力抑制前期阶段的贝氏体相变,促进后期阶段的贝氏体相变;在以冷却速度为90℃/s连续冷却时,压应力对整个贝氏体相变过程都有促进作用,特别是应力较大时:压应力使贝氏体相变开始温度Bs升高,贝氏体相变终了温度Bf降低.     

42CrMoA钢过冷奥氏体连续冷却相转变曲线

结合膨胀法和金相-硬度法,利用Gleeble-1500D热模拟机测定了42CrMoA钢的临界点Ac1、Ac3和Ms点,测定了该钢在不同冷却速度下连续冷却时的膨胀曲线,相转变点;分析了连续冷却过程中过冷奥氏体转变过程及转变产物的组织形貌;测定了不同冷却速度下相转变后的硬度,获得了该钢过冷奥氏体连续冷却相转变曲线.结果表明,当冷却速度小于0.1℃/s时,转变产物为铁素体和珠光体组织;当冷却速度0.2～0.6℃/s时转变产物是铁素体、珠光体、贝氏体的混合组织;当冷却速度为0.7～17℃/s时,转变产物是贝氏体和马氏体的混合组织;当冷却速度大于20℃/s时,转变产物为完全马氏体,此次实验并没有获得完全贝氏体.     

等温时间对60Si2Mn钢下贝氏体组织性能的影响

通过热模拟实验和盐浴淬火处理,研究了60Si2Mn钢盘条奥氏体化后在300℃等温盐浴淬火时的组织演变规律及相应的力学性能,结果表明:在300℃等温盐浴淬火,形成下贝氏体,相变孕育期约为100 s,相变完成时间约为3000 s。随等温时间延长,材料抗拉强度缓慢降低,而面缩率不断增加,等温3000 s后,材料抗拉强度保持在1800 MPa以上,面缩率可达到50%。组织分析结果显示,下贝氏体由针状铁素体和纳米级条状奥氏体组成,起到提高材料韧性的作用。     

一种非调质钢组织转变及性能的研究

一种非调质钢在Gleeble 3800热模拟机上进行试验,测定了该非调质钢在不同冷却速度下膨胀曲线,同时结合金相-硬度法获得了该非调质钢的连续冷却转变时静态CCT曲线、显微组织和维氏硬度,以及等温转变时显微组织和维氏硬度。奥氏体在连续冷却速度分别为0.1、0.5、1℃/s以及在560℃等温转变前后的连续冷却速度为2℃/s,等温时间分别为10、20 min时,转变组织为铁素体+珠光体;奥氏体在560℃等温转变前后的连续冷却速度分别为3、4℃/s,等温时间分别为10、20 min时,转变组织为铁素体+珠光体+微量或少量贝氏体。本研究结果,对下游用户使用圆钢锻造成零件后,获得铁素体+珠光体组织或铁素体+珠光体+微量或少量贝氏体组织的冷却工艺提供了参考。     

非调质钢40MnV热变形后冷却相变动力学

为了实现非调质钢轴类件楔横轧热成形后控制冷却过程性能优化和节能减排,采用物理模拟手段对热变形后的非调质钢40MnV进行了连续冷却和等温冷却相变动力学研究。首先采用膨胀仪测定试验钢临界点Ac1、Ac3温度,然后利用Gleeble 3500热模拟机测定了40MnV钢的冷却过程相变动力学转变曲线,并分析了转变产物的显微组织。结果表明:冷却速度增大将减小铁素体的晶粒尺寸,同时也减小铁素体的体积分数;奥氏体晶粒尺寸和钒都对转变温度有影响,但在相变区快冷时奥氏体晶粒尺寸起主要作用,且晶粒尺寸减小将提高转变温度;相变区冷却速度为3℃/s时相变生成贝氏体,且其形态为典型的上贝氏体,而相变区冷却速度为6℃/s时对应转变的组织是马氏体;随着冷却速度的增加,析出过程中V(C,N)的数量增加,最大颗粒尺寸减小;等温冷却中V(C,N)析出物的形态为圆形和方形且数量很少,析出物的颗粒尺寸随转变温度的降低而减小。     

奥氏体化温度对贝氏体钢等温转变及力学性能的影响

采用热膨胀仪和热模拟试验机在880~1050 ℃奥氏体化后进行300 ℃等温转变试验,研究了不同奥氏体化温度对中碳贝氏体钢等温相变动力学以及组织形貌、力学性能的影响。结果表明,奥氏体化温度升高导致晶粒尺寸增加,Ms点下降,贝氏体等温相变的孕育期延长;降低奥氏体化温度,可明显缩短贝氏体转变速率峰值出现的时间,说明较低的奥氏体化温度有利于加速贝氏体的转变。在本试验温度范围内,880 ℃奥氏体化处理试样的综合力学性能优异,抗拉强度为1671 MPa, 伸长率为13.3%。     

奥氏体化条件对高强度贝氏体钢相变动力学的影响

以低碳Si-Mn-Nb贝氏体钢为研究对象,利用相变仪进行贝氏体区等温实验。通过对热膨胀曲线的分析,获得了贝氏体相变动力学曲线;分析了奥氏体化条件对贝氏体相变动力学的影响;分析了奥氏体化条件及贝氏体区等温温度对贝氏体组织形态的影响。结果表明:随着奥氏体晶粒尺寸的细化,贝氏体相变动力学进程减缓,且相同等温温度下对应的贝氏体体积分数降低;随着贝氏体区等温温度的升高,贝氏体板条宽度增加,马氏体/奥氏体混合组织体积分数提高。     

新型的治疗阿尔茨海默氏症药物(1-二甲基磷酰基-2,2,2-三氯)-乙基-1-醇烟酸醋对体外神经细胞的作用

目的: 观察本实验室合成的一种治疗阿尔茨海默氏症(AD)的药物(1-二甲基磷酰基-2, 2, 2 -三氯)-乙基^-1-醇烟酸醋(NMF),对体外培养的皮层神经细胞活性的影响以及对海人藻酸(KA)所致的神经损伤的保护作用。方法: 采用体外培养皮层神经元的方法,解剖分离 15 d胚胎小鼠皮层神经细胞, 接种于 96孔板,48 h 后加药并培养 72 h,以 MIT 法 观察 NMF 对小鼠皮层神经细胞活性的影响;同时将接种于 24 孔板的细胞预先给予 NMF,d 3 时加或不加KA处理后,以台盼蓝染色鉴别并计数死、活细胞,可得出细胞的存活率。结果: NMF 明显促进胎鼠皮层神经元活性,其中 NMF1、0. 1、10nmol·L^-1促进神经元活性增殖率分别高达 34.7%、37.4%、36. 7%, NMF 明显促进正常胎鼠皮层神经元存活卒,与对照组比较,10nmol·L^-1 NMF 对皮层神经元的存活率分别提高 39.3%、73.5%。 NMF能显著 对抗 KA 所致的神经元损伤,与 KA 损伤组相比, NMF0.1、10、10nmol·L^-1对损伤皮层神经元的保护率分别为 77.30%、80.10%、84.15%。结论: NMF 明 显促进胎鼠皮层神经元的洁性、提高正常皮层神经元,的存活卒,并能有效地保护KA所致的神经元损伤,提示 NMF 是一种很有潜力的治疗 AD 的药物。     

Three-Dimensional Growth of Coherent Ferrite in Austenite: A Molecular Dynamics Study

Coherent second phase often exhibits anisotropic morphology with specifi c orientations with respect to both the second and the matrix phases. As a key feature of microstructure, the morphology of the coherent particles is essential for understanding the second-phase strengthening eff ect in various industrial alloys. This letter reports anisotropic growth of coherent ferrite from austenite matrix in pure iron based on molecular dynamics simulation. We found that the ferrite grain tends to grow into an elongated plate-like shape, independent of its initial confi guration. The fi nal shape of the ferrite is closely related to the misfi t between the two phases, with the longest direction and the broad facet of the plate being, respectively, consistent with the best matching direction and the best matching plane calculated via the Burgers vector content(BVC) method. The strain energy calculation in the framework of Eshelby's inclusion theory verifi es that the simulated orientation of the coherent ferrite is energetically favorable. It is anticipated that the BVC method will be applicable in analysis of anisotropic growth and morphology of coherent second phase in other phase transformation systems.     

Rheology Feature of Simple Metal Melt

The rheology feature of Sb, Bi melt and alloys was studied using coaxial cylinder high-temperature viscometer. The results showed that the curve of torsion-rotational speed for Sb melt presents a linear relation in all measured temperature ranges, whereas for the Bi melt, the curve presents obvious non-Newtonian feature within the low temperature range and at relative high shear stress. The rheology feature of Sb80Bi20 and Sb20Bi80 alloy melts was well correlated with that of Sb and Bi, respectively. It is considered that the rheology behavior of Sb melt plays a crucial role in Sb80Bi20 alloy and that of Bi melt plays a crucial role in Sb20Bi80 alloy.     

Effect of Short-Time Aging on the Pitting Corrosion Behavior of a Novel Lean Duplex Stainless Steel 2002

The effect of short-time aging in the temperature range between 400 and 1000 °C on the pitting corrosion behavior and mechanical property of a novel lean duplex stainless steel(LDSS) 2002 was investigated through the potentiostatic critical pitting temperature(CPT) tests and the Charpy impact tests. Both the pitting corrosion resistance and the toughness of aged specimens degraded due to the precipitation of detrimental secondary phases and the most significant reduction of CPT and impact energy emerged at 650 °C concurrently. The CPT of LDSS 2002 specimen aged at 650 °C decreased by 28 °C, and the impact energy dropped from 69 to 29 J/cm~2 compared with the solution-annealed sample. Transmission electron microscopy characterization showed that the main precipitates in LDSS 2002 were Cr_2N and M_(23)C_6 along the ferrite–austenite grain boundaries.     

INTRODUCTION TO PATENTS

The invention provides a method of making a mold which can reduce SOx generation rate while preventing decrease in hardening rate in the case of using sulfuric acid for a hardener composition. The method has a mixture step in which fire-resistant particles, a hardener composition and a binder composition are mixed to obtain a composition for a mold. The hardener composition contains sulfuric acid. In the mixture step, sodium carbonate is added. A molar ratio of the sulfuric acid to the sodium carbonate is 0.5 or more and 4.0 or less.     

China Foundry Week 2014

China Foundry Week, hosted by the Foundry Institution of Chinese Mechanical Engineering Society （FICMES） each year, is a large academic event in China. It is one of the ten high-impact activities sponsored by the Chinese Mechanical Engineering Society.     

17th Conference of Hydrodynamic and Electromechanical Control Engineering Call for papers

正1.Contents In order to promote the academic exchanges and technical communication of the research in the field of fluid power transmission and control,fluid control engineering specialized committee of the Chinese Society of Theoretical and Applied Mechanics will hold the 17th Conference of Hydrodynamic and Electromechanical Control Engineering on July 27-29,2014 in Tibet,Lhasa city.     

Information for Contributors

正The Transactions of Nonferrous Metals Society of China,founded in 1991 and sponsored by The Nonferrous Metals Society of China,is published monthly now and mainly contains reports of original research which reflect the new progresses in the field of nonferrous metals science and technology,including mineral processing,extraction metallurgy,metallic materials and heat treatments,metal working,physical metallurgy,powder metallurgy,with the emphasis     

Preface

<正>We are pleased to present this Special Issue of Transactions of Nonferrous Metals Society of China containing selected papers from the First Asian Conference on Aluminum Alloys(ACAA-2013),held in Beijing,China,13–17 October 2013.This conference has been initiated,with approval of     

Information for Contributors

The Transactions of Nonferrous Metals Society of China, founded in 1991 and sponsored by The Nonferrous Metals Society of China, is published monthly now and mainly contains reports of original research which reflect the new progresses in the field of nonferrous metals science and technology, including mineral processing, extraction metallurgy, metallic materials and heat treatments, metal working, physical metallurgy, powder metallurgy, with the emphasis on fundamental science. It is the unique preeminent publication in English for scientists, engineers, under/post-graduates on the field of nonferrous metals industry. This journal is covered by many famous abstract/index systems and databases such as SCI Expanded, Ei Compendex Plus, 1NSPEC, CA, METADEX, AJ and JICST.