热处理温度对TiNiCuCo合金的力学性能和形状记忆效应的影响

通过真空感应熔炼制备TiNiCuCo形状记忆合金铸锭,然后经锻造、轧制、热拉拔得到准0.5mm的线材,最后对线材进行300~700℃退火。通过拉伸试验和弯曲回复法等研究了不同温度热处理后TiNiCuCo合金的力学性能和形状记忆效应。结果表明:在300~500℃进行热处理,TiNiCuCo合金的抗拉强度和伸长率几乎不发生变化;在600~700℃进行热处理,其抗拉强度显著降低,伸长率显著增大。随着热处理温度的升高,平台应力先减小再增大。在热处理温度为500℃时平台应力最小,为32MPa。平台应变在300~400℃热处理几乎不发生变化,最大值为6.8%。随着热处理温度的升高,平台应变逐渐减小,700℃时平台应变为3.5%。TiNiCuCo合金在300~500℃热处理后具有良好的形状记忆效应;6%~8%弯曲应变后,合金的最大形状回复率可达96%以上。高于500℃进行热处理,合金的最大形状回复率降低。TiNiCuCo合金对温度的响应程度几乎不随热处理温度发生变化。     

退火工艺对挤压成型镁锰钛合金壳体磨损和腐蚀性能的影响

采用不同工艺对某新型挤压成型Mg-Mn-Ti合金壳体进行了退火热处理,并进行了磨损和腐蚀性能的测试与分析。结果表明:随热处理温度从260℃提高到380℃或热处理时间从2 h延长到8 h,合金壳体的磨损和腐蚀性能都先提高后下降。与260℃热处理相比,320℃热处理时合金壳体的磨损体积减小44%、腐蚀电位正移182 m V;与2 h热处理相比,5 h热处理时机械壳体的磨损体积减小41%、腐蚀电位正移162 m V。合金壳体的热处理温度和时间分别优选为320℃、5 h。     

大型透平机壳焊后热处理的残余应力数值模拟

采用热-粘弹塑性有限元模型,在考虑蠕变效应的基础上,对大型透平机壳进行焊后热处理数值模拟.结果表明,焊后机壳残余应力较高,部分节点超过材料的屈服强度;经过热处理后,机壳整体残余应力均低于材料的屈服强度.在300℃去应力退火,机壳残余应力降低幅度不大;当退火温度升到550℃时,机壳应力降低显著.     

激光沉积修复金属去应力退火局部热处理工艺北大核心CSCD

利用感应加热系统对激光沉积修复试样进行去应力退火局部热处理,研究了局部热处理的保温温度和时间对试样温度分布和残余应力的影响规律。结果表明:感应加热系统的局部加热效果明显;随着局部热处理保温温度的提高和保温时间的延长,加热区温度分布更加均匀;600℃去应力退火热处理后,残余应力平均降低30.6%以上,高于500℃去应力退火热处理后的应力消减幅度,局部热处理后由残余应力引起的端部变形量由2.67 mm消减为0.54 mm。试验验证了基于感应加热的局部热处理可有效消减修复应力和变形量。     

激光沉积修复金属去应力退火局部热处理工艺

利用感应加热系统对激光沉积修复试样进行去应力退火局部热处理,研究了局部热处理的保温温度和时间对试样温度分布和残余应力的影响规律。结果表明:感应加热系统的局部加热效果明显;随着局部热处理保温温度的提高和保温时间的延长,加热区温度分布更加均匀;600℃去应力退火热处理后,残余应力平均降低30.6%以上,高于500℃去应力退火热处理后的应力消减幅度,局部热处理后由残余应力引起的端部变形量由2.67 mm消减为0.54 mm。试验验证了基于感应加热的局部热处理可有效消减修复应力和变形量。     

热处理对变形AZ80镁合金组织和硬度的影响

研究了变形AZ80镁合金在不同热处理条件下组织和硬度变化。结果表明:镁合金在150~250℃退火时,晶粒先增大后减小,最终晶粒细小且均匀;但保温时间较长,退火温度为300~350℃时,晶粒尺寸比较稳定;在400℃退火处理后,短时间内晶粒立即出现异常长大现象,晶粒粗大且不均匀,合金性能较差。退火处理的最佳温度为280~350℃。热处理温度对AZ80镁合金的硬度值有显著影响,但退火处理时间的影响却不明显。     

退火热处理对高速电弧喷涂碳钢涂层组织性能的影响

采用高速电弧喷涂技术制备高碳钢涂层,并分别进行450、550和650℃保温2h的退火热处理,研究退火工艺对涂层的组织结构、相成分、残余应力及硬度的影响规律。结果表明,除了氧化物之外,高碳钢涂层在热处理前主要含有马氏体组织,450℃退火后出现了粒状渗碳体+铁素体特征的组织,550和650℃退火之后呈现块状特征的组织,且明显粗大;退火处理后涂层中的拉应力有减小的趋势;涂层硬度随着加热温度的升高而降低。因此,合适的热处理工艺可以有效地控制碳钢喷涂层的组织性能。     

焊后热处理对L245NCS微合金钢焊接残余应力的影响

采用履带式电加热法对L245NCS微合金钢焊接接头进行了不同退火温度和不同保温时间的焊后热处理,采用小孔法测量焊接残余应力。结果表明,560℃退火保温3.0 h焊后热处理方案和620℃退火保温1.5 h焊后热处理方案对降低焊接残余应力均较明显,其中560℃×3.0 h焊后热处理消除残余应力的松弛率在50%左右,620℃×1.5 h焊后热处理方案消除残余应力的松弛率基本高于80%,说明延长保温时间并不能有效地降低焊接残余应力。620℃×1.5 h焊后热处理方案对于消除L245NCS微合金钢焊接残余应力更为有效。     

Ti-Ni-V形状记忆合金超弹性研究

采用拉伸和应力-应变循环实验研究了退火温度、时效温度、时效时间、形变温度和应力-应变循环对Ti-50.8Ni-0.5V(原子分数,%)形状记忆合金超弹性(SE)的影响。随退火温度的升高,合金的应力诱发马氏体临界应力(σM)先减小后增大,超弹性残留应变(εR)先增大后减小再增大,为了获得优异的室温SE,退火温度应取500~600℃。随时效温度的升高,合金的σM降低,εR增加,SE变差;随时效时间延长,300℃时效态合金的SE稳定,400和500℃时效态合金的SE变差。随形变温度的升高,σM增加,SE改善。随循环次数增加,400℃退火态合金的SE稳定;500℃退火态合金的σM降低;600℃退火态合金的SE由非线性向线性转变。     

去应力退火对Ti40合金力学性能的影响

Ti40合金常规热处理后进行不同温度的去应力退火,观察并测试合金在不同去应力退火后的组织和力学性能。结果表明,不同的去应力工艺对材料的力学性能有较大的影响。当去应力温度在500℃到550℃之间时,Ti40合金室温、高温力学性能的强塑性匹配达到最好,此时持久性能虽有所降低,但能满足使用要求;而当去应力温度达到600℃以上时,合金的强度变化不大但是塑性急剧下降。推荐550℃×4 h为合金常规热处理后的最优退火工艺。     

Effects of Post-weld Heat Treatment on Microstructure,Mechanical Properties and the Role of Weld Reinforcement in 2219 Aluminum Alloy TIG-Welded Joints

In as-welded state, each region of 2219 aluminum alloy TIG-welded joint shows diff erent microstructure and microhardness due to the diff erent welding heat cycles and the resulting evolution of second phases. After the post-weld heat treatment, both the amount and the size of the eutectic structure or θ phases decreased. Correspondingly, both the Cu content in α-Al matrix and the microhardness increased to a similar level in each region of the joint, and the tensile strength of the entire joint was greatly improved. Post-weld heat treatment played the role of solid solution strengthening and aging strengthening. After the post-weld heat treatment, the weld performance became similar to other regions, but weld reinforcements lost their reinforcing eff ect on the weld and their existence was more of an adverse eff ect. The joint without weld reinforcements after the post-weld heat treatment had the optimal tensile properties, and the specimens randomly crack in the weld zone.     

The First Phase of the SRIF Industrialized Base in ＂West Area＂ Has Been Put into Operation

After nearly two years＇ tense construction, the first phase of industrialized base of Shenyang Research Institute of Foundry （SRIF）, located at the Tiexi Casting and Forging Industrial Park in the west of Tiexi District, has now been completed and formally put into operation.     

新型的治疗阿尔茨海默氏症药物(1-二甲基磷酰基-2,2,2-三氯)-乙基-1-醇烟酸醋对体外神经细胞的作用

目的: 观察本实验室合成的一种治疗阿尔茨海默氏症(AD)的药物(1-二甲基磷酰基-2, 2, 2 -三氯)-乙基^-1-醇烟酸醋(NMF),对体外培养的皮层神经细胞活性的影响以及对海人藻酸(KA)所致的神经损伤的保护作用。方法: 采用体外培养皮层神经元的方法,解剖分离 15 d胚胎小鼠皮层神经细胞, 接种于 96孔板,48 h 后加药并培养 72 h,以 MIT 法 观察 NMF 对小鼠皮层神经细胞活性的影响;同时将接种于 24 孔板的细胞预先给予 NMF,d 3 时加或不加KA处理后,以台盼蓝染色鉴别并计数死、活细胞,可得出细胞的存活率。结果: NMF 明显促进胎鼠皮层神经元活性,其中 NMF1、0. 1、10nmol·L^-1促进神经元活性增殖率分别高达 34.7%、37.4%、36. 7%, NMF 明显促进正常胎鼠皮层神经元存活卒,与对照组比较,10nmol·L^-1 NMF 对皮层神经元的存活率分别提高 39.3%、73.5%。 NMF能显著 对抗 KA 所致的神经元损伤,与 KA 损伤组相比, NMF0.1、10、10nmol·L^-1对损伤皮层神经元的保护率分别为 77.30%、80.10%、84.15%。结论: NMF 明 显促进胎鼠皮层神经元的洁性、提高正常皮层神经元,的存活卒,并能有效地保护KA所致的神经元损伤,提示 NMF 是一种很有潜力的治疗 AD 的药物。     

Three-Dimensional Growth of Coherent Ferrite in Austenite: A Molecular Dynamics Study

Coherent second phase often exhibits anisotropic morphology with specifi c orientations with respect to both the second and the matrix phases. As a key feature of microstructure, the morphology of the coherent particles is essential for understanding the second-phase strengthening eff ect in various industrial alloys. This letter reports anisotropic growth of coherent ferrite from austenite matrix in pure iron based on molecular dynamics simulation. We found that the ferrite grain tends to grow into an elongated plate-like shape, independent of its initial confi guration. The fi nal shape of the ferrite is closely related to the misfi t between the two phases, with the longest direction and the broad facet of the plate being, respectively, consistent with the best matching direction and the best matching plane calculated via the Burgers vector content(BVC) method. The strain energy calculation in the framework of Eshelby's inclusion theory verifi es that the simulated orientation of the coherent ferrite is energetically favorable. It is anticipated that the BVC method will be applicable in analysis of anisotropic growth and morphology of coherent second phase in other phase transformation systems.     

Effect of Rare Earth Doping on Impedance,Modulus and Conductivity Properties of Multiferroic Composites:0.5(BiLa_xFe_(1-x)O_3)–0.5(PbTiO_3)

The Lanthanum-doped bismuth ferrite–lead titanate compositions of 0.5(Bi LaxFe1-xO3)–0.5(Pb Ti O3)(x = 0.05,0.10,0.15,0.20)(BLxF1-x-PT) were prepared by mixed oxide method.Structural characterization was performed by X-ray diffraction and shows a tetragonal structure at room temperature.The lattice parameter c/a ratio decreases with increasing of La(x = 0.05–0.20) concentration of the composites.The effect of charge carrier/ion hopping mechanism,conductivity,relaxation process and impedance parameters was studied using an impedance analyzer in a wide frequency range(102–106Hz) at different temperatures.The nature of Nyquist plot confirms the presence of bulk effects only,and non-Debye type of relaxation processes occurs in the composites.The electrical modulus exhibits an important role of the hopping mechanism in the electrical transport process of the materials.The ac conductivity and dc conductivity of the materials were studied,and the activation energy found to be 0.81,0.77,0.76 and 0.74 e V for all compositions of x = 0.05–0.20 at different temperatures(200–300 °C).     

Quantitative Analysis of the Crystallographic Orientation Relationship Between the Martensite and Austenite in Quenching–Partitioning–Tempering Steels

The orientation relationships(ORs)between the martensite and the retained austenite in low-and medium-carbon steels after quenching–partitioning–tempering process were studied in this work.The ORs in the studied steels are identified by selected-area electron diffraction(SAED)as either K–S or N–W ORs.Meanwhile,the ORs were also studied based on numerical fitting of electron backscatter diffraction data method suggested by Miyamoto.The simulated K–S and N–W ORs in the low-index directions generally do not well coincide with the experimental pole figure,which may be attributed to both the orientation spread from the ideal variant orientations and high symmetry of the low-index directions.However,the simulated results coincide well with experimental pole figures in the high-index directions{123}_(bcc).A modified method with simplicity based on Miyamoto’s work was proposed.The results indicate that the ORs determined by modified method are similar to those determined by Miyamoto’method,that is,the OR is near K–S OR for the low-carbon Q–P–T steel,and with the increase of carbon content,the OR is closer to N–W OR in medium-carbon Q–P–T steel.     

Effect of Short-Time Aging on the Pitting Corrosion Behavior of a Novel Lean Duplex Stainless Steel 2002

The effect of short-time aging in the temperature range between 400 and 1000 °C on the pitting corrosion behavior and mechanical property of a novel lean duplex stainless steel(LDSS) 2002 was investigated through the potentiostatic critical pitting temperature(CPT) tests and the Charpy impact tests. Both the pitting corrosion resistance and the toughness of aged specimens degraded due to the precipitation of detrimental secondary phases and the most significant reduction of CPT and impact energy emerged at 650 °C concurrently. The CPT of LDSS 2002 specimen aged at 650 °C decreased by 28 °C, and the impact energy dropped from 69 to 29 J/cm~2 compared with the solution-annealed sample. Transmission electron microscopy characterization showed that the main precipitates in LDSS 2002 were Cr_2N and M_(23)C_6 along the ferrite–austenite grain boundaries.     

Information for Contributors

正The Transactions of Nonferrous Metals Society of China,founded in 1991 and sponsored by The Nonferrous Metals Society of China,is published monthly now and mainly contains reports of original research which reflect the new progresses in the field of nonferrous metals science and technology,including mineral processing,extraction metallurgy,metallic materials and heat treatments,metal working,physical metallurgy,powder metallurgy,with the emphasis     

Preface

<正>We are pleased to present this Special Issue of Transactions of Nonferrous Metals Society of China containing selected papers from the First Asian Conference on Aluminum Alloys(ACAA-2013),held in Beijing,China,13–17 October 2013.This conference has been initiated,with approval of     

Information for Contributors

The Transactions of Nonferrous Metals Society of China, founded in 1991 and sponsored by The Nonferrous Metals Society of China, is published monthly now and mainly contains reports of original research which reflect the new progresses in the field of nonferrous metals science and technology, including mineral processing, extraction metallurgy, metallic materials and heat treatments, metal working, physical metallurgy, powder metallurgy, with the emphasis on fundamental science. It is the unique preeminent publication in English for scientists, engineers, under/post-graduates on the field of nonferrous metals industry. This journal is covered by many famous abstract/index systems and databases such as SCI Expanded, Ei Compendex Plus, 1NSPEC, CA, METADEX, AJ and JICST.