铝合金和镀锌钢异种金属CMT焊接性分析

针对汽车工业中铝合金和镀锌钢板的轻量化结构制造,利用正交试验法对铝合金与镀锌钢薄板搭接件进行了异种材料冷金属过渡(CMT)熔钎焊连接,研究了工艺参数、焊丝成分以及镀锌层厚度对焊缝表面成形和接头力学性能的影响.铝/镀锌钢板CMT熔钎焊的接头为典型的搭接接头,在整个焊接过程中,硅和锌很好的起到了促进熔化的铝在钢板表面润湿和铺展的作用.通过试验得出理想的工艺参数,可以得到良好的焊接接头.     

Al2O3p/6061Al复合材料焊接工艺参数的优化及接头组织

通过与基体铝合金的对比试验研究了颗粒增强铝基复合材料Ａｌ２Ｏ３ｐ／６０６１Ａｌ扩散焊各主要工艺参数对接头强度的影响规律,探讨了接头区域微观组织状态对接头强度的影响。结果表明：焊接温度是影响接头强度的主要工艺参数,接头区域存在氧化物及增强相偏聚等缺陷,是造成该种材料焊接性差的主要原因,在此基础上成功实现了颗粒增强铝基复合材料Ａｌ２Ｏ３ｐ／６０６１Ａｌ的扩散连接。     

基于试验和数值模拟的铝合金压印连接研究

对压印连接的工艺过程和接头性能进行了研究.对铝合金板进行了压印连接,对压印接头进行了微观组织分析、拉伸—剪切试验和疲劳试验.建立了铝合金板压印连接过程的有限元模型,并由模拟连接过程得到接头截面的2D模型.然后由2D模型形成压印接头的3D模型,并采用3D模型进行拉伸—剪切试验和疲劳试验过程的模拟和分析.试验和模拟结果表明:压印连接过程中材料的强度值提高;压印接头的疲劳性能较好,疲劳极限约为接头最大拉剪强度的70％.     

铝锂合金填充式摩擦点焊工艺

以5A90铝锂合金搭接接头为研究对象,进行了不同工艺参数下的填充式摩擦点焊试验,并对点焊接头进行了剪切试验、十字拉伸试验,在此基础上对典型接头微观组织结构进行了金相分析和横截面显微硬度测试.结果表明,采用填充式摩擦点焊技术焊接1.5 mm壁厚铝锂合金搭接接头在旋转频率1800 r/min、焊接时间1.5 s左右可获得良好的抗剪能力;十字拉伸强度对于焊接工具旋转频率、下压量不敏感,但随焊接时间的增加而增加;对接头横截面进行金相观察发现,焊点与母材的竖直连接界面为连接薄弱区域,接头横截面显微硬度分布表明,在焊点中心附近水平连接面具有较低的硬度分布.     

TP304H/12Cr1MoV异种钢管的瞬时液相扩散连接

用FeNiCrSiB (A)合金作中间层,氩气保护,对12Cr1MoV珠光体耐热钢和TP304H奥氏体不锈钢管进行了瞬时液相扩散连接.用正交试验的方法研究了工艺参数对接头组织和性能的影响,分析了TLP连接接头的显微组织、断口形貌、力学性能和元素分布,确定出了合适的连接工艺参数.研究结果表明,连接温度1240℃,等温凝固时间3min,压力4MPa时,接头的强度最高达到590MPa,其断口呈韧性断裂特征.     

小试样加压铝热焊工艺及性能

为了改善铝热焊接头性能,本研究通过设计小试样加压铝热焊正交试验,研究了顶锻等待时间、顶锻量和预留焊缝间隙三个主要因素对接头性能的影响,通过极差分析获得了最佳焊接工艺参数,进行了性能研究和组织分析。结果表明,选择加压铝热焊最佳工艺参数进行加压铝热焊,可明显改善接头组织,细化晶粒,减少焊接缺陷,从而提高焊接接头的强度和塑性。与常规铝热焊接头相比较,加压铝热焊接头的强度和韧性高,质量好。     

过渡层对铝/钢FSB接头性能和组织的影响

通过镀覆镍及Ni/Cu复合过渡层,采用锌作为钎料,对工业纯铝和低碳钢板进行了搅拌摩擦钎焊(FSB)连接. 对焊接接头进行了拉剪和抗撕裂试验,并与无任何过渡层接头进行了对比. 用扫描电镜及能谱对接头界面形貌和微观组织进行了分析,研究分析了过渡层对铝/钢FSB接头力学性能和微观组织的影响. 结果表明,过渡层能有效阻止脆性Al-Fe金属间化合物的生成,增加了接头抗撕裂载荷强度,提高接头的力学性能.     

相变超塑性扩散连接方法及工艺研究

利用相变超塑性现象 ,在自制的电阻加热扩散连接试验机上 ,对扩散连接的方法以及热作模具钢 3Cr2W8V与H13扩散连接接头的性能进行了试验研究 ,分析了不同条件对接头显微组织和连接效果的影响。结果表明 :本试验条件下按优选工艺参数连接的试样在拉断试验时 ,断裂发生在基体处 ,表明接头强度已不低于基体强度     

铜-铝异种金属超声波焊缝成型机制与接头性能研究

对铜箔-铝箔进行超声波焊接试验研究,优化设计工艺参数;采用金相显微镜、能谱仪、扫描电镜等分析焊接接头的微观组织;采用高速摄影系统实时监控焊接过程,研究超声波焊缝成型机制。结果表明:焊接压力、焊接振幅、焊接时间对接头性能影响很大,这些工艺参数过大或过小都会使接头强度降低。当焊接压力0.20 MPa,焊接振幅30μm,焊接时间0.05 s时,接头强度达到最大值,破断拉伸力为200 N。保持压力和振幅不变,随着焊接时间的增加,铜-铝接头的有效连接长度增加,接头强度增加;进一步增加焊接时间,铜-铝接头有效连接长度没有明显变化,接头强度下降。超声波焊接可分为四个过程:初始接触,摩擦产热,焊接软化,固相结合。     

12Cr2MoV/TP304H异种钢管瞬时液相扩散焊

采用氩气保护.用Fe基和BNi2合金箔作为中间层,进行了12Cr2MoV贝氏体耐热钢和TP304H奥氏体不锈钢管的瞬时液相扩散连接,分析了接头的力学性能、显微组织和断121特征,确定出了合适的连接工艺参数.研究表明,在合适的工艺参数下,用Fe基-BNirFe基三层中间层连接的接头室温下的拉伸强度和弯曲强度等于或超过基体.     

新型的治疗阿尔茨海默氏症药物(1-二甲基磷酰基-2,2,2-三氯)-乙基-1-醇烟酸醋对体外神经细胞的作用

目的: 观察本实验室合成的一种治疗阿尔茨海默氏症(AD)的药物(1-二甲基磷酰基-2, 2, 2 -三氯)-乙基^-1-醇烟酸醋(NMF),对体外培养的皮层神经细胞活性的影响以及对海人藻酸(KA)所致的神经损伤的保护作用。方法: 采用体外培养皮层神经元的方法,解剖分离 15 d胚胎小鼠皮层神经细胞, 接种于 96孔板,48 h 后加药并培养 72 h,以 MIT 法 观察 NMF 对小鼠皮层神经细胞活性的影响;同时将接种于 24 孔板的细胞预先给予 NMF,d 3 时加或不加KA处理后,以台盼蓝染色鉴别并计数死、活细胞,可得出细胞的存活率。结果: NMF 明显促进胎鼠皮层神经元活性,其中 NMF1、0. 1、10nmol·L^-1促进神经元活性增殖率分别高达 34.7%、37.4%、36. 7%, NMF 明显促进正常胎鼠皮层神经元存活卒,与对照组比较,10nmol·L^-1 NMF 对皮层神经元的存活率分别提高 39.3%、73.5%。 NMF能显著 对抗 KA 所致的神经元损伤,与 KA 损伤组相比, NMF0.1、10、10nmol·L^-1对损伤皮层神经元的保护率分别为 77.30%、80.10%、84.15%。结论: NMF 明 显促进胎鼠皮层神经元的洁性、提高正常皮层神经元,的存活卒,并能有效地保护KA所致的神经元损伤,提示 NMF 是一种很有潜力的治疗 AD 的药物。     

Rheology Feature of Simple Metal Melt

The rheology feature of Sb, Bi melt and alloys was studied using coaxial cylinder high-temperature viscometer. The results showed that the curve of torsion-rotational speed for Sb melt presents a linear relation in all measured temperature ranges, whereas for the Bi melt, the curve presents obvious non-Newtonian feature within the low temperature range and at relative high shear stress. The rheology feature of Sb80Bi20 and Sb20Bi80 alloy melts was well correlated with that of Sb and Bi, respectively. It is considered that the rheology behavior of Sb melt plays a crucial role in Sb80Bi20 alloy and that of Bi melt plays a crucial role in Sb20Bi80 alloy.     

Microstructures and Mechanical Properties of a Newly Developed Austenitic Heat Resistant Steel

The effect of heat treatment on the microstructures and mechanical properties of a newly developed austenitic heat resistant steel(named as T8 alloy) for ultra-supercritical applications have been studied. Results show that the main phases in the alloy after solution treatment are γ and primary MX. Subsequent aging treatment causes the precipitation of M_(23)C_6 carbides along the grain boundaries and a small number of nanoscale MX inside the grains. In addition, with increasing the aging temperature and time, the morphology of M_(23)C_6 carbides changes from semi-continuous chain to continuous network.Compared with a commercial HR3C alloy, T8 alloy has comparable tensile strength, but higher stress rupture strength. The dominant cracking mechanism of the alloy during tensile test at room temperature is transgranular, while at high temperature, intergranular cracking becomes the main cracking mode, which may be caused by the precipitation of continuous M_(23)C_6 carbides along the grain boundaries. Typical intergranular cracking is the dominant cracking mode of the alloy at all stress rupture tests.     

Three-Dimensional Growth of Coherent Ferrite in Austenite: A Molecular Dynamics Study

Coherent second phase often exhibits anisotropic morphology with specifi c orientations with respect to both the second and the matrix phases. As a key feature of microstructure, the morphology of the coherent particles is essential for understanding the second-phase strengthening eff ect in various industrial alloys. This letter reports anisotropic growth of coherent ferrite from austenite matrix in pure iron based on molecular dynamics simulation. We found that the ferrite grain tends to grow into an elongated plate-like shape, independent of its initial confi guration. The fi nal shape of the ferrite is closely related to the misfi t between the two phases, with the longest direction and the broad facet of the plate being, respectively, consistent with the best matching direction and the best matching plane calculated via the Burgers vector content(BVC) method. The strain energy calculation in the framework of Eshelby's inclusion theory verifi es that the simulated orientation of the coherent ferrite is energetically favorable. It is anticipated that the BVC method will be applicable in analysis of anisotropic growth and morphology of coherent second phase in other phase transformation systems.     

The 15th Global Foundry Sourcing Conference 2014held in Qingdao China

Organized by Suppliers China Co., Ltd and co-organized by the National Technical Committee 54 on Foundry of Standardization Administration of China, the 15th Global Foundry Sourcing Conference 2014 （hereinafter referred to as FSC 2014） was successfully held on Sep. 23rd in Grand Regency Hotel, Qingdao. More than 500 delegates from home and abroad attended this conference, including over 130 purchasers from 20 countries and 380 domestic and foreign suppliers.     

Secondary Recrystallization Behaviors of Grain-Oriented 6.5 wt% Silicon Steel Sheets Produced by Rolling and Nitriding Processes

By rolling and nitriding processes, 0.23- to 0.3-mm-thick grain-oriented 6.5 wt% silicon steel sheets were produced. The core losses of grain-oriented 6.5 wt% silicon steel at frequencies ranging from 400 Hz to 20 k Hz were lower than that of the grain-oriented 3 wt% silicon steel with the same thickness by 16.6–35.8%. The secondary recrystallization behavior was investigated by scanning electron microscopy, energy-dispersive spectroscopy, and electron backscattered diffraction. The results show that the secondary recrystallization in high-silicon steel sheets develops more completely as the nitrogen content increases after nitriding, secondary recrystallized grain sizes become larger, and the sharpness of Goss texture increases. Because more {110}116 grains in the subsurface and the central layer of the sheets have a lot of 20°–45° high-energy boundaries in addition to Goss grains, {110}116 can be the main component through selective growth during secondary recrystallization when the inhibitor quantity is not enough and inhibitor intensity is weaker. The increases in nitrogen content can increase the inhibitor intensity and hinder abnormal growth of a mount of {110}116 grains and therefore enhance the sharpness of Goss texture.     

Laser Cladded TiCN Coatings on the Surface of Titanium

Laser cladded coatings of TiCN were produced on the surface of titanium. To obtain the optimal techniques, several conditions were tested by varying the laser scanning rate. The choice of shielding gas was also studied. The cladded coatings were then evaluated from the surface mechanics point of view based on their microhardness. The microstructure of some interesting samples was investigated by optical micrographs (OM). The results showed that under the condition of fixed pulse frequency and pulse width, the laser scanning rate and the shielding gas are the main factors influencing the components of coatings. TiCN coatings were decompounded and oxidized during the cladding process in the condition of no shielding gas of N2. X-ray diffraction results indicated that the composite coatings composed of TiCN, TiC, Ti2N, and TiO2 were produced using appropriate techniques. The results indicated that the best condition in terms of the surface microhardness is obtained when the scanning rate is 1.5mm / s, the pulse frequency is 15Hz, the pulse width is 3.0ms, and N2 is chosen as the shielding gas. The microhardness of the composite coatings is about 1331kg · mm - 2, which is about 4 times that of the substrate. The optical micrographs indicated that the cladding zone is made up of TiCN, TiO2, and some interdendritic Ti, but the diffusion zone mainly consists of the dendrites phase, and the cladded depth is about 80?滋m, which is more than 2 times that of the laser nitrided sample. There were no microcracks or air bubbles in the cladded sample, which was cladded using the above optimal techniques.     

Effect of Short-Time Aging on the Pitting Corrosion Behavior of a Novel Lean Duplex Stainless Steel 2002

The effect of short-time aging in the temperature range between 400 and 1000 °C on the pitting corrosion behavior and mechanical property of a novel lean duplex stainless steel(LDSS) 2002 was investigated through the potentiostatic critical pitting temperature(CPT) tests and the Charpy impact tests. Both the pitting corrosion resistance and the toughness of aged specimens degraded due to the precipitation of detrimental secondary phases and the most significant reduction of CPT and impact energy emerged at 650 °C concurrently. The CPT of LDSS 2002 specimen aged at 650 °C decreased by 28 °C, and the impact energy dropped from 69 to 29 J/cm~2 compared with the solution-annealed sample. Transmission electron microscopy characterization showed that the main precipitates in LDSS 2002 were Cr_2N and M_(23)C_6 along the ferrite–austenite grain boundaries.     

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正The Transactions of Nonferrous Metals Society of China,founded in 1991 and sponsored by The Nonferrous Metals Society of China,is published monthly now and mainly contains reports of original research which reflect the new progresses in the field of nonferrous metals science and technology,including mineral processing,extraction metallurgy,metallic materials and heat treatments,metal working,physical metallurgy,powder metallurgy,with the emphasis